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丙烯酸-2,4,6-三硝基苯乙酯的合成及热分解 被引量:2
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作者 刘强强 金波 +3 位作者 彭汝芳 舒远杰 楚士晋 董海山 《含能材料》 EI CAS CSCD 北大核心 2012年第5期579-582,共4页
以TNT、甲醛为原料,在弱碱性条件下反应合成得到2,4,6-三硝基苯乙醇(PicCH2CH2OH);PicCH2CH2OH在浓硫酸催化下和丙烯酸在甲苯中回流反应24h,合成得到丙烯酸-2,4,6-三硝基苯乙酯,产率为62%。采用紫外可见光谱(UV-Vis)、核磁共振氢谱(1HN... 以TNT、甲醛为原料,在弱碱性条件下反应合成得到2,4,6-三硝基苯乙醇(PicCH2CH2OH);PicCH2CH2OH在浓硫酸催化下和丙烯酸在甲苯中回流反应24h,合成得到丙烯酸-2,4,6-三硝基苯乙酯,产率为62%。采用紫外可见光谱(UV-Vis)、核磁共振氢谱(1HNMR)、红外光谱(FTIR)、质谱(MS)以及元素分析等对产物结构进行了表征。利用热重分析(TG)对产物热稳定性进行了研究,采用Kissinger方法和Ozawa方法计算其热分解活化能Ea分别为99.78,102.96kJ·mol-1。 展开更多
关键词 有机化 2 4 6-三硝基苯乙醇 丙烯酸-2 4 6-三硝基苯乙酯 热稳定性 活化能
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情理与义理——论王阳明与程朱理学在理解孔子正名思想上的差异
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作者 肖平 《中国儒学》 2013年第1期159-173,共15页
阳明心学与程朱理学的比较一直为学界所关注,笔者近期整理王阳明《传习录》,其中阳明对孔子正名思想的一段独特诠释引起了笔者的关注,顺此线索,笔者进而发现以程颐等为代表的宋代儒家学者对孔子正名思想的不同诠释,针对同一历史事件,心... 阳明心学与程朱理学的比较一直为学界所关注,笔者近期整理王阳明《传习录》,其中阳明对孔子正名思想的一段独特诠释引起了笔者的关注,顺此线索,笔者进而发现以程颐等为代表的宋代儒家学者对孔子正名思想的不同诠释,针对同一历史事件,心学理学的不同诠释是否各有其思想根源?本文尝试分析之。 展开更多
关键词 思想 学与程 整理 事件 笔者 传习录
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In situ Colonization of Marine Biofilms on UNS S32760 Duplex Stainless Steel Coupons in Areas with Different Water Qualities: Implications for Corrosion Potential Behavior 被引量:2
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作者 Luciana V. R. de Messano Barbara L. Ignacio +1 位作者 Maria H. C. B. Neves Ricardo Coutinho 《Journal of Marine Science and Application》 2014年第3期346-353,共8页
In the presence of biofilms, stainless steels (SS) exhibits an increase in corrosion potential, called ennoblement. In the present study, the corrosion potential (Eco,) behavior of the duplex SS UNS S32760 was rec... In the presence of biofilms, stainless steels (SS) exhibits an increase in corrosion potential, called ennoblement. In the present study, the corrosion potential (Eco,) behavior of the duplex SS UNS S32760 was recorded simultaneously with the in situ marine biofilm formation in two areas at Arraial do Cabo, Southeastern Brazil. The biofilm at Forno Harbor (an anthropogenically disturbed area) was characterized by higher relative abundances of Bacteria at day 2, followed by diatoms (especially Navicula sp.) on day 10 and dinoflagellates on day 18, whereas no clear trend was recorded at Cabo Frio Island (an undisturbed area). The ennoblement of Ecor values was site-dependent. In a complementary laboratory assay, biofilms were removed and the Eco values registered in sterile conditions for the subsequent 10 days and corroborated in situ results. Understanding biofilms and SS interactions has important implications for materials science and engineering decisions as well as helping to fill in imnortant gaps in this knowledge. 展开更多
关键词 duplex stainless steel microbiologically influencedcorrosion corrosion potential ennoblement marine biofilm fieldexperiment
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快速自动成型技术及在实践中的应用
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作者 早热木.依玛尔 热依汗古丽.木沙 《现代机械》 2004年第1期50-51,共2页
本文论述了目前在工业化国家得到迅速发展的一种直接由计算机几何模型制成工件的新型制造技术———快速自动成型技术。内容包括 :快速自动成型技术的基本概念 ,还包括该技术在工业中的应用实例。
关键词 快速自动成型技术 增材制造 分层制造 快速原型制造
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Research on the Enterprise Strategic Management Course based on Problem Oriented Teaching Methodology
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作者 Qinghua Song Guohua Wu Jing Xue 《International Journal of Technology Management》 2015年第11期46-48,共3页
With the rapid development of the management science and technology, the management related course is becoming popular. In this research paper, we research on the enterprise strategic management course based on the pr... With the rapid development of the management science and technology, the management related course is becoming popular. In this research paper, we research on the enterprise strategic management course based on the problem oriented teaching methodology. We reviewed the latest strategic management recently developed various theories and academic point of view to from the theoretical level of modern enterprise strategy management pattern to generalize and summarize, thus to guide the strategic management of modern enterprises. Enterprise strategic management is to point to determine its mission according to the external environment and internal conditions set strategic goals of the enterprise. Through combing the development of the strategic management theory, grasp the context and the regularity of the evolution of enterprise strategic thinking and the development trend of enterprise strategic theory at home and abroad was discussed to promote the existing strategic management research provides some unique ideas and thoughts. 展开更多
关键词 Strategic Management Problem Oriented Teaching Methodology Enterprise.
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Multi-criteria decision-making selection model with application to chemical engineering management decisions
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作者 Mohsen Pirdashti Mehrdad Mohammad 《Journal of Agricultural Science and Technology》 2009年第8期53-62,共10页
Chemical industry project management involves complex decision making situations that require discerning abilities and methods to make sound decisions. Chemical engineers as project managers are faced with decision en... Chemical industry project management involves complex decision making situations that require discerning abilities and methods to make sound decisions. Chemical engineers as project managers are faced with decision environments and problems in chemical industry projects that are complex. Multiple-criteria decision making (MCDM) approaches are major parts of decision theory and analysis. This paper presents all of MCDM approaches for use in chemical engineering management decisions. In this work, case study is Research and Development (R&D) project selection in chemical industry. The ability to make sound decisions is very important to success of R&D projects. It is hoped that this work will provide a ready reference on MCDM and this will encourage the application of the MCDM in chemical engineering management. 展开更多
关键词 chemical engineering R&D project MCDM SELECTION
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基于小波消噪的EMD模型在GPS振动信号处理中的应用 被引量:4
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作者 李旋 孙磊 +2 位作者 骆辉 戴吾蛟 何伟 《工程勘察》 CSCD 北大核心 2011年第3期72-76,共5页
经验模式分解和小波分解是当前有效处理非平稳信号的两种时频分析方法,它们各具有其优缺点,适用于不同的应用。从对GPS振动信号的预处理、时域和频域处理入手,结果分析表明,对GPS振动信号先进行小波滤波消除随机噪声的干扰,再应用经验... 经验模式分解和小波分解是当前有效处理非平稳信号的两种时频分析方法,它们各具有其优缺点,适用于不同的应用。从对GPS振动信号的预处理、时域和频域处理入手,结果分析表明,对GPS振动信号先进行小波滤波消除随机噪声的干扰,再应用经验模式分解更有利于变形特征信息的分离和提取,提取的信号与振动平台记录数据更加吻合。 展开更多
关键词 经验模式分解(EMD) 小波分解(WD) 全球定位系统 振动变形
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Promoting Student Participation in Seminar Courses:A Case Study 被引量:1
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作者 张超 金利民 《Chinese Journal of Applied Linguistics》 2011年第3期54-71,127,128,共20页
Using a conversation analysis approach, the present study investigates the teacher-led question-answer sequences of one successful seminar course (Short Stories and Western Culture) within the curriculum reform for ... Using a conversation analysis approach, the present study investigates the teacher-led question-answer sequences of one successful seminar course (Short Stories and Western Culture) within the curriculum reform for English majors in Beijing Foreign Studies University, aiming at uncovering an effective way of integrating disciplinary learning with language skills development. The result of the analysis shows that the teacher of the course, who perceives student participation as an indispensable ingredient of his class, often uses more divergent, opinion-seeking questions to initiate discussion and uses four types of expansion question on his turns to promote student participation, namely, probing questions (PQ), clue-giving questions (CQ), elaboration requests (ER), and agreement checks (AC). The study also generates an I-R-(E)-F-FC [Initiation-Response-(Evaluation)-FoUow up-Further Contribution] model, in which the teacher attempts to promote student participation and guide the construction of students' understanding. 展开更多
关键词 seminar courses student participation question-answer sequence conversation analysis
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