P-methoxy-N,N-bis(2-cyanoethyl)aniline was synthesized by using p-methoxyaniline,acrylonitrile,AlCl3 and BE.The experimental result had proved that AlCl3 and BE was an excellent catalyst system.The appropriate reactiv...P-methoxy-N,N-bis(2-cyanoethyl)aniline was synthesized by using p-methoxyaniline,acrylonitrile,AlCl3 and BE.The experimental result had proved that AlCl3 and BE was an excellent catalyst system.The appropriate reactive condition is that AlCl3 was 20%(mol) of p-methoxyaniline,BE was 10%(mol) of p-methoxyaniline,the reaction temperature was 78℃ and the reaction time was 8 hours.The catalyst system had high catalyst efficiency and selectivity together with yield over 94%.展开更多
文摘P-methoxy-N,N-bis(2-cyanoethyl)aniline was synthesized by using p-methoxyaniline,acrylonitrile,AlCl3 and BE.The experimental result had proved that AlCl3 and BE was an excellent catalyst system.The appropriate reactive condition is that AlCl3 was 20%(mol) of p-methoxyaniline,BE was 10%(mol) of p-methoxyaniline,the reaction temperature was 78℃ and the reaction time was 8 hours.The catalyst system had high catalyst efficiency and selectivity together with yield over 94%.
