TiO2 nanotube arrays (TNTs) electrode loaded with Zn nanoparticles was prepared by anodization and the size of Zn nanoparticle loaded on TNTs electrode was controlled by chronoamperometry deposition time. Results of...TiO2 nanotube arrays (TNTs) electrode loaded with Zn nanoparticles was prepared by anodization and the size of Zn nanoparticle loaded on TNTs electrode was controlled by chronoamperometry deposition time. Results of SEM and XRD analysis show that Zn nanoparticles had a diameter of about 15-25 nm when the deposition time was 3-5 s. The UV-Vis diffuse reflectance spectra show the Zn loaded harvest light with 480-780 nm more effectively than the unloaded sample. The photocurrent response of Zn loaded TNTs electrodes were studied, the results showed that TNTs electrodes loaded with Zn nanoparti-cles has 50% increased photocurrent response under high-pressure mercury lamp irradiation compared with unloaded TNTs electrode.展开更多
The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscat...The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscatter diffraction (EBSD) and X-ray diffraction (XRD).The deformation condition of hot compression is 350 ℃,0.1 s?1.The microstructural evolution under TRC-HC deformation followed by annealing at different temperatures and time was discussed.The results show that TRC provides more modified microstructure compared with DC.Twins are found in TRC processing;dynamic recrystallization (DRX),shear bands and twins are found in TRC-HC.A short annealing time has little effect on hardness,while during a long time annealing,it is found that low annealing temperatures increase the micro-hardness and high temperature decreases it.展开更多
The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the comp...The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the composites.The relationship between the performance of depositing coat and pH value,temperature,reaction time and the way of agitation was studied.Results show that the depositing quality is stable under pH between 4.5 and 5.0,temperature between 75 ℃ and 85 ℃,reaction time for 10 min and air agitation.The uniform and compact nickel layer deposited on carbon fibers was proved by XRD and SEM,and the electrical resistivity of carbon fibers with nickel coating was tested.Results indicate that the electrical resistivity of carbon fibers with electroless nickel plating is decreased by an order of magnitude compared with that of carbon fibers.It means that nickel coating can greatly improve the electromagnetic interference shielding properties of carbon fibers.展开更多
Al-doped ZnO (ZAO) films were successfully deposited on the surface of common glasses by using low-temperature hydrothermal approach. In the reaction solution, the molar ratio of Al3+ to Zn2+ was 1∶100, the annealing...Al-doped ZnO (ZAO) films were successfully deposited on the surface of common glasses by using low-temperature hydrothermal approach. In the reaction solution, the molar ratio of Al3+ to Zn2+ was 1∶100, the annealing temperature and time were 200 ℃ and 2-6 h, respectively. The structure of the thin films was identified by X-ray diffraction (XRD), the surface morphology and thickness of the thin films were observed by scanning electron microscopy (SEM), and the electrical performance of the thin films was measured by four-point probes. It was shown that the films with an average particle size of 27.53 nm had a preferential orientation along (002), Al3+ had replaced the position of Zn2+ in the lattice without forming the Al2O3 phase and its thickness was 20-25 μm. With the increased annealing time, the intensity of diffraction peaks was decreased, the film exhibited irregular surface morphology gradually, and the resistivity of ZAO films was increased. The lowest resistivity obtained in this study was 3.45×10-5Ω·cm.展开更多
Emission in the X-ray and ultraviolet (200-300 nanometers) region of spectrum is found out during combustion of heterogeneous systems with the formation of condensed products, and pulses from microwave emission with...Emission in the X-ray and ultraviolet (200-300 nanometers) region of spectrum is found out during combustion of heterogeneous systems with the formation of condensed products, and pulses from microwave emission with short duration are recorded as well. Combustion of a Ti-B powder system showed that self-propagating high-temperature synthesis (SHS) is accompanied by two types of X-ray radiation. Radiation of the first type has the maximum quantum energy - 5 keV. It is supposed that this type is caused by micro-breakdowns due to the charge separation in combustion products. Runaway electrons and soft X-ray radiation are generated due to the concentration of electric field on microparticles during breakdown. Radiation of the second type has the quantum energy up to - 15 keV. It is supposed that it is caused by exoemission of photons. UV radiation in the region of 200-300 nm is recorded during SHS in different gases (He, Ar, N2). This radiation is shown to have the highest intensity in helium at the pressure - 25 x 103 Pa.展开更多
Objective:The optimal treatment of patients with metastatic spinal cord compression(MSCC) is still being debated.This randomized trial was planned to compare the functional outcome and its related prognostic factors,t...Objective:The optimal treatment of patients with metastatic spinal cord compression(MSCC) is still being debated.This randomized trial was planned to compare the functional outcome and its related prognostic factors,toxicity and in-field recurrence of the three schedules of radiotherapy.Methods:Two hundred and eighty five patients enrolled in the study of which 95 received 1 × 8 Gy,100 received 10 x 3 Gy and 90 received the radiation treatment of 20 × 2 Gy.Irradiation was performed with 6-10 Mv linear accelerators or cobalt-60 units by single posterior field or parallel opposed fields according to depth of irradiation spines.Premedication with dexamethasone was started from the first day of clinico-radiologic diagnosis till 4-5 days after the end of radiotherapy(RT) then tapered off during 10 days.Potential prognostic factors were evaluated with respect to functional outcome.Results:All groups were balanced for patient's characteristics and potential prognostic factors.No statistically significant difference was observed between the 3 groups as regard functional outcome and toxicity while single fraction was associated with higher in-field recurrences(22.8%) with statistically significant difference between the 3 groups(P = 0.01).Functional outcome was significantly better with younger age(≤ 60 y),Eastern Cooperative Oncology Group performance status(ECOG-PS) of 1-2,involved vertebra of 1-2,favorable tumor type,absence of visceral or other bone metastasis,decreased time of developing motor deficit before radiotherapy,long interval between cancer diagnosis to metastatic spinal cord compression,and normal ambulatory status.Conclusion:The three schedules provided similar functional outcome.Single-radiation dose was associated with higher in-field recurrence.To minimize treatment time and costs,the dose of 1 × 8 Gy is recommended for patients with poor predicated survival and 10 × 3 Gy for other patients.展开更多
In order to protect historical ciphertext when the private key leaked in the broadcasting system,the forward-secure multi-receiver signcryption scheme is designed based on the generic graded multilinear mapping encodi...In order to protect historical ciphertext when the private key leaked in the broadcasting system,the forward-secure multi-receiver signcryption scheme is designed based on the generic graded multilinear mapping encoding structure,which effectively prevents illegal access from intruder to the ciphertext in the past time period when the private key in current time period is revealed.Through the generalization of the existing multilinear mapping encoding system,it proposes the generic graded multilinear mapping encoding structure and the generic graded decision Diffie-Hellman problem.Because of the generic graded multilinear mapping encoding system adopted,almost all candidate multilinear mapping encoding systems can automatically adapt to our scheme.Under the assumption of generic graded decision Diffie-Hellman problem,it has proved that the scheme has the information confidentiality and unforgeability in the current time period.After putting forward the security model of forward-secure multi-receiver signcryption scheme,and under the assumption of generic graded decision Diffie-Hellman problem,it has proved that the scheme has the message forward-confidentiality and forward-unforgeability.Compared with other forward-secure public key encryption schemes,the relationship between our scheme and time periods is sub-linear,so it is less complex.展开更多
Based on the new data from the database of the University of Michigan Radio Astronomy Observatory (UMRAO), we analyze the spectral index and optical variability of OJ287 and 3C279. The main results show that 1) the...Based on the new data from the database of the University of Michigan Radio Astronomy Observatory (UMRAO), we analyze the spectral index and optical variability of OJ287 and 3C279. The main results show that 1) the time delay among three radio bands (4.8, 8, and 14.5 GHz) shows: r8-14.5 = 31 d, r4.8-8 = 41 d for OJ287, but no time delay lying in 3C279; 2) strong correlation lies in the polarization and flux density at 8 GHz for OJ287 and at 8, 14.5 GHz for 3C279; 3) the logarithmic brightness temperature log(TB) = 14.l K for OJ287 is 14.1 K, log(TB) = 15.1 K for 3C279.展开更多
The mono-frequency peak luminosity and the corresponding photon energy of the time-integrated (L~, Eg) and peak time (L~, ffp) vfv spectra were derived for a sample of 38 redshift-known Fermi GRBs by fitting the s...The mono-frequency peak luminosity and the corresponding photon energy of the time-integrated (L~, Eg) and peak time (L~, ffp) vfv spectra were derived for a sample of 38 redshift-known Fermi GRBs by fitting the spectra with the Band function. It was found that Ept is generally consistent with Ep, and Lp is averagely three times larger than Lp. The slope of the Lp1 -Etp relation was consistent with that of the Lps - Eps relation. The photon indices in the peak time spectrum, particularly, the index of the low energy end was, were statistically larger than that in the time-integrated spectrum. These results indicate that Lp and Ep are dominated by Lp1 and Ept, respectively. The difference of the spectral indices between the time-integrated and peak time spectra may be because of the overlap effect of a series of time-resolved spectra within a GRB. Our simulations, which were based on the observed spectral evolution and correlation between the energy flux and the peak energy within individual GRBs support our speculations. The Lt - Et, relation may be less contaminated by the overla!a effect, and it would may be an intrinsic feature of radiation ohvsics.展开更多
Cosmic rays(CR)play an important role in space weather-related studies.Their temporal variability,both of a quasi-periodic character as well as an irregular one,has been studied from ground-based direct measurements,a...Cosmic rays(CR)play an important role in space weather-related studies.Their temporal variability,both of a quasi-periodic character as well as an irregular one,has been studied from ground-based direct measurements,as well as from cosmogenic nuclides,over a long time.We attempt to describe the current knowledge of selected quasi-periodicities in CR flux in the energy range above the atmospheric threshold,from direct measurements.The power spectrum density(PSD)of the CR time series as measured by neutron monitors(NMs)and by muon detectors has a rather complicated character.Along with the shape(slope)of the PSD,knowledge of the contribution of quasi-periodic variations(q-per)to the CR signal is of importance for the modulation,as well as for checking the links of CR to space weather,and/or to space climate effects.The rotation of the Earth and solar rotation cause two types of mechanisms behind the certain q-per observed in secondary CR on the Earth’s surface.Solar activity and solar magnetic field cyclicities contribute to the q-per signals in CR if studied over a longer time.The complexity of the spatial structure of the interplanetary magnetic field(IMF)and its evolution within the heliosphere,in addition to the changes in the geomagnetic field,cause variability in contributions of the q-per in CR.Wavelet spectra are useful tools for checking the fine structure of q-per and their temporal behaviour.Over a long time NMs and muon telescopes provide information about q-per in CR.展开更多
基金ACKNOWLEDGMENTS This work was supported by the Science Foundation of Chongqing Science and Technology Committee (No.CSTS2009BB4047), and Innovative Talent Training Project, the Third Stage of "211 Project" of Chongqing University (No.S-09109).
文摘TiO2 nanotube arrays (TNTs) electrode loaded with Zn nanoparticles was prepared by anodization and the size of Zn nanoparticle loaded on TNTs electrode was controlled by chronoamperometry deposition time. Results of SEM and XRD analysis show that Zn nanoparticles had a diameter of about 15-25 nm when the deposition time was 3-5 s. The UV-Vis diffuse reflectance spectra show the Zn loaded harvest light with 480-780 nm more effectively than the unloaded sample. The photocurrent response of Zn loaded TNTs electrodes were studied, the results showed that TNTs electrodes loaded with Zn nanoparti-cles has 50% increased photocurrent response under high-pressure mercury lamp irradiation compared with unloaded TNTs electrode.
基金Project(10020072) supported by the Korean Ministry of Commerce,Industry and EnergyProject(Y2008F27) supported by the Natural Science Foundation of Shandong Province,China
文摘The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscatter diffraction (EBSD) and X-ray diffraction (XRD).The deformation condition of hot compression is 350 ℃,0.1 s?1.The microstructural evolution under TRC-HC deformation followed by annealing at different temperatures and time was discussed.The results show that TRC provides more modified microstructure compared with DC.Twins are found in TRC processing;dynamic recrystallization (DRX),shear bands and twins are found in TRC-HC.A short annealing time has little effect on hardness,while during a long time annealing,it is found that low annealing temperatures increase the micro-hardness and high temperature decreases it.
文摘The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the composites.The relationship between the performance of depositing coat and pH value,temperature,reaction time and the way of agitation was studied.Results show that the depositing quality is stable under pH between 4.5 and 5.0,temperature between 75 ℃ and 85 ℃,reaction time for 10 min and air agitation.The uniform and compact nickel layer deposited on carbon fibers was proved by XRD and SEM,and the electrical resistivity of carbon fibers with nickel coating was tested.Results indicate that the electrical resistivity of carbon fibers with electroless nickel plating is decreased by an order of magnitude compared with that of carbon fibers.It means that nickel coating can greatly improve the electromagnetic interference shielding properties of carbon fibers.
文摘Al-doped ZnO (ZAO) films were successfully deposited on the surface of common glasses by using low-temperature hydrothermal approach. In the reaction solution, the molar ratio of Al3+ to Zn2+ was 1∶100, the annealing temperature and time were 200 ℃ and 2-6 h, respectively. The structure of the thin films was identified by X-ray diffraction (XRD), the surface morphology and thickness of the thin films were observed by scanning electron microscopy (SEM), and the electrical performance of the thin films was measured by four-point probes. It was shown that the films with an average particle size of 27.53 nm had a preferential orientation along (002), Al3+ had replaced the position of Zn2+ in the lattice without forming the Al2O3 phase and its thickness was 20-25 μm. With the increased annealing time, the intensity of diffraction peaks was decreased, the film exhibited irregular surface morphology gradually, and the resistivity of ZAO films was increased. The lowest resistivity obtained in this study was 3.45×10-5Ω·cm.
文摘Emission in the X-ray and ultraviolet (200-300 nanometers) region of spectrum is found out during combustion of heterogeneous systems with the formation of condensed products, and pulses from microwave emission with short duration are recorded as well. Combustion of a Ti-B powder system showed that self-propagating high-temperature synthesis (SHS) is accompanied by two types of X-ray radiation. Radiation of the first type has the maximum quantum energy - 5 keV. It is supposed that this type is caused by micro-breakdowns due to the charge separation in combustion products. Runaway electrons and soft X-ray radiation are generated due to the concentration of electric field on microparticles during breakdown. Radiation of the second type has the quantum energy up to - 15 keV. It is supposed that it is caused by exoemission of photons. UV radiation in the region of 200-300 nm is recorded during SHS in different gases (He, Ar, N2). This radiation is shown to have the highest intensity in helium at the pressure - 25 x 103 Pa.
文摘Objective:The optimal treatment of patients with metastatic spinal cord compression(MSCC) is still being debated.This randomized trial was planned to compare the functional outcome and its related prognostic factors,toxicity and in-field recurrence of the three schedules of radiotherapy.Methods:Two hundred and eighty five patients enrolled in the study of which 95 received 1 × 8 Gy,100 received 10 x 3 Gy and 90 received the radiation treatment of 20 × 2 Gy.Irradiation was performed with 6-10 Mv linear accelerators or cobalt-60 units by single posterior field or parallel opposed fields according to depth of irradiation spines.Premedication with dexamethasone was started from the first day of clinico-radiologic diagnosis till 4-5 days after the end of radiotherapy(RT) then tapered off during 10 days.Potential prognostic factors were evaluated with respect to functional outcome.Results:All groups were balanced for patient's characteristics and potential prognostic factors.No statistically significant difference was observed between the 3 groups as regard functional outcome and toxicity while single fraction was associated with higher in-field recurrences(22.8%) with statistically significant difference between the 3 groups(P = 0.01).Functional outcome was significantly better with younger age(≤ 60 y),Eastern Cooperative Oncology Group performance status(ECOG-PS) of 1-2,involved vertebra of 1-2,favorable tumor type,absence of visceral or other bone metastasis,decreased time of developing motor deficit before radiotherapy,long interval between cancer diagnosis to metastatic spinal cord compression,and normal ambulatory status.Conclusion:The three schedules provided similar functional outcome.Single-radiation dose was associated with higher in-field recurrence.To minimize treatment time and costs,the dose of 1 × 8 Gy is recommended for patients with poor predicated survival and 10 × 3 Gy for other patients.
基金Sponsored by the National Natural Science Foundation of China(Grant No.61401226,61672270,61602216)the MOE(Ministry of Education in China) Project of Humanities and Social Sciences(Grant No.14YJAZH023,15YJCZH129)+2 种基金the Basic Research Program of Jiangsu University of Technology(Grant No.KYY14007)the Qing Lan Project for Young Researchers of Jiangsu Province of China(Grant No.KYQ14004)the Open Fund of State Key Laboratory of Information Security,Institute of Information Engineering,Chinese Academy of Sciences(Grant No.2015-MSB-10)
文摘In order to protect historical ciphertext when the private key leaked in the broadcasting system,the forward-secure multi-receiver signcryption scheme is designed based on the generic graded multilinear mapping encoding structure,which effectively prevents illegal access from intruder to the ciphertext in the past time period when the private key in current time period is revealed.Through the generalization of the existing multilinear mapping encoding system,it proposes the generic graded multilinear mapping encoding structure and the generic graded decision Diffie-Hellman problem.Because of the generic graded multilinear mapping encoding system adopted,almost all candidate multilinear mapping encoding systems can automatically adapt to our scheme.Under the assumption of generic graded decision Diffie-Hellman problem,it has proved that the scheme has the information confidentiality and unforgeability in the current time period.After putting forward the security model of forward-secure multi-receiver signcryption scheme,and under the assumption of generic graded decision Diffie-Hellman problem,it has proved that the scheme has the message forward-confidentiality and forward-unforgeability.Compared with other forward-secure public key encryption schemes,the relationship between our scheme and time periods is sub-linear,so it is less complex.
基金supported by the National Natural Science Foundation of China (Grant No. 10633010)the National Basic Research Program of China (Grant No. 2007CB815405)+1 种基金the Bureau of Education of Guangzhou Municipality (Grant No. 11 Sui-Jiao-Ke[2009]),and GDUPS (2009)supported by the University of Michigan and the National Science Foundation
文摘Based on the new data from the database of the University of Michigan Radio Astronomy Observatory (UMRAO), we analyze the spectral index and optical variability of OJ287 and 3C279. The main results show that 1) the time delay among three radio bands (4.8, 8, and 14.5 GHz) shows: r8-14.5 = 31 d, r4.8-8 = 41 d for OJ287, but no time delay lying in 3C279; 2) strong correlation lies in the polarization and flux density at 8 GHz for OJ287 and at 8, 14.5 GHz for 3C279; 3) the logarithmic brightness temperature log(TB) = 14.l K for OJ287 is 14.1 K, log(TB) = 15.1 K for 3C279.
基金supported by the National Basic Research Program of China(Grant No.2014CB845800)the National Natural Science Foundation of China(Grant No.11025313)+1 种基金Guangxi Science Foundation(Grant No.2013GXNSFFA019001)Key Laboratory for the Structure and Evolution of Celestial Objects of Chinese Academy of Sciences,and the Strategic Priority Research Program"The Emergence of Cosmological Structures"of the Chinese Academy of Sciences(Grant No.XDB09000000)
文摘The mono-frequency peak luminosity and the corresponding photon energy of the time-integrated (L~, Eg) and peak time (L~, ffp) vfv spectra were derived for a sample of 38 redshift-known Fermi GRBs by fitting the spectra with the Band function. It was found that Ept is generally consistent with Ep, and Lp is averagely three times larger than Lp. The slope of the Lp1 -Etp relation was consistent with that of the Lps - Eps relation. The photon indices in the peak time spectrum, particularly, the index of the low energy end was, were statistically larger than that in the time-integrated spectrum. These results indicate that Lp and Ep are dominated by Lp1 and Ept, respectively. The difference of the spectral indices between the time-integrated and peak time spectra may be because of the overlap effect of a series of time-resolved spectra within a GRB. Our simulations, which were based on the observed spectral evolution and correlation between the energy flux and the peak energy within individual GRBs support our speculations. The Lt - Et, relation may be less contaminated by the overla!a effect, and it would may be an intrinsic feature of radiation ohvsics.
基金Project VEGA 2/0040/13 for supportKuwait for supporting project HS-13-01
文摘Cosmic rays(CR)play an important role in space weather-related studies.Their temporal variability,both of a quasi-periodic character as well as an irregular one,has been studied from ground-based direct measurements,as well as from cosmogenic nuclides,over a long time.We attempt to describe the current knowledge of selected quasi-periodicities in CR flux in the energy range above the atmospheric threshold,from direct measurements.The power spectrum density(PSD)of the CR time series as measured by neutron monitors(NMs)and by muon detectors has a rather complicated character.Along with the shape(slope)of the PSD,knowledge of the contribution of quasi-periodic variations(q-per)to the CR signal is of importance for the modulation,as well as for checking the links of CR to space weather,and/or to space climate effects.The rotation of the Earth and solar rotation cause two types of mechanisms behind the certain q-per observed in secondary CR on the Earth’s surface.Solar activity and solar magnetic field cyclicities contribute to the q-per signals in CR if studied over a longer time.The complexity of the spatial structure of the interplanetary magnetic field(IMF)and its evolution within the heliosphere,in addition to the changes in the geomagnetic field,cause variability in contributions of the q-per in CR.Wavelet spectra are useful tools for checking the fine structure of q-per and their temporal behaviour.Over a long time NMs and muon telescopes provide information about q-per in CR.