The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the comp...The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the composites.The relationship between the performance of depositing coat and pH value,temperature,reaction time and the way of agitation was studied.Results show that the depositing quality is stable under pH between 4.5 and 5.0,temperature between 75 ℃ and 85 ℃,reaction time for 10 min and air agitation.The uniform and compact nickel layer deposited on carbon fibers was proved by XRD and SEM,and the electrical resistivity of carbon fibers with nickel coating was tested.Results indicate that the electrical resistivity of carbon fibers with electroless nickel plating is decreased by an order of magnitude compared with that of carbon fibers.It means that nickel coating can greatly improve the electromagnetic interference shielding properties of carbon fibers.展开更多
This work aims to evaluate the feasibility of the fabrication of nanostructured Cu/Al/Ag multi-layered composites by accumulative roll bonding(ARB),and to analyze the tensile properties and electrical conductivity of ...This work aims to evaluate the feasibility of the fabrication of nanostructured Cu/Al/Ag multi-layered composites by accumulative roll bonding(ARB),and to analyze the tensile properties and electrical conductivity of the produced composites.A theoretical model using strengthening mechanisms and some structural parameters extracted from X-ray diffraction is also developed to predict the tensile strength of the composites.It was found that by progression of ARB,the experimental and calculated tensile strengths are enhanced,reach a maximum of about 450 and 510 MPa at the fifth cycle of ARB,respectively and then are reduced.The electrical conductivity decreased slightly by increasing the number of ARB cycles at initial ARB cycles,but the decrease was intensified at the final ARB cycles.In conclusion,the merit of ARB to fabricate this type of multi-layered nanocomposites and the accuracy of the developed model to predict tensile strength were realized.展开更多
Cu/Al multilayers were produced by high-temperature accumulative roll bonding(ARB)methods up to three passes.To achieve a high bonding strength,prior to ARB processing,the Cu and Al sheets were heated to 350,400,450 a...Cu/Al multilayers were produced by high-temperature accumulative roll bonding(ARB)methods up to three passes.To achieve a high bonding strength,prior to ARB processing,the Cu and Al sheets were heated to 350,400,450 and 500 ℃,respectively.The mechanical properties were evaluated by tensile tests.The microstructure was examined by optical microscopy and scanning electron microscopy equipped with energy dispersive spectrometry.The ultimate tensile stress,the grain size and the thickness of diffusion layer of lamellar composites increase with rolling temperature.When the rolling temperature is 400 ℃,the laminates show the highest ductility,but the yield stress is the lowest.As the rolling temperature further increases,both the yield stress and the ultimate tensile stress increase and the ductility decreases slightly.The mechanical properties of lamellar composites processed by low and high temperature ARB are determined by grain size and the thickness of diffusion layer,respectively.展开更多
Effects of current density, duty cycle and frequency on microstructure and particles content of electrodeposited Co-BN (hexagonal) nano composite coatings were analyzed by SEM, FESEM, EDS, AFM and XRD techniques. Th...Effects of current density, duty cycle and frequency on microstructure and particles content of electrodeposited Co-BN (hexagonal) nano composite coatings were analyzed by SEM, FESEM, EDS, AFM and XRD techniques. The microhardness, tribological behavior and wear mechanism were also investigated. Generally, as the current density and frequency increased, the particles content and microhardness of the coatings increased firstly and then decreased. Moreover, by reducing duty cycle, more particles were incorporated and higher microhardness was obtained. The best tribological behavior was achieved under the conditions duty cycle of 10%, frequency of 50 Hz and current density of 100 mA/cm2.展开更多
The investigating of the hot press process parameters on the flexural properties of LVL (Laminated Veneer Lumber) reinforced composites derived from rubber wood veneer reinforced with fiber glass woven and epoxy adh...The investigating of the hot press process parameters on the flexural properties of LVL (Laminated Veneer Lumber) reinforced composites derived from rubber wood veneer reinforced with fiber glass woven and epoxy adhesive were performed via the DOE (design of experimental) approach. It was discovered that pressure was the most significantly and negatively effect on the product properties. Enhancing in the mechanical properties was related to decrease the processing pressure. Beside, press time was also significantly and positively effect. Although time was not clearly reflect from the mechanical results, but it was detected from the ANOVA (analysis of variance)results. The mechanical properties were increased with increasing compression time. From the results, the optimal condition to maximize mechanical properties was assumed at low pressure, 15 bars, low temperature, 70℃, and long time, 60 mins. The durability testing including screw nail withdrawal strength, water absorption, and termite resistance of LVL reinforced composite were also studied. The results are shown that the LVL wood has superior properties when compare with solid woods. It was found the withdrawal strength of LVL reinforce composite was higher than the solid woods. As expected that solid woods, except eucalyptus, had low water absorption resistance as it more hygroscopic corresponded to LVL reinforced wood. Also solid woods, except teal(, had low resistance to termite attack. Therefore, LVL reinforced was the best candidate by mean of durability properties compared to solid wood.展开更多
An atomic layer deposition (ALD) method has been employed to synthesize Fe3O4/graphene and Ni/graphene composites. The structure and microwave absorbing properties of the as-prepared composites are investigated. The...An atomic layer deposition (ALD) method has been employed to synthesize Fe3O4/graphene and Ni/graphene composites. The structure and microwave absorbing properties of the as-prepared composites are investigated. The surfaces of graphene are densely covered by Fe3O4 or Ni nanoparticles with a narrow size distribution, and the magnetic nanoparticles are well distributed on each graphene sheet without significant conglomeration or large vacancies. The coated graphene materials exhibit remarkably improved electromagnetic (EM) absorption properties compared to the pristine graphene. The optimal reflection loss (RL) reaches -46.4 dB at 15.6 GHz with a thickness of only 1.4 mm for the Fe3O4/graphene composites obtained by applying 100 cycles of Fe2O3 deposition followed by a hydrogen reduction. The enhanced absorption ability arises from the effective impedance matching, multiple interfacial polarization and increased magnetic loss from the added magnetic constituents. Moreover, compared with other recently reported materials, the composites have a lower filling ratio and smaller coating thickness resulting in significantly increased EM absorption properties. This demonstrates that nanoscale surface modification of magnetic particles on graphene by ALD is a very promising way to design lightweight and high-efficiency microwave absorbers.展开更多
文摘The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the composites.The relationship between the performance of depositing coat and pH value,temperature,reaction time and the way of agitation was studied.Results show that the depositing quality is stable under pH between 4.5 and 5.0,temperature between 75 ℃ and 85 ℃,reaction time for 10 min and air agitation.The uniform and compact nickel layer deposited on carbon fibers was proved by XRD and SEM,and the electrical resistivity of carbon fibers with nickel coating was tested.Results indicate that the electrical resistivity of carbon fibers with electroless nickel plating is decreased by an order of magnitude compared with that of carbon fibers.It means that nickel coating can greatly improve the electromagnetic interference shielding properties of carbon fibers.
文摘This work aims to evaluate the feasibility of the fabrication of nanostructured Cu/Al/Ag multi-layered composites by accumulative roll bonding(ARB),and to analyze the tensile properties and electrical conductivity of the produced composites.A theoretical model using strengthening mechanisms and some structural parameters extracted from X-ray diffraction is also developed to predict the tensile strength of the composites.It was found that by progression of ARB,the experimental and calculated tensile strengths are enhanced,reach a maximum of about 450 and 510 MPa at the fifth cycle of ARB,respectively and then are reduced.The electrical conductivity decreased slightly by increasing the number of ARB cycles at initial ARB cycles,but the decrease was intensified at the final ARB cycles.In conclusion,the merit of ARB to fabricate this type of multi-layered nanocomposites and the accuracy of the developed model to predict tensile strength were realized.
基金Project(51674303) supported by the National Natural Science Foundation of ChinaProject supported by National Youth Thousand Plan of China+2 种基金Project(2018RS3015) supported by Huxiang High-Level Talent Gathering Program of Hunan Province,ChinaProject(2019CX006) supported by Innovation Driven Program of Central South University,ChinaProject supported by the Research Fund of the Key Laboratory of High Performance Complex Manufacturing at Central South University,China
文摘Cu/Al multilayers were produced by high-temperature accumulative roll bonding(ARB)methods up to three passes.To achieve a high bonding strength,prior to ARB processing,the Cu and Al sheets were heated to 350,400,450 and 500 ℃,respectively.The mechanical properties were evaluated by tensile tests.The microstructure was examined by optical microscopy and scanning electron microscopy equipped with energy dispersive spectrometry.The ultimate tensile stress,the grain size and the thickness of diffusion layer of lamellar composites increase with rolling temperature.When the rolling temperature is 400 ℃,the laminates show the highest ductility,but the yield stress is the lowest.As the rolling temperature further increases,both the yield stress and the ultimate tensile stress increase and the ductility decreases slightly.The mechanical properties of lamellar composites processed by low and high temperature ARB are determined by grain size and the thickness of diffusion layer,respectively.
文摘Effects of current density, duty cycle and frequency on microstructure and particles content of electrodeposited Co-BN (hexagonal) nano composite coatings were analyzed by SEM, FESEM, EDS, AFM and XRD techniques. The microhardness, tribological behavior and wear mechanism were also investigated. Generally, as the current density and frequency increased, the particles content and microhardness of the coatings increased firstly and then decreased. Moreover, by reducing duty cycle, more particles were incorporated and higher microhardness was obtained. The best tribological behavior was achieved under the conditions duty cycle of 10%, frequency of 50 Hz and current density of 100 mA/cm2.
文摘The investigating of the hot press process parameters on the flexural properties of LVL (Laminated Veneer Lumber) reinforced composites derived from rubber wood veneer reinforced with fiber glass woven and epoxy adhesive were performed via the DOE (design of experimental) approach. It was discovered that pressure was the most significantly and negatively effect on the product properties. Enhancing in the mechanical properties was related to decrease the processing pressure. Beside, press time was also significantly and positively effect. Although time was not clearly reflect from the mechanical results, but it was detected from the ANOVA (analysis of variance)results. The mechanical properties were increased with increasing compression time. From the results, the optimal condition to maximize mechanical properties was assumed at low pressure, 15 bars, low temperature, 70℃, and long time, 60 mins. The durability testing including screw nail withdrawal strength, water absorption, and termite resistance of LVL reinforced composite were also studied. The results are shown that the LVL wood has superior properties when compare with solid woods. It was found the withdrawal strength of LVL reinforce composite was higher than the solid woods. As expected that solid woods, except eucalyptus, had low water absorption resistance as it more hygroscopic corresponded to LVL reinforced wood. Also solid woods, except teal(, had low resistance to termite attack. Therefore, LVL reinforced was the best candidate by mean of durability properties compared to solid wood.
文摘An atomic layer deposition (ALD) method has been employed to synthesize Fe3O4/graphene and Ni/graphene composites. The structure and microwave absorbing properties of the as-prepared composites are investigated. The surfaces of graphene are densely covered by Fe3O4 or Ni nanoparticles with a narrow size distribution, and the magnetic nanoparticles are well distributed on each graphene sheet without significant conglomeration or large vacancies. The coated graphene materials exhibit remarkably improved electromagnetic (EM) absorption properties compared to the pristine graphene. The optimal reflection loss (RL) reaches -46.4 dB at 15.6 GHz with a thickness of only 1.4 mm for the Fe3O4/graphene composites obtained by applying 100 cycles of Fe2O3 deposition followed by a hydrogen reduction. The enhanced absorption ability arises from the effective impedance matching, multiple interfacial polarization and increased magnetic loss from the added magnetic constituents. Moreover, compared with other recently reported materials, the composites have a lower filling ratio and smaller coating thickness resulting in significantly increased EM absorption properties. This demonstrates that nanoscale surface modification of magnetic particles on graphene by ALD is a very promising way to design lightweight and high-efficiency microwave absorbers.