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水产品中地西泮胶体金快速检测卡产品性能评估
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作者 谢俊平 肖毅美 +1 位作者 吴文玲 许李仙 《农产品加工》 2024年第13期71-74,79,共5页
对水产品中地西泮胶体金快速检测卡的可靠性及实用性进行评价。通过制备地西泮胶体金快速检测卡,对其检出限、抗干扰性、稳定性等进行测试。结果表明,检测卡对地西泮的最低检出限为0.5μg/kg;检测盲样时,检测卡的假阳性率<5%,假阴性... 对水产品中地西泮胶体金快速检测卡的可靠性及实用性进行评价。通过制备地西泮胶体金快速检测卡,对其检出限、抗干扰性、稳定性等进行测试。结果表明,检测卡对地西泮的最低检出限为0.5μg/kg;检测盲样时,检测卡的假阳性率<5%,假阴性率为0;样品检测结果与液相色谱-质谱法检测结果相符;检测卡不受外源性干扰物质的影响;试纸在室温保存1年,仍然具有良好的稳定性;且同一批次内、5个批次间稳定性良好。检测卡法具有快速、准确、方便、灵敏等特点,适用于基层对水产品中地西泮残留进行定性分析。 展开更多
关键词 地西泮 胶体金免疫层析检测卡 水产品 灵敏度 干扰性测试 稳定
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High-frequency interference in low strain integrity testing of large-diameter pipe piles 被引量:19
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作者 DING XuanMing LIU HanLong ZHANG Bo 《Science China(Technological Sciences)》 SCIE EI CAS 2011年第2期420-430,共11页
The high-frequency interference exists obviously in low strain integrity testing of large-diameter pipe pile when a transientpoint load is applied. An analytical solution of vertical vibratory response of large-diamet... The high-frequency interference exists obviously in low strain integrity testing of large-diameter pipe pile when a transientpoint load is applied. An analytical solution of vertical vibratory response of large-diameter pipe piles in low strain testing isdeduced in this paper. The analytical solution is verified by both numerical simulation and model test results. The time-domainvelocity responses on pile top are analyzed. The calculation results indicate that the time-domain responses at various pointssuffer different high-frequency interferences, thus the peak values and phases of different points are different. The influence ofvibratory modes on high-frequency interference is analyzed. It is found that the high-frequency interference at 90° point main-ly derives from the second flexural mode, but for other points it mainly originates from the first flexural mode. The factors af-fecting the frequency and peak value of interference waves have been investigated in this study. The results indicate that thelarger radius angle between the receiving and 90° points leads to greater peak value of high frequency wave crest. The leasthigh-frequency interference is detected at the angle of 90°. The frequency of interference waves is decreased with the increaseof pile radius, while the peak value is almost constant. The frequency is also related to pile modulus, i.e. the larger pile modu-lus results in greater frequency. The peak value varies with impulse width and soil resistance, i.e., the wider impulse width andlarger soil resistance cause smaller peak value. In conclusion, the frequency of interference waves is dependent on the geomet-rical and mechanics characteristics of the piles such as pile radius and modulus, but independent of the external conditionssuch as impulse width and soil resistance. On the other hand, the peak value of interference waves is mainly dependent on theexternal conditions but independent of the geometrical and mechanics characteristics of the piles. In practice, some externalmeasures should be adopted to weaken high-frequency interference such as using soft hammer, hammer cushion and adoptingsuitable receiving point. 展开更多
关键词 large-diameter pipe pile low strain integrity testing high-frequency interference vibratory response analytic solution
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