期刊文献+
共找到12篇文章
< 1 >
每页显示 20 50 100
用凯氏定氮法测定植物干样品中的氮含量 被引量:32
1
作者 戴宏林 吴小骏 《江苏农学院学报》 CSCD 1995年第3期70-70,共1页
用凯氏定氮法测定植物干样品中的氮含量戴宏林,吴小骏(江苏农学院理化测试中心,扬州225009)自从1883年Kjeldahl提出测定全氮的方法以来,在改善方法的精确度、缩短消化时间,对不同样品的分析等方面已有不少研究... 用凯氏定氮法测定植物干样品中的氮含量戴宏林,吴小骏(江苏农学院理化测试中心,扬州225009)自从1883年Kjeldahl提出测定全氮的方法以来,在改善方法的精确度、缩短消化时间,对不同样品的分析等方面已有不少研究。至今,这些仍是化学家们十分感兴趣... 展开更多
关键词 植物 凯氏定氮法 植物干样品 测定
下载PDF
高温高压下干样品体系中氧逸度控制的新方法——以Cu-O体系为例
2
作者 李和平 谢鸿森 +3 位作者 郭捷 张月明 许祖鸣 徐济安 《科学通报》 EI CAS CSCD 北大核心 1998年第9期988-991,共4页
通过在样品及氧库 (一种固体氧缓冲剂 )间置入固体氧离子导体 (YSZ)以及于样品及氧库间外加一直流电压 ,负极区的氧在该电压作用下经由YSZ被迫进入正极区 .以此样品中氧逸度可独立于温度、压力得到就位控制 .以Cu O体系为样品的试验表... 通过在样品及氧库 (一种固体氧缓冲剂 )间置入固体氧离子导体 (YSZ)以及于样品及氧库间外加一直流电压 ,负极区的氧在该电压作用下经由YSZ被迫进入正极区 .以此样品中氧逸度可独立于温度、压力得到就位控制 .以Cu O体系为样品的试验表明 ,该方法非常成功 .无疑 ,该技术对有变价元素参与的高温高压实验具有重要的意义 . 展开更多
关键词 氧逸度控制 干样品体系 高温 高压 氧离子导体
原文传递
检测干血片样品中促甲状腺素和苯丙氨酸实验影响因素的研究 被引量:14
3
作者 李文杰 李明训 +1 位作者 林闽华 王梅 《上海医学检验杂志》 北大核心 2003年第1期49-51,共3页
目的 探讨新生儿筛查滤纸干血样法检测过程中 ,可能影响促甲状腺激素 (TSH)及苯丙氨酸 (Phe)测定结果的因素。方法 分别用酶免疫标记法和细菌抑制法检测滤纸血片TSH及Phe含量。结果 TSH测定 :干血片中TSH在 4°C环境能够稳定 30... 目的 探讨新生儿筛查滤纸干血样法检测过程中 ,可能影响促甲状腺激素 (TSH)及苯丙氨酸 (Phe)测定结果的因素。方法 分别用酶免疫标记法和细菌抑制法检测滤纸血片TSH及Phe含量。结果 TSH测定 :干血片中TSH在 4°C环境能够稳定 30d ,血斑中心到边缘 1/ 2以内区域检测结果最为可靠 ;新生儿出生 72h后采血结果稳定 ,季节间TSH水平有差异 ,血片递送周期应限制在 15d以内。Phe测定 :制板温度以 5 5°C~6 0°C为宜 ;试剂中加入抗生素可以有效降低假阴性率 ;72h后采血可降低假阳性率。结论 采血时间、标本保存时间、血片处理等因素影响筛查结果 ,选择最佳试验条件 。 展开更多
关键词 检测 血片样品 影响因素 研究 甲状腺激素 苯丙氨酸 新生儿筛查
下载PDF
稻田土壤干鲜样品速效钾的相关测定
4
作者 刘淑君 《河北农垦科技》 1996年第2期34-35,共2页
本文通过对稻田土壤中速效K含量进行干鲜样品对比测定试验分析,证明了水稻土壤的新鲜样品完全可代替风干样品进行速效K的测定分析试验。
关键词 水稻 稻田土壤 样品速效钾 相关测定
下载PDF
柳枝稷鲜样及干样的稀酸预处理及乙醇发酵研究 被引量:2
5
作者 于泳 田沈 +3 位作者 左壮 李丰田 段仰凯 杨秀山 《太阳能学报》 EI CAS CSCD 北大核心 2011年第4期468-471,共4页
为了比较柳枝稷的鲜样品与干样品生产乙醇的差异,首先对柳枝稷鲜样品和干样品进行稀酸水解研究,接着用本实验室酵母菌种Y7对两种原料的稀酸水解糖液进行未脱毒的乙醇发酵。研究结果表明:柳枝稷鲜样品稀酸水解的纤维素和半纤维素转化率... 为了比较柳枝稷的鲜样品与干样品生产乙醇的差异,首先对柳枝稷鲜样品和干样品进行稀酸水解研究,接着用本实验室酵母菌种Y7对两种原料的稀酸水解糖液进行未脱毒的乙醇发酵。研究结果表明:柳枝稷鲜样品稀酸水解的纤维素和半纤维素转化率、还原糖得率和水解液的乙醇产率都明显优于风干样品。该研究为柳枝稷的充分利用生产乙醇提供了新的有效途径。 展开更多
关键词 柳枝稷稷鲜干样品 稀酸预处理 未脱毒水解液乙醇发酵 酵母菌株Y7
下载PDF
微波消解-电感耦合等离子体发射光谱(ICP-OES)法测定植物样品中的磷、硫 被引量:12
6
作者 端爱玲 王思远 +3 位作者 董艳红 张树雄 杨树俊 韩张雄 《中国无机分析化学》 CAS 北大核心 2021年第6期126-130,共5页
采用微波消解处理样品,电感耦合等离子体发射光谱(ICP-OES)法测定植物样品中的磷、硫含量,选用优化微波消解条件进行样品前处理,磷和硫方法最低检出限分别为0.93和1.9 mg/kg,相对标准偏差(RSD)和相对误差(RE)均小于3%,对新鲜植物样品进... 采用微波消解处理样品,电感耦合等离子体发射光谱(ICP-OES)法测定植物样品中的磷、硫含量,选用优化微波消解条件进行样品前处理,磷和硫方法最低检出限分别为0.93和1.9 mg/kg,相对标准偏差(RSD)和相对误差(RE)均小于3%,对新鲜植物样品进行加标回收实验,加标回收率为90.5%~107%,表明方法既可用于检测干植物样品,又可检测新鲜植物样品。 展开更多
关键词 微波消解 谱线选择 干样品 新鲜样品
下载PDF
利用干血斑样品对1例HIV-1感染者进行辅助确认
7
作者 程绍辉 夏建晖 +2 位作者 宁铁林 柳忠泉 朱效科 《中国艾滋病性病》 CAS 2009年第6期642-642,646,共2页
关键词 艾滋病病毒I型 血斑样品 基因片段 测序分析
原文传递
A new method of combined rock drilling 被引量:5
8
作者 Tang Jiren Lu Yiyu +3 位作者 Ge Zhaolong Xia Binwei Sun Huijuan Du Peng 《International Journal of Mining Science and Technology》 SCIE EI 2014年第1期1-6,共6页
Based on the technologies of traditionally mechanical drilling and water jet,we propose a new method of abrasive water jet in combination with rock drilling,and establish a combined rock drilling system for the gas pr... Based on the technologies of traditionally mechanical drilling and water jet,we propose a new method of abrasive water jet in combination with rock drilling,and establish a combined rock drilling system for the gas pre-drainage.This study chose the common sandstone and silicon limestone as the rock sample.A series of experiments were completed in the case of dry drilling,existing technology drilling,combined drilling with high pressure water jet and combined drilling with abrasive water jet,respectively.The drilling efficiency and performance were contrasted and analyzed in detail.The results indicate that it is better to choose the method of combined drilling with the high-pressure water jet for soft rocks.The method of combined drilling with abrasive water jet is feasible for the hard rock drilling and has higher drilling efficiency and performance.In this paper,compared with the existing technology,the drilling depth has increased by about 65%,the axial force and torque have reduced by about 14%and 17%,respectively,and the drill wear reduces obviously in the same conditions. 展开更多
关键词 Gas extraction Drilling Abrasive water jet Mechanical bit
下载PDF
Experimental investigation on the energy evolution of dry and water-saturated red sandstones 被引量:26
9
作者 Zhang Zhizhen Gao Feng 《International Journal of Mining Science and Technology》 SCIE EI CSCD 2015年第3期383-388,共6页
In order to investigate the effect of water content on the energy evolution of red sandstone, the axial loading–unloading experiments on dry and water-saturated sandstone samples were conducted, and the distribution ... In order to investigate the effect of water content on the energy evolution of red sandstone, the axial loading–unloading experiments on dry and water-saturated sandstone samples were conducted, and the distribution and evolution of elastic energy and dissipated energy within the rock were measured.The results show that the saturation process from dry to fully-saturated states reduces the strength, rigidity and brittleness of the rock by 30.2%, 25.5% and 16.7%, respectively. The water-saturated sample has larger irreversible deformation in the pre-peak stage and smaller stress drop in the post-peak stage.The saturation process decreases the accumulation energy limit by 38.9%, but increases the dissipated energy and residual elastic energy density, thus greatly reducing the magnitude and rate of energy release. The water-saturated sample has lower conversion efficiency to elastic energy by 3% in the prepeak region; moreover, the elastic energy ratio falls with a smaller range in the post-peak stage.Therefore, saturation process can greatly reduce the risk of dynamic disaster, and heterogeneous water content can lead to dynamic disaster possibly on the other hand. 展开更多
关键词 Rock mechanics Energy evolution Energy distribution Triaxial compression Saturation process
下载PDF
Effect of Radiant Energy Vacuum on Physical and Microbial Properties of Beef Jerky
10
作者 John Scott Church Carley Marie Maclntyre +4 位作者 Wade Robert Archambault Paul Edward Moote Jason Laco Cochran Timothy Douglas Durance Jonathan Douglas Van Hamme 《Journal of Food Science and Engineering》 2013年第1期33-39,共7页
To test the feasibility of radiant energy vacuum (REV) dehydration, a technology that couples microwave cooking with vacuum pressure, on beef jerky preparation, the physical and microbial properties of the final jer... To test the feasibility of radiant energy vacuum (REV) dehydration, a technology that couples microwave cooking with vacuum pressure, on beef jerky preparation, the physical and microbial properties of the final jerky product was compared to conventional preparation methods. Physical characteristics assessed using puncture and shear tests of samples prepared using REV dehydration compared to the traditional method were not statistically different (P 〈 0.05). Moisture content and water activity levels were also very similar between the two products, To test microbiological quality, samples were homogenized in a stomacher and a variety of 3 M Petrifilms were used to evaluate the microbial load. Raw beef harboured low numbers of microbes, but the post-marination pasteurization/smoking step used in both treatments eliminated all culturable microorganisms tested for. To further investigate the ability of REV dehydration to kill microbes, samples were spiked with Listeria innocua after the pasteurization/smoking step but prior to REV dehydration. Samples were taken at different time intervals for microbial enumeration, and a decimal reduction time of 1 min was calculated, with 99.99% of 1.98 × 10^7 CFU g^-1 Listeria being killed in five min. Improved drying times were observed for jerky samples prepared using the REV method offering potential energy savings during jerky preparation. 展开更多
关键词 MICROWAVE food safety DEHYDRATION PRESERVATION Listeria innocua beef jerky.
下载PDF
Effect of Wetting-Drying Cycles on Redistribution of Lead in Some Semi-Arid Zone Soils Spiked with a Lead Salt 被引量:2
11
作者 H.KHODAVERDILOO M.RAHMANIAN +3 位作者 S.REZAPOUR S.GHORBANI DASHTAKI H.HADI F.X.HAN 《Pedosphere》 SCIE CAS CSCD 2012年第3期304-313,共10页
Mobility and bioavailability of lead (Pb) could be affected considerably by soil physicochemical properties; however, less is known about the effect of Pb levels and aging time. This study was conducted to evaluate ... Mobility and bioavailability of lead (Pb) could be affected considerably by soil physicochemical properties; however, less is known about the effect of Pb levels and aging time. This study was conducted to evaluate the effects of Pb levels and wetting-drying (WD) cycles on distribution and bioavailability of Pb in three semi-arid zone soils treated with different levels of Pb(NO3)2. Wetting-drying cycles simulated the actual field irrigation in the semi-arid soils. A soil with a long history of Pb contamination was also taken as a reference soil. The soils were spiked with various levels of Pb and incubated under WD cycles for 160 d. Sequential extractions and batch sorption experiments were performed to assess the fractionation of Pb in the spiked soils. Redistribution index (Uts) and reduced partitioning parameter (IR) were applied to semi-quantify the distribution of Pb in the spiked soils. A small amount of Pb sorbed was desorbed by the soils, indicating a strong and irreversible binding of Pb in the studied soils. Contribution of carbonate-bound (Car) and residual (Res) Pb fl'actions to the total Pb of the soils was more than 97%. The Car, soluble plus exchangeable (SE), and organic matter-bound (OMB) fractions of Pb were transferred to the Res fraction under the WD cycles. The IR and Uts values were influenced by Pb loading levels and WD; therefore, the Pb lability and/or redistribution pattern could semi-quantitatively be assessed via these parameters. At the end of the experiment, the Ia and Uts values for the Pb salt-spiked soils did not show the quasi- equilibrium state. The lability of Pb in the soils decreased with increasing incubation time and showed a strong dependence on Pb levels and soil chemical composition. WD cycles significantly affected the overall lability of Pb in soils through influencing the redistribution of Pb among solid-phase components. 展开更多
关键词 BIOAVAILABILITY heavy metals mobility redistribution index reduced partitioning parameter
原文传递
Evaluating Loss-on-Ignition Method for Determinations of Soil Organic and Inorganic Carbon in Arid Soils of Northwestern China 被引量:7
12
作者 WANG Jia-Ping WANG Xiu-Jun ZHANG Juan 《Pedosphere》 SCIE CAS CSCD 2013年第5期593-599,共7页
There is a need for determinations of soil organic carbon (SOC) and inorganic carbon (SIC) due to increasing interest in soil carbon sequestration. Two sets of soil samples were collected separately from the Yanqi Bas... There is a need for determinations of soil organic carbon (SOC) and inorganic carbon (SIC) due to increasing interest in soil carbon sequestration. Two sets of soil samples were collected separately from the Yanqi Basin of northwest China to evaluate loss-on-ignition (LOI) method for estimating SOC and SIC in arid soils through determining SOC using an element analyzer, a modified Walkley-Black method and a LOI method with combustion at 375℃ for 17 h and determining SIC using a pressure calcimeter method and a LOI procedure estimated by a weight loss between 375 to 800℃. Our results indicated that the Walkley-Black method provided 99%recovery of SOC for the arid soils tested. There were strong linear relationships(r > 0.93, P < 0.001) for both SOC and SIC between the traditional method and the LOI technique. One set of soil samples was used to develop relationships between LOI and SOC(by the Walkley-Black method), and between LOI and SIC(by the pressure calcimeter method), and the other set of soil samples was used to evaluate the derived equations by comparing predicted SOC and SIC with measured values. The mean absolute errors were small for both SOC (1.7 g C kg-1) and SIC(1.22 g C kg-1), demonstrating that the LOI method was reliable and could provide accurate estimates of SOC and SIC for arid soils. 展开更多
关键词 calcareous soil dry combustion linear regression pressure calcimeter method Walkley-Black method
原文传递
上一页 1 下一页 到第
使用帮助 返回顶部