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采用扫描电镜-能谱仪比较水飞法、水洗法及干研法对雄黄饮片质量的影响 被引量:3
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作者 张慧 高岩 +5 位作者 熊慧 薛雪 刘梦楠 刘欢 张颖 李向日 《中国实验方剂学杂志》 CAS CSCD 北大核心 2018年第11期22-26,共5页
目的:比较雄黄水飞品、水洗品及干研品中二硫化二砷及各元素的含量,以阐明水飞法、水洗法及干研法对雄黄饮片质量的影响,并对雄黄水飞品、水洗品及干研品进行快速鉴别。方法:依据2015年版《中国药典》(一部)雄黄项下规定对3种炮制... 目的:比较雄黄水飞品、水洗品及干研品中二硫化二砷及各元素的含量,以阐明水飞法、水洗法及干研法对雄黄饮片质量的影响,并对雄黄水飞品、水洗品及干研品进行快速鉴别。方法:依据2015年版《中国药典》(一部)雄黄项下规定对3种炮制品进行含量测定;采用扫描电镜-能谱仪对雄黄3种炮制品进行形貌观察,对3种炮制品中的元素种类及含量进行分析。结果:3种炮制品的二硫化二砷含量排序为水飞品〉水洗品〉干研品;水飞品及水洗品的形貌相似,而干研品的形貌与其他2种炮制品不同;3种炮制品的氧元素含量排序呈现干研品〉水洗品〉水飞品的趋势。结论:采用扫描电镜-能谱仪可以对雄黄水飞品和干研品进行快速鉴别,为鉴别雄黄不同炮制品提供了一定的技术支持。水飞法的除杂减毒效果最好,水飞品质量优于水洗品和干研品,说明水飞法炮制雄黄具有一定的科学依据。 展开更多
关键词 雄黄 水飞法 水洗 干研品 扫描电镜-能谱仪
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Effects of Ultra-drying Treatment on Large Amounts of Four Kinds of Crop Seeds 被引量:10
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作者 孟淑春 张海英 +1 位作者 刘庞源 何伟明 《Agricultural Science & Technology》 CAS 2009年第2期82-85,89,共5页
This study was to understand the physiological changes of four kinds of crop seeds including baby corn, cowpea, radish and rape- seed, under the treatment of ultra-drying. Large amounts of seeds as experimental materi... This study was to understand the physiological changes of four kinds of crop seeds including baby corn, cowpea, radish and rape- seed, under the treatment of ultra-drying. Large amounts of seeds as experimental materials ( 10 kg for each material) were respectively dried to the suitable water content consistent with the ultra-dried seed criterion via heating at 50 ~C; then the physiological indices of these ultra-dried seeds such as water content, seed germination, dehydrogenase activity and SOD activity were measured. The results showed that except cowpea seeds, whose ultra-drying treatment should be controlled between two and four days, other three kinds of seeds were tolerant to high tem- perature and low water content. The ultra-dried seeds assumed similar or even higher activities than CKs, but showed no damage symptom. Our result proves that ultra-drying treatment via heating at 50 ℃ is safe and efficient to experimental seeds. 展开更多
关键词 Large amounts of seeds Ultra-drying treatment via heating Water content Seed vigor
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Effect of Bentonite on the Sandy Soils of Arid Regions: Study of Behavior of an Association of Wheat and Chickpea
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作者 H.Y. Reguieg M. Belkhodja A. Chibani 《Journal of Environmental Science and Engineering》 2011年第12期1668-1677,共10页
The sandy soils of Mostaganem plateau are vety, poor in clay. They are characterized by very low fertility and water holding capacity. The addition of bentonite to these soils and the cultivation of durum wheat, in co... The sandy soils of Mostaganem plateau are vety, poor in clay. They are characterized by very low fertility and water holding capacity. The addition of bentonite to these soils and the cultivation of durum wheat, in combination with the chickpeas, are two eco-physiological strategies to rehabilitate their agricultural suitability. This study was conducted on two plant species: a local variety of durum wheat (Waha) and a legume, chickpea (variety ILC 3279), on a substrate bentonite at 10% dose. For each stage of growth measurements of stem height, leaf area and plants vegetative nitrogen content were quantified. Changes in total nitrogen content of durum wheat grown in substrates amended with 10% bentonite or not during the development of durum wheat in monoculture and in association with the chickpeas were analyzed. The results showed that the total nitrogen content of durum wheat was significantly higher at three leaves and tailoring stages, when durum wheat was associated with chickpea in the same soil. However, the results showed no difference during the lifting and two leaves stages. There was also a positive effect of treatment at 10% of bentonite on the plant total nitrogen content regardless of the stage and the culture system. 展开更多
关键词 Sandy soil BENTONITE arid zones durum wheat CHICKPEA physicochemical characterization of soil.
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