Failure mechanisms and destruction characteristics of cemented coal gangue backfill under compression effect of non-uniform load

Backfill mining is one of the most important technical means for controlling strata movement and reducing surface subsidence and environmental damage during exploitation of underground coal resources. Ensuring the stability of the backfill bodies is the primary prerequisite for maintaining the safety of the backfilling working face, and the loading characteristics of backfill are closely related to the deformation and subsidence of the roof. Elastic thin plate model was used to explore the non-uniform subsidence law of the roof, and then the non-uniform distribution characteristics of backfill bodies’ load were revealed. Through a self-developed non-uniform loading device combined with acoustic emission (AE) and digital image correlation (DIC) monitoring technology, the synergistic dynamic evolution law of the bearing capacity, apparent crack, and internal fracture of cemented coal gangue backfills (CCGBs) under loads with different degrees of non-uniformity was deeply explored. The results showed that: 1) The uniaxial compressive strength (UCS) of CCGB increased and then decreased with an increase in the degree of non-uniformity of load (DNL). About 40% of DNL was the inflection point of DNL-UCS curve and when DNL exceeded 40%, the strength decreased in a cliff-like manner;2) A positive correlation was observed between the AE ringing count and UCS during the loading process of the specimen, which was manifested by a higher AE ringing count of the high-strength specimen. 3) Shear cracks gradually increased and failure mode of specimens gradually changed from “X” type dominated by tension cracks to inverted “Y” type dominated by shear cracks with an increase in DNL, and the crack opening displacement at the peak stress decreased and then increased. The crack opening displacement at 40% of the DNL was the smallest. This was consistent with the judgment of crack size based on the AE b-value, i. e., it showed the typical characteristics of “small b-value-large crack and large b-value-small crack”. The research results are of significance for preventing the instability and failure of backfill.

核桃果柄分离力与其影响因素的相关系数研究

【目的】寻找适宜核桃振动采收装置的技术参数,对新新2、扎343、实生核桃三个品种的果柄分离力和影响因素进行测试与研究。【方法】以核桃的青皮硬度、果皮开裂度作为影响果柄分离力的主要因素进行测试,分析各因素与果柄分离力的皮尔森相关系数。【结果】由相关性检验可知,在0.01水平下3个品种果实青皮硬度与果柄分离力正相关,青皮开裂度与果柄分离力负相关。【结论】曲线拟合结果中,开裂度对果柄分离力的影响,扎343欠佳;青皮硬度对果柄分离力的影响,实生核桃欠佳,其他拟合度均较高。

热应力作用下缺陷花岗岩的渗流规律

为探讨热应力对缺陷花岗岩节理面渗透规律的影响,以岩石变形为切入点,以花岗岩裂隙的开裂度为桥梁,研究热应力作用下花岗岩裂隙渗透系数与开裂度的关系。重点分析了温度对等效水力张开度的作用,得到了裂隙渗透系数公式。数值模拟结果表明,温度越高,热应力对花岗岩节理面渗透率影响越大。模拟结果与理论计算结果较接近,证明了渗透系数公式的合理性。该研究可为高温岩体地热开发提供一定的参考。

Mapping of QTLs for Dehiscence Length at Basal Part of Thecae in Rice Based on TD70/Kasalath RIL Population

A population of 240 recombinant inbred lines （RIL） was derived from a cross between Japonica rice cultivar TD70 and Indica cultivar Kasalath, and their linkage map including 141 SSR markers was used to locate the QTLs controlling the length of dehiscence at the basal part of thecae （LDBT）. Then, the correlations between LDBT and other agronomic traits of rice were analyzed. Two QTLs con- trolling LDBT were mapped on chromosome 6 and 8, respectively, qLDBT6 was mapped between RM3 and RM3628 markers on chromosome 6 with a LOD value of 3.23, contribution rate of 6.18% and additive effect of 17.74%. qLDBT8 was mapped between RM1376-RM4085 markers on chromosome 8 with a LOD value 2.95, contribution rate of 8.00% and additive effect of 20.09%. This domain probably had a relationship with the sterility of rice. The LDBT of RILs had extremely signifi- cant positive correlations with flag leaf width, 1 000-grain weight, grain width, grain length and grain thickness, but no significant correlations with other agronomic traits, such as plant height, heading date, tiller number, flag leaf length, average and the maximum temperature during heading period or rice.

Effect of a novel three-step aging on strength, stress corrosion cracking and microstructure of AA7085

The influence of a novel three-step aging on strength, stress corrosion cracking(SCC) and microstructure of AA7085 was investigated by tensile testing and slow strain rate testing combined with transmission electron microscopy(TEM). The results indicate that with the increase of second-step aging time of two-step aging, the mechanical properties increase first and then decrease, while the SCC resistance increases. Compared with two-step aging, three-step aging treatment improves SCC resistance and the strength increases by about 5%. The effects of novel three-step aging on strength and SCC resistance are explained by the role of matrix precipitates and grain boundary precipitates, respectively.

Residual stress distribution in different depths of TiNi/Ti_2Ni-based laser clad coating prepared at different environmental temperatures

This study aimed to effectively reduce the cracking susceptibility of the laser clad coating by enhancing the environmental temperature during laser cladding,and reveal the residual stress distribution in different depths of the coating.The TiNi/Ti2Ni-based coatings were prepared on Ti6Al4V by laser cladding at different environmental temperatures of25,400,600and800°C.The changes in residual stress along the depth of the coatings were investigated in detail by the nanoindentation method.Results showed that the average residual stress of2.90GPa in the coating prepared at25°C was largest.With the increase in environmental temperature,the average residual stress was reduced to1.34GPa(400°C),0.70GPa(600°C)and0GPa(800°C).For all the coatings,the residual stress was increased with increasing the distance from the coating surface.Enhancing the environmental temperature can effectively reduce the cracking susceptibility of the coatings.

Influence of temperature on acoustic emission source location accuracy in underground structure

An acoustic emission(AE)experiment was carried out to explore the AE location accuracy influenced by temperature.A hollow hemispherical specimen was used to simulate common underground structures.In the process of heating with the flame,the pulse signal of constant frequency was stimulated as an AE source.Then AE signals received by each sensor were collected and used for comparing localization accuracy at different temperatures.Results show that location errors of AE keep the same phenomenon in the early and middle heating stages.In the later stage of heating,location errors of AE increase sharply due to the appearance of cracks.This provides some beneficial suggestions on decreasing location errors of structural cracks caused by temperature and improves the ability of underground structure disaster prevention and control.

Measurement of Walnut Properties and Analysis on the Compressive Stiffness of the Critical Value of Shell-cracking

Based on the measurement of walnut properties, a computational analysis was conducted on the compressive stiffness of the critical val-ue of shell-cracking. As indicated by the results, to crack the walnuts shell from its longitudinal or edge directions could save lots of efforts. The study provided theoretical basis for the design and improvement of walnut shell-cracking machine as well as theoretical references for the design, mak ng and use of some spec a crack ng-a d ng too s such as nutcracker.

Effect of anions on stress corrosion cracking behaviors of ultra-high strength steel 23Co14Ni12Cr3Mo

The effects of chloride,sulfate and carbonate anions on stress corrosion behaviors of ultra-high strength steel 23Co14Ni12Cr3Mo were studied by stress corrosion cracking(SCC)test method using double cantilever beam(DCB)specimens.The SCC morphology was observed by using scanning electron microscopy(SEM)and the composition of corrosion products was analyzed by using energy dispersive spectrometer(EDS).The results show that the crack propagates to bifurcation in NaCl and Na2SO4 solution,while the crack in Na2CO3 solution propagates along the load direction.The SCC rate in NaCl solution is the highest,while lower in Na2SO4 solution and little in Na2CO3 solution.From the SEM morphologies,quasi-cleavage fracture was observed in NaCl and Na2SO4 solutions,but intergranular features in Na2CO3 solution.The mechanism of anion effect on SCC of steel 23Co14Ni12Cr3Mo was studied by using full immersion test and electrochemical measurements.

Research on replacement depth of black cotton soil based on cracking behavior of embankment

In order to analyze the influence of replacement depth of black cotton soil(BCS)foundation on the initial cracking depth of a highway embankment,the laboratory tests were performed to construct the constitutive relationship between state variables and stress variables of BCS,and the coupled consolidation theory for unsaturated soils was employed to simulate the change in the major principal stress of the subgrade soils caused by water loss shrinkage of BCS with the help of Abaqus 6.11 codes.The simulation results indicate that the water losing shrinkage of BCS causes tensile stress within the subgrade,which leads to embankment cracking.The crack depth decreases with the increase in the BCS replacement depth and the embankment height,and increases with the increase in the burial depth of BCS.In the distribution area of deep BCS,the key values of foundation replacement depth for controlling the crack depth of the embankment with the height of 1 to 4 m are 1.2 and 1.5 m.In the low filling section,when the buried depth of BCS is 2,3 and 4 m,the key values of the foundation replacement depth to control the crack depth of the embankment are 0.8 and 1.2 m.In order to control the embankment cracking induced by the water losing shrinkage of BCS,a reasonable replacement depth of the foundation should be selected while slope protection is carried out well.

Mechanical properties and cracking behaviors of limestone-like samples with two parallel fissures before and after grouting

In the present work,uniaxial compressive tests were carried out on limestone-like samples containing two parallel open fissures or cement-infilled fissures with different geometries.Mechanical property and crack behavior of limestone-like samples with two parallel open fissures or cement-infilled fissures were affected by bridge inclination angle and fissure inclination angle.Four types of coalescence of rock bridge for samples containing open fissures or cement-infilled fissures were summarized and classified.The closure of tensile crack was observed in the samples with small fissure inclination angle.This is a new phenomenon which is not mentioned in previous studies.Test results show that the peak strength,crack initiation stress,and coalescence type are different between open fissures and cement infilled fissures.The reason for this phenomenon is that grouting of cement can transfer stress and reduce stress concentration at the flaw tip and rock bridge area.

Unloading responses of pre-flawed rock specimens under different unloading rates

Based on the stress redistribution analysis of rock mass during the deep underground excavation, the unloading process of pre-flawed rock material was simulated by distinct element method (DEM). The effects of unloading rate and flaw inclination angle on unloading strengths and cracking properties of pre-flawed rock specimens are numerically revealed. The results indicate that the unloading failure strength of pre-flawed specimen exhibits a power-function increase trend with the increase of unloading period. Moreover, combined with the stress state analysis on the flaws, it is found that the unloading failure strength increases with the increase of flaw inclination angle. The cracking distribution of pre-flawed specimens under the unloading condition closely depends on the flaw inclination angle, and three typical types of flaw coalescence are observed. Furthermore, at a faster unloading rate, the pre-flawed specimen experiences a sharper and quicker unloading failure process, resulting in more splitting cracks in the specimens.

Fractured zone height of longwall mining and its effects on the overburden aquifers

As mining depth becomes deeper and deeper,the possibility of undermining overburden aquifers is increasing.It is very important for coal miners to undertake studies on the height of fractured zone during longwall mining and the effects of longwall mining on the underground water while mining under surface water bodies and underground aquifers.In order to study this problem,piezometers for monitoring underground water levels were installed above the longwall panels in an American coalmine.Large amounts of pre-mining,during mining and post-mining monitoring data were collected.Based on the data,the heights of fractured zones were obtained and the effects of longwall mining on the underground water were studied.The results demonstrate that when the piezometer monitoring wells had an interburden thickness of less than 72.7 m,the groundwater level decreased immediately to immeasurable levels and the wells went dry after undermining the face of longwall.The height of the fractured zone is 72.7-85.3 m in the geological and mining conditions.The results also show that the calculated values of fractured zones by the empirical formulae used in China are smaller than the actual results.Therefore,it is not always safe to use them for analyses while mining under water bodies.

Theoretical and experimental study of initial cracking mechanism of an expansive soil due to moisture-change

Swelling and shrinkage due to moisture-change is one of the characteristics of the expansive soil,which is similar to the behavior of most materials under thermal effect,If the deformation is restricted,stress in expansive soil is caused by the swell-shrinking.The stress is defined as "moisture-change stress" and is adopted to analyze swell-shrinkage deformation based on the elasticity mechanics theory.The state when the total stress becomes equal to the soil tensile strength is considered as the cracking criterion as moisture-change increases.Then,the initial cracking mechanism due to evaporation is revealed as follows:Different rates of moisture loss at different depths result in greater shrinkage deformation on the surface while there is smaller shrinkage deformation at the underlayer in expansive soil;cracks will grow when the nonuniform shrinkage deformation increases to a certain degree.A theoretical model is established,which may be used to calculate the stress caused by moisture-change.The depth of initial cracks growing is predicted by the proposed model in expansive soil,A series of laboratory tests are carried out by exposing expansive soil samples with different moisture-changes.The process of crack propagation is investigated by resistivity method.The test results show good consistency with the predicted results by the proposed theoretical model.

Production of Bio-gasoline by Co-cracking of Acetic Acid in Bio-oil and Ethanol

Abstract Acetic acid was selected as the model compound representing the carboxylic acids present in bio-oil. This work focuses the co-cracking of acetic acid with ethanol for bio-gasoline production. The influences of reaction temperature and pressure on the conversion of reactants as well as the selectivity and Conaposition of the crudegasoline phase were investigated. It was found that increasing reaction temperature benefited the conversion of reactants and pressurized cracking produced a higher crude gasoline yield. At 400 ℃ and 1 MPa, the conversion of the reactants reached over 99% and the selectivity of the gasoline phase reached 42.79% （by mass）. The gasoline phase shows outstanding quality, with a hydrocarbon content of 100%.

Role of matrix structure and flaw size distribution modification on deflection hardening behavior of polyvinyl alcohol fiber reinforced engineered cementitious composites(PVA-ECC)

The multiple cracking and deflection hardening performance of polyvinyl alcohol fiber reinforced engineered cementitious composites(PVA-ECC)under four-point flexural loading have been investigated.Matrices with different binder combinations and W/B ratios(from 0.44 to 0.78)providing satisfactory PVA fiber dispersion were specially designed.Effect of pre-existing flaw size distribution modification on deflection hardening behavior was comparatively studied by adding 3 mm diameter polyethylene beads into the mixtures(6%by total volume).Natural flaw size distributions of composites without beads were determined by cross sectional analysis.The crack number and crack width distributions of specimens after flexural loading were characterized and the possible causes of changes in multiple cracking and deflection hardening behavior by flaw size distribution modification were discussed.Promising results from the view point of deflection hardening behavior were obtained from metakaolin incorporated and flaw size distribution modified PVA-ECCs prepared with W/B=0.53.The dual roles of W/B ratio and superplasticizer content on flaw size distribution,cracking potential and fiber-matrix bond behavior were evaluated.Flaw size distribution modification is found beneficial in terms of ductility improvement at an optimized W/B ratio.

Evaluation of parameters affecting reflection cracking in geogrid-reinforced overlay

The influence of the most important parameters on the service life of reinforced asphalt overlay with geogrid materials in bending mode was examined by employing the Taguchi method and analysis of variance techniques. The objectives of this experiment was to investigate the effects of grid stiffness, tensile strength, coating type, amount of tack coat, overlay thickness, crack width and stiffnesses of asphalt overlay and existing asphalt concrete on propagation of the reflection cracking. Results indicate that the stiffnesses of cracked layer and overlay are the main significant factors that can directly improve the service life of an overlay against the reflection cracking. Generally, glass grid is more effective in reinforced overlay than polyester grid. Effect of crack width of the existing layer is significant when its magnitude increases from 6 to 9 mm.

Critical crack tip opening displacement of different strength concrete

Critical crack tip opening displacement (CTODc) of concrete using experimental and analytical evaluation with seven different compressive strengths ranging from 30 up to 150 MPa was studied based on two types of fracture tests:three-point bending (TPB) and wedge splitting (WS).In the tests,the values of CTODc were experimentally recorded using a novel technique,in which fiber Bragg grating (FBG) sensors were used,and two traditional techniques,in which strain gauges and clip gauges were deployed.The values of CTODc of tested concrete were also predicted using two existing analytical formulae proposed by JENQ & SHAH and XU,respectively.It is found that the values of CTODc obtained by both experimental measurements and analytical formulae exhibit a negligible variation as the compressive strength of concrete increases,and the test geometry adopted has little impact on the value of CTODc.Regarding the experimental measurement of CTODc,the clip gauge method generally leads to a larger value of CTODc and shows a more significant scatter as compared with the other two methods,while the strain gauge method leads to a slightly lower CTODc as compared with the FBG sensor method.The analytical formula proposed by JENQ and SHAH is found to generally lead to an overestimation,while the analytical formula proposed by XU shows a good accuracy.

SCC evaluation of ultra-high strength steel in acidic chloride solution

The stress corrosion crack （SCC） susceptibility of ultra-high strength steel AerMet 100 was investigated by slow strain rate technique （SSRT）, tensile with polarization and surface analysis technique. The curves of tf^Cl/tf^W -strain rate are divided into three regions： stress-dominated region, SCC-dominated region, and corrosion-dominated region, so as the curves of εf^Cl/εf^W - strain rate and tm/tf-strain rate. The results of tensile tests with polarization show that the main SCC mechanism of AerMet 100 is anodic dissolution, which controls the corrosion process. The three regions have been discussed according to the relationship between the rate of slip-step formation and the rate of dissolution. Fracture appearances in different environments were analyzed by scanning electron microscopy （SEM）. SCC fracture appears as a mixture of intergranular and dimples, while it is totally dimples in the inert environment. The εf becomes the parameter to predict tf because the relationship between εf^Cl/εf^W and tf^Cl/tf^w is a straight line for AerMet 100.

Improvement of hydrogen embrittlement and stress corrosion cracking by annealing for Al-4.4Mg-0.6Mn alloy

With no annealing treatment, cathodic polarization trends in 5083F A1 alloy revealed concentration polarization and activation polarization. However, the annealed specimens have lower current densities at corrosion protection potential compared to the non-annealed specimen. The results of SSRTs conducted in seawater at the applied potential range of-l.8 V to -0.5 V indicated that the maximum tensile strength, elongation, and time-to-fracture had high values at applied potentials of -0.7 to -1.4 V. The maximum tensile strength, elongation, and time-to-f？acture decreased when the potential values were beyond this range in either anodic or cathodic direction. In general, the increased shear lip caused by annealing treatment indicates elongation. Time-to-fracture would likely increase with elongation. Potentials between -0.5 V to -0.6 V were found to be in the region of stress corrosion cracking. The corrosion protection zone was determined to be -0.7 V to -J,4 V because these potential ranges produced good mechanical properties. Potential less than -1.4 V produced a fractured surface with a mixture of dimples （ductile fractures） and a quasi-cleavage pattern resulting from the effects of hydrogen gas.