Rapidly solidified Fe100-xGax （x=16-20） alloy rods were prepared by induction melting and copper mold casting under the protection of inert gases. The optical microscopy observation shows that the large and elongate...Rapidly solidified Fe100-xGax （x=16-20） alloy rods were prepared by induction melting and copper mold casting under the protection of inert gases. The optical microscopy observation shows that the large and elongated columnar grains grow along the radial direction, which is parallel to the temperature gradient direction. The preferred orientation texture along the axial direction of the rod was detected by XRD. With the increase of Ga content, the saturation magnetization （Ms） of the alloys decreases distinctly and the dynamic response in low magnetic field increases drastically, the maximum longitudinal saturation magnetostriction for as-cast Fe82Ga18 alloy rods is 92×10-6 under an applied magnetic field strength of 30 kA/m. The large magnetostriction of Fe100-xGax alloys is attributed to the rapidly solidified disordered A2 phase and the high concentration of short range order of Ga atom clusters, which are arranged in the direction and finally trigger the formation of modified-DO3 structure, just as shown by the split of the （200） diffraction peak. Ordered DO3 phase is not conducive to the magnetostriction.展开更多
Multiple characterization and analysis techniques including electron backscatter diffraction（EBSD）, electron channeling contrast（ECC） imaging, transmission electron microscopy（TEM） and microhardness test were jo...Multiple characterization and analysis techniques including electron backscatter diffraction（EBSD）, electron channeling contrast（ECC） imaging, transmission electron microscopy（TEM） and microhardness test were jointly employed to investigate microstructural characteristics such as local composition, morphology, grain boundary characteristics and interphase orientation relationship of a forged Zr-2.5Nb alloy before and after β-air-cooling. Results show that the as-forged specimen is composed of equiaxed and lamellar α grains and continuous net-like β-Zr films. After the β-air-cooling, the microstructure of the specimen is featured by basket-weave Widmanst？tten structure, in which the inter-α-plate second phases are nanoscale β-Zr. Analyses for crystallographic orientations reveal that the Burgers relationship has been strictly followed during the β→α cooling. Compared to the as-forged specimen, the hardness of the β-air-cooled specimen is higher, which could be attributed to the decreased structural sizes of both α and β phases, and the increased fraction of high angle boundaries as well.展开更多
The effect of Cu content on the microstructure,grain orientation and mechanical properties of Sn-xCu(x=0-4.0 wt.%)lead-free solder was studied.Results showed that added Cu induced the formation of intermetallic phases...The effect of Cu content on the microstructure,grain orientation and mechanical properties of Sn-xCu(x=0-4.0 wt.%)lead-free solder was studied.Results showed that added Cu induced the formation of intermetallic phases.Only theη-Cu;Sn;andε-Cu;Sn phases were present in theβ-Sn matrix.For all contents,the strongly preferred orientation of theβ-Sn phase was formed on the{001}plane.In Sn doped with 1.0 wt.%Cu,theη-Cu;Sn;phase exhibited the preferred orientation of{0001}plane,whereas doping with 3.0 or 4.0 wt.%Cu transformed the preferred orientation to the{010}plane.In addition,only the{0001}and{■}planes were present in theε-Cu;Sn phase.The high Cu contents contributed to an increased number of low-angle boundaries,high residual strain,tensile strength and microhardness.展开更多
In order to predict the mechanism of the formation and propagation of rolling contact fatigue cracks in Hadfield steel railway crossings(HSRC),the residual strain,microstructure,crystal orientation,and microhardness s...In order to predict the mechanism of the formation and propagation of rolling contact fatigue cracks in Hadfield steel railway crossings(HSRC),the residual strain,microstructure,crystal orientation,and microhardness surrounding fatigue cracks were investigated.Results show that the formation and propagation of fatigue cracks in HSRC have no correlation with the crystal orientation and boundaries of grains.The hardness and residual strain in the field around the fatigue crack are lower than those in other regions.The compressive strain around the fatigue crack is released after crack propagates,which reduces the hardness around the fatigue crack.Deformation twins and dislocations play a key role in the work hardening of HSRC.展开更多
基金Project (11004091) supported by the National Natural Science Foundation of ChinaProject (Y4090219) supported by the Natural Science Foundation of Zhejiang Province, China+1 种基金Project (0916RJZA025) supported by the Natural Science Foundation of Gansu Province, ChinaProject (Q201104) supported by the "Hongliu Outstanding Youth" Foundation of Lanzhou University of Technology, China
文摘Rapidly solidified Fe100-xGax （x=16-20） alloy rods were prepared by induction melting and copper mold casting under the protection of inert gases. The optical microscopy observation shows that the large and elongated columnar grains grow along the radial direction, which is parallel to the temperature gradient direction. The preferred orientation texture along the axial direction of the rod was detected by XRD. With the increase of Ga content, the saturation magnetization （Ms） of the alloys decreases distinctly and the dynamic response in low magnetic field increases drastically, the maximum longitudinal saturation magnetostriction for as-cast Fe82Ga18 alloy rods is 92×10-6 under an applied magnetic field strength of 30 kA/m. The large magnetostriction of Fe100-xGax alloys is attributed to the rapidly solidified disordered A2 phase and the high concentration of short range order of Ga atom clusters, which are arranged in the direction and finally trigger the formation of modified-DO3 structure, just as shown by the split of the （200） diffraction peak. Ordered DO3 phase is not conducive to the magnetostriction.
基金Project(51401040) supported by the National Natural Science Foundation of ChinaProject(CSTC2017JCYJAX0114) supported by the Fundamental and Cutting-edge Research Plan of Chongqing,China+1 种基金Project(E2015203250) supported by the Natural Science Foundation of Hebei Province,ChinaProject(14LGA005) supported by the Young Teachers Program of Yanshan University,China
文摘Multiple characterization and analysis techniques including electron backscatter diffraction（EBSD）, electron channeling contrast（ECC） imaging, transmission electron microscopy（TEM） and microhardness test were jointly employed to investigate microstructural characteristics such as local composition, morphology, grain boundary characteristics and interphase orientation relationship of a forged Zr-2.5Nb alloy before and after β-air-cooling. Results show that the as-forged specimen is composed of equiaxed and lamellar α grains and continuous net-like β-Zr films. After the β-air-cooling, the microstructure of the specimen is featured by basket-weave Widmanst？tten structure, in which the inter-α-plate second phases are nanoscale β-Zr. Analyses for crystallographic orientations reveal that the Burgers relationship has been strictly followed during the β→α cooling. Compared to the as-forged specimen, the hardness of the β-air-cooled specimen is higher, which could be attributed to the decreased structural sizes of both α and β phases, and the increased fraction of high angle boundaries as well.
基金Rajamangala University of Technology Rattanakosin and School of Engineering,King Mongkut’s Institute of Technology Ladkrabang for the laboratory support of this research。
文摘The effect of Cu content on the microstructure,grain orientation and mechanical properties of Sn-xCu(x=0-4.0 wt.%)lead-free solder was studied.Results showed that added Cu induced the formation of intermetallic phases.Only theη-Cu;Sn;andε-Cu;Sn phases were present in theβ-Sn matrix.For all contents,the strongly preferred orientation of theβ-Sn phase was formed on the{001}plane.In Sn doped with 1.0 wt.%Cu,theη-Cu;Sn;phase exhibited the preferred orientation of{0001}plane,whereas doping with 3.0 or 4.0 wt.%Cu transformed the preferred orientation to the{010}plane.In addition,only the{0001}and{■}planes were present in theε-Cu;Sn phase.The high Cu contents contributed to an increased number of low-angle boundaries,high residual strain,tensile strength and microhardness.
基金supported by the National Science Foundation for Distinguished Young Scholars(Grant No.50925522)
文摘In order to predict the mechanism of the formation and propagation of rolling contact fatigue cracks in Hadfield steel railway crossings(HSRC),the residual strain,microstructure,crystal orientation,and microhardness surrounding fatigue cracks were investigated.Results show that the formation and propagation of fatigue cracks in HSRC have no correlation with the crystal orientation and boundaries of grains.The hardness and residual strain in the field around the fatigue crack are lower than those in other regions.The compressive strain around the fatigue crack is released after crack propagates,which reduces the hardness around the fatigue crack.Deformation twins and dislocations play a key role in the work hardening of HSRC.
