Microwave was applied to roasting the zinc oxide fume obtained from fuming furnace for the removal of F and Cl. The effects of important parameters, such as roasting temperature, holding time and stirring speed, were ...Microwave was applied to roasting the zinc oxide fume obtained from fuming furnace for the removal of F and Cl. The effects of important parameters, such as roasting temperature, holding time and stirring speed, were investigated and the process conditions were optimized using response surface methodology (RSM). The results show that the effects of roasting temperature and holding time on the removal rate of F and Cl are the most significant, and the effect of stirring speed is the second. The defluorination rate reaches 92.6% while the dechlorination rate reaches 90.2%, under the process conditions of roasting temperature of 700 °C, holding time of 80 min and stirring speed of 120 r/min. The results indicate that the removal of F and Cl from fuming furnace production of zinc oxide fumes using microwave roasting process is feasible and reliable.展开更多
[Objective] In order to take full advantage of processing by-product of water chestnut, the microwave extraction method of flavonoids from water chestnut skin dregs was optimized. The extracted flavonoids had a relati...[Objective] In order to take full advantage of processing by-product of water chestnut, the microwave extraction method of flavonoids from water chestnut skin dregs was optimized. The extracted flavonoids had a relatively high yield. [Method] The Box-Behnken design-based response surface method was adopted to optimize the microwave extraction of flavonoids from water chestnut skin dregs, a by-product of water chestnut starch. The mathematical relationships between various influencing factors and flavonoids yield were established. [Result] The optimum extraction conditions of flavonoids from water chestnut skin dregs were as follows: ethanol concentration of 55.4%, solid/liquid ratio of 1:30 g/ml, microwave power of 320 W, microwave time of 3 min and microwave time of 2 times. Under the optimum extraction conditions, the theoretical flavonoids yield was 2.376%. However, the actual flavonoids yield under the optimum extraction conditions was 2.365%. The relative error between actual values and theoretically predicted values was 0.461%. [Conclusion] The results showed the optimized extraction method is reliable, and it can provide a reference for the comprehensive and highly efficient utilization of water chestnut processing wastes.展开更多
In order to optimize the microwave-assisted extraction technology of polyphenols from Loropetalum chinense (R. Br.) Oliv., the effects of microwave power, ethanol concentration, solid to liquid ratio and extraction ...In order to optimize the microwave-assisted extraction technology of polyphenols from Loropetalum chinense (R. Br.) Oliv., the effects of microwave power, ethanol concentration, solid to liquid ratio and extraction time on polyphenols extraction rate were investigated. On the basis of single-factor test, a four-factor and three-level orthogonal test was designed by response surface method to establish a mathematical model between the response value and various factors. The results showed that the intensity of effect of different influencing factor on polyphenols ex- traction rate ranked as microwave power's〉solid to liquid ratio's〉extraction time's〉 ethanol concentration's. The optimum microwave-assisted extraction conditions for polyphenols from L. chinense were as follows: extraction power 254 W, ethanol concentration 60%, extraction time 12.5 rain and solid to liquid ratio 1:17. Under the optimum extraction conditions, the extraction rate of polyphenols from L. chinense was 19.17%.展开更多
In the non-linear microwave drying process, the incremental improved back-propagation (BP) neural network and response surface methodology (RSM) were used to build a predictive model of the combined effects of ind...In the non-linear microwave drying process, the incremental improved back-propagation (BP) neural network and response surface methodology (RSM) were used to build a predictive model of the combined effects of independent variables (the microwave power, the acting time and the rotational frequency) for microwave drying of selenium-rich slag. The optimum operating conditions obtained from the quadratic form of the RSM are: the microwave power of 14.97 kW, the acting time of 89.58 min, the rotational frequency of 10.94 Hz, and the temperature of 136.407 ℃. The relative dehydration rate of 97.1895% is obtained. Under the optimum operating conditions, the incremental improved BP neural network prediction model can predict the drying process results and different effects on the results of the independent variables. The verification experiments demonstrate the prediction accuracy of the network, and the mean squared error is 0.16. The optimized results indicate that RSM can optimize the experimental conditions within much more broad range by considering the combination of factors and the neural network model can predict the results effectively and provide the theoretical guidance for the follow-up production process.展开更多
Under microwave irradiation, with dimethypyridine-2,6-dicarboxylate and hydrazine hydrate as raw materials, 2,6-pyridine dicarboxylic hydrazine was produced. At the same time, the influence factors of production rate,...Under microwave irradiation, with dimethypyridine-2,6-dicarboxylate and hydrazine hydrate as raw materials, 2,6-pyridine dicarboxylic hydrazine was produced. At the same time, the influence factors of production rate, such as microwave radiation time, reaction power, the amount of dimethypyridine-2,6-dicarboxylate and hydrazine hydrate was further explored. Through the orthogonal experiments, better technology conditions were found which make the synthetic process turn from the new type of microwave technology.展开更多
A microwave photonic filter(MPF) based on multi-wavelength fiber laser and infinite impulse response(IIR) is proposed. The filter uses a multi-wavelength fiber laser as the light source, two sections of polarization m...A microwave photonic filter(MPF) based on multi-wavelength fiber laser and infinite impulse response(IIR) is proposed. The filter uses a multi-wavelength fiber laser as the light source, two sections of polarization maintaining fiber(PMF) and three polarization controllers(PCs) as the laser frequency selection device. By adjusting the PC to change the effective length of the PMF, the laser can obtain three wavelength spacings, which are 0.44 nm, 0.78 nm and 1.08 nm, respectively. And the corresponding free spectral ranges(FSRs) are 8.46 GHz, 4.66 GHz and 3.44 GHz, respectively. Thus changing the wavelength spacing of the laser can make the FSR variable. An IIR filter is introduced based on a finite impulse response(FIR) filter. Then the 3-d B bandwidth of the MPF is reduced, and the main side-lobe suppression ratio(MSSR) is increased. By adjusting the gain of the radio frequency(RF) signal amplifier, the frequency response of the filter can be enhanced.展开更多
基金Project(51104073)supported by the National Natural Science Foundation of ChinaProject(2013AA064003)supported by the High-tech Research and Development Program of China+1 种基金Project(2014CB643404)supported by the National Basic Research Program of ChinaProject(2012HB008)supported by Yunnan Province Young Academic Technology Leader Reserve Talents,China
文摘Microwave was applied to roasting the zinc oxide fume obtained from fuming furnace for the removal of F and Cl. The effects of important parameters, such as roasting temperature, holding time and stirring speed, were investigated and the process conditions were optimized using response surface methodology (RSM). The results show that the effects of roasting temperature and holding time on the removal rate of F and Cl are the most significant, and the effect of stirring speed is the second. The defluorination rate reaches 92.6% while the dechlorination rate reaches 90.2%, under the process conditions of roasting temperature of 700 °C, holding time of 80 min and stirring speed of 120 r/min. The results indicate that the removal of F and Cl from fuming furnace production of zinc oxide fumes using microwave roasting process is feasible and reliable.
文摘[Objective] In order to take full advantage of processing by-product of water chestnut, the microwave extraction method of flavonoids from water chestnut skin dregs was optimized. The extracted flavonoids had a relatively high yield. [Method] The Box-Behnken design-based response surface method was adopted to optimize the microwave extraction of flavonoids from water chestnut skin dregs, a by-product of water chestnut starch. The mathematical relationships between various influencing factors and flavonoids yield were established. [Result] The optimum extraction conditions of flavonoids from water chestnut skin dregs were as follows: ethanol concentration of 55.4%, solid/liquid ratio of 1:30 g/ml, microwave power of 320 W, microwave time of 3 min and microwave time of 2 times. Under the optimum extraction conditions, the theoretical flavonoids yield was 2.376%. However, the actual flavonoids yield under the optimum extraction conditions was 2.365%. The relative error between actual values and theoretically predicted values was 0.461%. [Conclusion] The results showed the optimized extraction method is reliable, and it can provide a reference for the comprehensive and highly efficient utilization of water chestnut processing wastes.
基金Supported by Open Funds for Innovation Platforms of Colleges and Universities in Hunan Province(15K066)National College Students'Innovative Entrepreneuria Training Program(201510553003)Research Study and Innovative Experiment Plan Project for College Students in Hunan Province(2015-499)~~
文摘In order to optimize the microwave-assisted extraction technology of polyphenols from Loropetalum chinense (R. Br.) Oliv., the effects of microwave power, ethanol concentration, solid to liquid ratio and extraction time on polyphenols extraction rate were investigated. On the basis of single-factor test, a four-factor and three-level orthogonal test was designed by response surface method to establish a mathematical model between the response value and various factors. The results showed that the intensity of effect of different influencing factor on polyphenols ex- traction rate ranked as microwave power's〉solid to liquid ratio's〉extraction time's〉 ethanol concentration's. The optimum microwave-assisted extraction conditions for polyphenols from L. chinense were as follows: extraction power 254 W, ethanol concentration 60%, extraction time 12.5 rain and solid to liquid ratio 1:17. Under the optimum extraction conditions, the extraction rate of polyphenols from L. chinense was 19.17%.
基金Project(50734007) supported by the National Natural Science Foundation of China
文摘In the non-linear microwave drying process, the incremental improved back-propagation (BP) neural network and response surface methodology (RSM) were used to build a predictive model of the combined effects of independent variables (the microwave power, the acting time and the rotational frequency) for microwave drying of selenium-rich slag. The optimum operating conditions obtained from the quadratic form of the RSM are: the microwave power of 14.97 kW, the acting time of 89.58 min, the rotational frequency of 10.94 Hz, and the temperature of 136.407 ℃. The relative dehydration rate of 97.1895% is obtained. Under the optimum operating conditions, the incremental improved BP neural network prediction model can predict the drying process results and different effects on the results of the independent variables. The verification experiments demonstrate the prediction accuracy of the network, and the mean squared error is 0.16. The optimized results indicate that RSM can optimize the experimental conditions within much more broad range by considering the combination of factors and the neural network model can predict the results effectively and provide the theoretical guidance for the follow-up production process.
文摘Under microwave irradiation, with dimethypyridine-2,6-dicarboxylate and hydrazine hydrate as raw materials, 2,6-pyridine dicarboxylic hydrazine was produced. At the same time, the influence factors of production rate, such as microwave radiation time, reaction power, the amount of dimethypyridine-2,6-dicarboxylate and hydrazine hydrate was further explored. Through the orthogonal experiments, better technology conditions were found which make the synthetic process turn from the new type of microwave technology.
基金supported by the National High Technology Research and Development Program of China(No.2013AA014200)the National Natural Science Foundation of China(No.11444001)the Tianjin Natural Science Foundation(No.14JCYBJC16500)
文摘A microwave photonic filter(MPF) based on multi-wavelength fiber laser and infinite impulse response(IIR) is proposed. The filter uses a multi-wavelength fiber laser as the light source, two sections of polarization maintaining fiber(PMF) and three polarization controllers(PCs) as the laser frequency selection device. By adjusting the PC to change the effective length of the PMF, the laser can obtain three wavelength spacings, which are 0.44 nm, 0.78 nm and 1.08 nm, respectively. And the corresponding free spectral ranges(FSRs) are 8.46 GHz, 4.66 GHz and 3.44 GHz, respectively. Thus changing the wavelength spacing of the laser can make the FSR variable. An IIR filter is introduced based on a finite impulse response(FIR) filter. Then the 3-d B bandwidth of the MPF is reduced, and the main side-lobe suppression ratio(MSSR) is increased. By adjusting the gain of the radio frequency(RF) signal amplifier, the frequency response of the filter can be enhanced.