降水云含有水膜冰球时的微波辐亮温

利用Eddington近似解析算法和一含有冰水相态混合层的降水云模型，改变滴谱，并／或使云中冰球带上水膜，可以改变云内一些高度上的辐射通量，而对降水云在云顶和地面两处的射出辐亮温的影响，则与雨强和微波频率以及水膜冰球谱和水膜厚度有关。云中相态混合层内水成物相态和滴谱对6．6、10．7和18GHz辐射传输和射出辐亮温有较大的影响，对更高的频率（37．0、85．6和183GHz）影响较小。

微波辅助萃取/气相色谱-质谱联用分析蔬菜中的有机磷农药

建立了微波辅助萃取 (MAE) /气相色谱 质谱联用法 (GC MS)测定蔬菜样品中二嗪磷、对硫磷、水胺硫磷的分析方法 ,研究了不同溶剂的萃取效率。选择二氯甲烷为萃取溶剂 ,采用二因素三水平的正交设计实验优化了萃取溶剂体积和萃取时间。方法的线性范围分别为二嗪磷和对硫磷 4ng/ g～ 40 0ng/ g、水胺硫磷 2 0ng/ g～ 40 0ng/ g,检出限分别为二嗪磷 0 2 9ng/g、对硫磷 1 70ng/g、水胺硫磷 2 30ng/g。测定 2 0 0 0ng/g和 50 0ng/g加标蔬菜样品 ,回收率为 72 2 %～ 1 0 2 0 % ,RSD为 1 5 %～ 1 1 0 %。与传统的机械振荡萃取法相比 ,不仅萃取效率相当 。

微波辅助下MMA/AA无皂乳液聚合的反应性研究

在微波辐照条件下,采用无皂乳液聚合的方法合成甲基丙烯酸甲酯和丙烯酸的共聚物,考察一定条件下引发剂用量、单体配比、微波辐射时间对单体转化率的影响;利用场发射扫描电镜和红外光谱对共聚物的形状、大小、结构进行分析。结果表明:引发剂用量控制在0.1%～0.5%,VMMA∶VAA控制在(10∶1)～(5∶1),微波辐射时间为45 min时,可以得到单体转化率较高、均一稳定的乳胶粒子;并且粒径随着引发剂用量的增大而减小,随着AA所占比例的增大而增大。

Comparison between Infrared and Microwave Radiometers for Retrieving Sea Surface Temperature

The basic principles of sea surface temperature （SST） remote sensing using infrared and microwave radiometers are introduced, and the differences between two sensors for retrieving sea surface temperature are investigated. The ground resolution, atmospheric effect, sea surface wind, skin depth and so on have important influence on precision of sea surface temperature retrieved by two sensors. The better understanding of the advantage and disadvantage of sea surface temperature detected by infrared and microwave radiometers would help us to imply SST remote sensing data more effectively and correctly.

Structural design and experimental research of microwave radiation heater for asphalt pavements

In order to improve the efficiency of heating and the uniformity of temperature distribution in recycling asphalt mixtures, a pyramidal radiation heater is designed. The principles of designing horn surface size and antenna length are established according to the law of energy conservation and microwave antenna radiation theory. Modeling and simulation are carried out using IE3D software. The simulation results demonstrate that, with a fixed horn surface size, the shortened electric antenna length is the main factor leading to the improved heating uniformity. On the other hand, with a fixed antenna length and diminished surface size, the standing wave ratio decreases with the improved radiation efficiency. Furthermore, the efficiency of radiation drops with increased distance between the horn surface and the asphalt pavement. Microwave heating experiments are carried out using this type of heater. The temperature distribution of asphalt samples is obtained by the grid temperature measurement method, and Matlab simulation is performed. The experimental results are in good agreement with the simulation.

Heat transfer model for microwave hot in-place recycling of asphalt pavements

In order to solve for temperature fields in microwave heating for recycling asphalt mixtures, a two-dimensional heat transfer model for the asphalt mixtures within the heating range is built based on the theory of unsteady heat conduction. Four onedimensional heat transfer models are established for the asphalt mixtures outside the heating range, which are simplified into four half-infinite solids. The intensity of the radiation electric field is calculated through experiment by using heating water loads. It is suggested that the mathematical model of boundary conditions can be established in two ways, which are theoretical deduction and experimental reverse. The actual temperature field is achieved by fitting temperatures of different positions collected in the heating experiment. The simulant temperature field, which is solved with the Matlab PDE toolbox, is in good agreement with the actual temperature field. The results indicate that the proposed models have high precision and can be directly used to calculate the temperature distribution of asphalt pavements.

Rapid microwave irradiation fast preparation and characterization of few-layer graphenes

Few-layer graphenes were fabricated from expandable graphite by rapid microwave exfoliation. Expandable graphite was irradiated in a domestic microwave in full power for 3 min, then soaked in mixed strong hydrogen nitrate and sulfuric acid with volume ratio of 1：1 for 24 h and re-irradiated, thus few-layer graphene sheets were obtained. Specimens gained from every step were selectively characterized by different techniques, such as SEM, XRD, Raman, AFM, XPS, FTIR and combustion elemental analysis. The results show that expandable graphite with loose, porous and worm-like morphology forms instantaneously in microwave irradiation with crackling sound and sparkles, which manifests physical exfoliation of graphene sheets. Few-layer graphene sheets with a dozen or more layers and average thickness of about 4.7 nm are obtained eventually after sequential treatment of microwave irradiation, mixed acid soaking and second microwave irradiation. The as-prepared few-layer graphenes still have high crystallinity and high purity with traces of oxide groups and without serious unrecoverable oxidation damage.

Oxidative Degradation of Soda Lignin Assisted by Microwave Irradiation

The effects of oxidant dosage,oxidation temperature and time on the degradation of soda lignin by hydrogen peroxide with and without the presence of microwave irradiation were investigated.It is found that the oxidative degradation of lignin includes the cleavage of ether bond inβ-O-4 structure,the partial destruction of aromatic ring,and the re-condensation of the degraded lignin.Compared to the conventionally heated oxidation of lignin,the microwave irradiation efficiently facilitates the degradation of the lignin with high molecular weight and the re-condensation of that with low molecular weight at a low oxidant dosage,low oxidation temperature,or a short oxidation time,which leads to the formation of the degraded lignin with narrower molecular weight distribution and lower molecular weight.Additionally,the lignin degraded in the presence of microwave irradiation has the characteristics of higher content of phenolic hydroxyl group,lower content of methoxyl group,and lower degree of condensation,which enhances the reactivity of lignin.Therefore,the oxidative degradation of lignin assisted by microwave irradiation may be a new pretreatment approach for efficiently utilizing the soda lignin.

Drying Kinetics and Energy Consumption in Vacuum Drying Process with Microwave and Radiant Heating

The general objective of this work is to analyze energy input in a vacuum process with the incorporation of microwave heating. Thus, necessary criteria for designing an efficient freeze-drying operation are considered through the analysis of strategies based on the combination of different intensities of radiant and microwave heating.The other aim of this research topic is to study the kinetics of drying in relation to mass transfer parameters.Five freeze-drying strategies using both heating systems were used. Consequently, energy input could be related to diffusivity coefficients, temperature and pressure profiles during dehydration of the product and analyzed in comparison to a conventional freeze-drying process.

Comparison of CloudSat Cloud Liquid Water Paths in Arctic Summer Using Ground-Based Microwave Radiometer

Arctic clouds strongly influence the regional radiation balance, temperature, melting of sea ice, and freezing of sea water. Despite their importance, there is a lack of systematic and reliabie observations of Arctic clouds. The CloudSat satellite launched in 2006 with a 94GHz Cloud Profiling Radar （CPR） may contribute to close this gap. Here we compare one of the key parameters, the cloud liquid water path （LWP） retrieved from CloudSat observations and from microwave radiometer （MWR） data taken during the ASCOS （Arctic Summer Cloud Ocean Study） cruise of the research vessel Oden from August to September 2008. Over the 45 days of the ASCOS cruise, collocations closer than 3 h and 100 km were found in only 9 d, and collocations closer than 1 h and 30 km in only 2 d. The poor correlations in the scatter plots of the two LWP retrievals can be explained by the patchiness of the cloud cover in these two days （August 5th and September 7th）, as confirmed by coincident MODIS （Moderate-resolution Imaging Spectroradiome- ter） images. The averages of Oden-observed LWP values are systematically higher （40-70 g m-2） than the corresponding CloudSat observations （0-50 g m2）. These are cases of generally low LWP with presumably small droplets, and may be explained by the little sensitivity of the CPR to small droplets or by the surface clutter.

Satellite retrieval of hurricane wind speeds using the AMSR2 microwave radiometer

The AMSR2 microwave radiometer is the main payload of the GCOM-W1 satellite,launched by the Japan Aerospace Exploration Agency in 2012. Based on the pre-launch information extraction algorithm,the AMSR2 enables remote monitoring of geophysical parameters such as sea surface temperature,wind speed,water vapor,and liquid cloud water content. However,rain alters the properties of atmospheric scattering and absorption,which contaminates the brightness temperatures measured by the microwave radiometer. Therefore,it is difficult to retrieve AMSR2-derived sea surface wind speeds under rainfall conditions. Based on microwave radiative transfer theory,and using AMSR2 L1 brightness temperature data obtained in August 2012 and NCEP reanalysis data,we studied the sensitivity of AMSR2 brightness temperatures to rain and wind speed,from which a channel combination of brightness temperature was established that is insensitive to rainfall,but sensitive to wind speed. Using brightness temperatures obtained with the proposed channel combination as input parameters,in conjunction with HRD wind field data,and adopting multiple linear regression and BP neural network methods,we established an algorithm for hurricane wind speed retrieval under rainfall conditions. The results showed that the standard deviation and relative error of retrievals,obtained using the multiple linear regression algorithm,were 3.1 m/s and 13%,respectively. However,the standard deviation and relative error of retrievals obtained using the BP neural network algorithm were better(2.1 m/s and 8%,respectively). Thus,the results of this paper preliminarily verified the feasibility of using microwave radiometers to extract sea surface wind speeds under rainfall conditions.

Dynamic compressive strength and failure mechanisms of microwave damaged sandstone subjected to intermediate loading rate

To investigate the influence of microwave heating on the dynamic behavior and failure mechanisms of rock,dynamic compression tests were conducted on microwave-irradiated sandstone specimens using a modified split Hopkinson pressure bar(SHPB)system.Experimental results show that microwave radiation can effectively weaken the compressive strength of sandstone.Rock specimens show three different failure modes under impact load:tensile failure,tensile−shear composite failure and compressive−shear failure.The dynamic Poisson’s ratio,calculated using the measured P-and S-wave velocities,is introduced to describe the deformation characteristics of sandstone.With the increase in microwave power and heating time,the Poisson’s ratio declines first and then increases slightly,and the turning point occurs at 244.6℃.Moreover,the microstructural characteristics reveal that microwave radiation produces dehydration,pore expansion,and cracking of the rock.The damage mechanisms caused by microwave radiation are discussed based on thermal stress and steam pressure inside the rock,which provides a reasonable explanation for the experimental results.

Mutagenesis and Screening of High Yield Xylanase Production Strain of Aspergillus usamii by Microwave Irradiation

A high yield xylanase producing strain, A. usamii L336-23, was screened out from its parent strain A.usamii L336 after microwave irradiation. Its productivity of xylanase activity increased by 35.7% from 21000μu·ml-1 to 28500μu·ml-1 and was stable after frequent subcultures and storage for more than two months. The mechanism of microwave mutation was also discussed.

Synthesis and thermoelectric properties of Mg_2Si_(1-x)Sn_x solid solutions by microwave irradiation

In order to reduce the oxidizing and volatilizing caused by Mg element in the traditional methods for synthesizing Mg2Sil-xSnx （x=0.2, 0.4, 0.6, 0.8） solid solutions, microwave irradiation techniques were used in preparing them as thermoelectric materials. Structure and phase composition of the obtained materials were investigated by X-ray diffraction （XRD）. The electrical conductivity, Seebeck coefficient and thermal conductivity were measured as a function of temperature from 300 to 750 K. It is found that Mg2Si1-xSnx solid solutions are well formed with excessive content of 5% （molar fraction） Mg from the stoichiometric MgESil.xSnx under microwave irradiation. A maximum dimensionless figure of merit, ZT, of about 0.26 is obtained for Mg2Si1-xSnx solid solutions at about 500 K for x=0.6.

Influence of assimilating ground-based microwave radiometer data into the WRF model on precipitation

Ground-based microwave radiometers profilers(MWRPs)have been used in numerical weather prediction(NWP)systems and show different impacts on forecasts.Currently,there are around hundreds of ground-based MWPRs used in weather stations over China;however,the application of MWPRs in NWP systems is rather limited.In this work,two MWRP retrieved profiles were assimilated into the Weather Research and Forecasting(WRF)model for a rainstorm event that occurred in Beijing,China.The quality of temperature and humidity profiles retrieved from the MWRP was evaluated against radiosonde observations and showed the reliability of the two MWRP products.Then,comparisons between the measurements of ground-based rain gauges and the corresponding forecasted precipitation in different periods of the rainstorm were investigated.The results showed that assimilating the two MWRPs affected the distribution and intensity of rainfall,especially in the early stage of the rainstorm.With the development of the rainstorm,adding MWRP data showed only a slight influence on the precipitation during the stable and mature period of the rainstorm,since the two MWRP observations were too limited to affect the large area of heavy rainfall.

Retrieval algorithm of sea surface wind vectors for WindSat based on a simple forward model

WindSat/Coriolis is the first satellite-borne polarimetric microwave radiometer, which aims to improve the potential of polarimetric microwave radiometry for measuring sea surface wind vectors from space. In this paper, a wind vector retrieval algorithm based on a novel and simple forward model was developed for WindSat. The retrieval algorithm of sea surface wind speed was developed using multiple linear regression based on the simulation dataset of the novel forward model. Sea surface wind directions that minimize the difference between simulated and measured values of the third and fourth Stokes parameters were found using maximum likelihood estimation, by which a group of ambiguous wind directions was obtained. A median filter was then used to remove ambiguity of wind direction. Evaluated with sea surface wind speed and direction data from the U.S. National Data Buoy Center （NDBC）, root mean square errors are 1.2 rn/s and 30~ for retrieved wind speed and wind direction, respectively. The evaluation results suggest that the simple forward model and the retrieval algorithm are practicable for near-real time applications, without reducing accuracy.

A new algorithm for sea-surface wind-speed retrieval based on the L-band radiometer onboard Aquarius

Aquarius is the second satellite mission to focus on the remote sensing of sea-surface salinity from space and it has mapped global sea-surface salinity for nearly 3 years since its launch in 2011. However,benefiting from the high atmospheric transparency and moderate sensitivity to wind speed of the L-band brightness temperature(TB),the Aquarius L-band radiometer can actually provide a new technique for the remote sensing of wind speed. In this article,the sea-surface wind speeds derived from TBs measured by Aquarius' L-band radiometer are presented,the algorithm for which is developed and validated using multisource wind speed data,including Wind Sat microwave radiometer and National Data Buoy Center buoy data,and the Hurricane Research Division of the Atlantic Oceanographic and Meteorological Laboratory wind field product. The error analysis indicates that the performance of retrieval algorithm is good. The RMSE of the Aquarius wind-speed algorithm is about 1 and 1.5 m/s for global oceans and areas of tropical hurricanes,respectively. Consequently,the applicability of using the Aquarius L-band radiometer as a near all-weather wind-speed measuring method is verified.

EXPERIMENTAL STUDY ON SOIL MOISTURE USING DUAL-FREQUENCY MICROWAVE RADIOMETER

An experiment of measuring soil moisture was carried out by using dual-frequency microwave radiometer designed by the authors. The measured data were analyzed by using statistical regression method and the empirical regression model of retrieving soil moisture in L-band and C-band was developed. The soil moisture in a rainfall event was retrieved using the experiential regression model, which is consistent well with the field sampling value. The results show that when soil moisture is lower than 75%, the brightness temperature is linear with soil moisture. However, when soil moisture is higher than 75%, the brightness temperature is not linear with soil moisture, so it is difficult for microwave radiometer to measure the changes of soil moisture. The experiment verifies the effectiveness and feasibility of microwave remote sensing soil moisture. Although this method for linear regression based on the data measured with the radiometer is simple, and has strong adaptability, generally it has only local application value, and lacks universal applicability for different areas and different conditions.