A new method for the control of the speed of an ultrasonic motor and its implementation are proposed. The method is merely used by detecting the time when motor′s monitor signal reaches a non zero reference valu...A new method for the control of the speed of an ultrasonic motor and its implementation are proposed. The method is merely used by detecting the time when motor′s monitor signal reaches a non zero reference value than a zero one, the direction, in which the driving frequency of the motor should be shifted, can be promptly calculated. With the aid of a CPU and the phase locked frequency doubling technique, the motor can be steadily driven in a wide range of frequency and the optimum frequency can be captured rapidly and precisely. Experiment shows that the above method is available.展开更多
Microencapsulation of phase change materials(Micro PCMs) has been paid special attention because of their extensive applications in saving and releasing energy. Micro PCMs containing paraffin with a melting point of ...Microencapsulation of phase change materials(Micro PCMs) has been paid special attention because of their extensive applications in saving and releasing energy. Micro PCMs containing paraffin with a melting point of 55 ℃ in polystyrene-divinylbenzene(P(St-DVB)) were prepared by suspension-like polymerization. The characterization of microcapsules by FTIR, DSC and TG proved that paraffin had been successfully encapsulated and the proportion of encapsulated paraffin was 49.8%—58.5%. The effects of polyvinylpyrrolidone(PVP) with different molecular weights serving as the suspension stabilizer were investigated in detail. The results illustrated that the type of PVP had a significant influence on the particle size of Micro PCMs. The average diameter of Micro PCMs decreased with an increasing molecular weight of PVP. Moreover, the crosslinker-postaddition method was adopted in this study to improve the morphology of P(St-DVB) Micro PCMs. SEM images showed that when the DVB was added at the 2nd hour of polymerization the morphology of obtained P(St-DVB) Micro PCMs exhibited good sphericity since it could avoid the influence of cross-linker agent during the nucleation period.展开更多
We applied the combination of in situ electrochemical liquid-phase microextraction and square-wave voltammetric stripping analysis for the first time as a highly sensitive and selective approach for the detection of d...We applied the combination of in situ electrochemical liquid-phase microextraction and square-wave voltammetric stripping analysis for the first time as a highly sensitive and selective approach for the detection of dopamine. A mixed gel of graphene sheets and an ionic liquid of 1-octyl-3-methylimidazolium hexaflurophosphate(OMim PF6) was used as a micro liquid-phase to pre-concentrate dopamine by controlled potential electrolysis from an aqueous solution(as a donor phase), followed by square-wave voltammetric stripping detection. Under optimized conditions, a linear calibration curve was obtained in the range of 0.05 to 1.0 ?mol/L in the presence of excess ascorbic acid and uric acid. The detection limit has been found to be 8.0 nmol/L(S/N=3).展开更多
文摘A new method for the control of the speed of an ultrasonic motor and its implementation are proposed. The method is merely used by detecting the time when motor′s monitor signal reaches a non zero reference value than a zero one, the direction, in which the driving frequency of the motor should be shifted, can be promptly calculated. With the aid of a CPU and the phase locked frequency doubling technique, the motor can be steadily driven in a wide range of frequency and the optimum frequency can be captured rapidly and precisely. Experiment shows that the above method is available.
基金financially supported by the National Natural Science Foundation of China (No. 20973022 and 11472048)the State Key Laboratory of Catalytic Materials and Reaction Engineering (RIPP, SINOPEC)
文摘Microencapsulation of phase change materials(Micro PCMs) has been paid special attention because of their extensive applications in saving and releasing energy. Micro PCMs containing paraffin with a melting point of 55 ℃ in polystyrene-divinylbenzene(P(St-DVB)) were prepared by suspension-like polymerization. The characterization of microcapsules by FTIR, DSC and TG proved that paraffin had been successfully encapsulated and the proportion of encapsulated paraffin was 49.8%—58.5%. The effects of polyvinylpyrrolidone(PVP) with different molecular weights serving as the suspension stabilizer were investigated in detail. The results illustrated that the type of PVP had a significant influence on the particle size of Micro PCMs. The average diameter of Micro PCMs decreased with an increasing molecular weight of PVP. Moreover, the crosslinker-postaddition method was adopted in this study to improve the morphology of P(St-DVB) Micro PCMs. SEM images showed that when the DVB was added at the 2nd hour of polymerization the morphology of obtained P(St-DVB) Micro PCMs exhibited good sphericity since it could avoid the influence of cross-linker agent during the nucleation period.
基金financially supported by the National Natural Science Foundation of China(21335001,21075004)
文摘We applied the combination of in situ electrochemical liquid-phase microextraction and square-wave voltammetric stripping analysis for the first time as a highly sensitive and selective approach for the detection of dopamine. A mixed gel of graphene sheets and an ionic liquid of 1-octyl-3-methylimidazolium hexaflurophosphate(OMim PF6) was used as a micro liquid-phase to pre-concentrate dopamine by controlled potential electrolysis from an aqueous solution(as a donor phase), followed by square-wave voltammetric stripping detection. Under optimized conditions, a linear calibration curve was obtained in the range of 0.05 to 1.0 ?mol/L in the presence of excess ascorbic acid and uric acid. The detection limit has been found to be 8.0 nmol/L(S/N=3).
