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MnO_2微米容器的制备及缓蚀剂封装释放性能研究 被引量:1
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作者 谢洪彬 张邈 +2 位作者 张丝雨 王立达 刘贵昌 《电镀与涂饰》 CAS CSCD 北大核心 2015年第2期100-105,共6页
通过模板法制备了二氧化锰微米容器,利用脱溶剂法实现了微米容器对苯并三氮唑(BTA)的封装。通过扫描电子显微镜和X射线衍射仪表征了微米容器的表面形貌及晶体结构,使用红外光谱确定了微米容器对BTA缓蚀剂的负载,利用紫外可见分光光度计... 通过模板法制备了二氧化锰微米容器,利用脱溶剂法实现了微米容器对苯并三氮唑(BTA)的封装。通过扫描电子显微镜和X射线衍射仪表征了微米容器的表面形貌及晶体结构,使用红外光谱确定了微米容器对BTA缓蚀剂的负载,利用紫外可见分光光度计、交流阻抗谱、动电位极化曲线等测试手段分析了携载BTA缓蚀剂的Mn O2微米容器在模拟海水中BTA的释放速率及缓蚀性能。结果表明,脱溶剂法可有效地实现Mn O2微米容器对BTA缓蚀剂的封装,封装量为3.9%,而且携载BTA缓蚀剂的Mn O2微米容器在3.5%Na Cl溶液中能有效地释放BTA,实现了对铜基体的腐蚀防护。 展开更多
关键词 二氧化锰 微米容器 苯并三氮唑 缓蚀剂 封装 防腐
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Experiment and simulation of diffusion of micron-particle in porous ceramic vessel 被引量:2
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作者 李彩亭 张巍 +6 位作者 魏先勋 高宏亮 文青波 樊小鹏 刘海 舒心 魏蔚 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第12期2358-2365,共8页
The general behavior of micron-particles in the inner domain of porous ceramic vessel was simulated by computational fluid dynamics software in terms of sampling experimental data.The results show that there is an opt... The general behavior of micron-particles in the inner domain of porous ceramic vessel was simulated by computational fluid dynamics software in terms of sampling experimental data.The results show that there is an optimum porosity of 0.32 to get a higher efficiency and lower pressure drop during filtration.According to the results of simulation and experiment,it is evident that lower inlet velocity can maintain lower pressure drop and obtain higher collection efficiency and inlet concentration also has a crucial influence on the collection efficiency.The collection efficiency of equipment increases significantly with the increase of inlet concentration when the inlet concentration is less than 6.3 g/m3,but it gradually tends to be stable in the range of 97.3%-99.7%when the inlet concentration is over this concentration. 展开更多
关键词 micron particle ceramic vessel pressure drop porous medium
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