Tensile test of the as-cast Mg-6Zn-2Er alloy was conducted at room temperature. The results indicate that the alloy is inclined to failure when the strain reaches 5.6%. The coarse secondary phases are responsible for ...Tensile test of the as-cast Mg-6Zn-2Er alloy was conducted at room temperature. The results indicate that the alloy is inclined to failure when the strain reaches 5.6%. The coarse secondary phases are responsible for the failure, especially for the Mg3Zn3Er2 phase (W-phase). It is indicated that the existence of the W-phase activates the stress concentrations due to the incapacity of W-phase for the load transfer, which results in the void at the inner of the W-phase. In comparison, the interface between the matrix and the secondary phase is stable. In conclusion, the characters of the secondary phases with respect to size, distribution, morphology and type, play an important role in the plastic deformation behavior of the alloy.展开更多
The nominal Ti44Al6Nb1.0Cr2.0V alloy was newly designed and prepared by vacuum consumable melting technique with the ingot sizes of d225 mm×320 mm. The results show that the average lamella colony size is 780-18...The nominal Ti44Al6Nb1.0Cr2.0V alloy was newly designed and prepared by vacuum consumable melting technique with the ingot sizes of d225 mm×320 mm. The results show that the average lamella colony size is 780-1830 μm. This as-cast alloy has a modified near lamellar(M-NL) structure that is composed of mainly larger(α2+γ) lamella colonies and smaller(B2+equiaxed γ) blocky morphology. It exhibits the moderate tensile properties at room temperature, in which the Region(5) yields the ultimate tensile strength(UTS) about 499 MPa and the elongation about 0.53%. The obvious brittle fracture characteristics and trans-granular interlamellar fracture are the predominant modes. After room temperature tensile testing, there are some <101] and a few 1/2<112] superdislocations in the γ phase. The as-cast microcrack is the main factor to deteriorate the tensile property, which results in the premature fracture, poor ductility and few dislocations. The addition of Nb, Cr and V can decrease stacking fault energy(SFE) obviously, which is helpful to enhancing the ductility of the alloy.展开更多
Vickers indentation test was used to study the effects of mineral composition and microstructure on crack resistance of sintered ore, and the initiation and propagation of cracks in different minerals contained in sin...Vickers indentation test was used to study the effects of mineral composition and microstructure on crack resistance of sintered ore, and the initiation and propagation of cracks in different minerals contained in sintered ore were examined. The results indicate that the microstructure of calcium ferrites is a major factor influencing crack resistance of sintered ore. Finer grain size of calcium ferrite will lead to higher cracking threshold and better crack resistance of sintered ore. The formation of calcium ferrite with fine grain size during sintering process is favorable for crack resistance of sintered ore.展开更多
Microstructural analysis and fatigue crack propagation behavior of three types of rail steels, was performed. These are premium pearlitic, austenitic manganese (AM) and bainitic rail steels. Rectangular un-notched a...Microstructural analysis and fatigue crack propagation behavior of three types of rail steels, was performed. These are premium pearlitic, austenitic manganese (AM) and bainitic rail steels. Rectangular un-notched and notched test specimens were machined from railheads of each material using electrical discharge machining (EDM) and used for the mechanical properties and fatigue evaluation respectively. Bainitic steel has the highest yield strength, ultimate strength, and strain to failure as compared to both pearlitic and austenitic manganese steels. Fatigue studies showed that the crack speed for the bainitic steel is lower than that for the pearlitie and the AM steels over the entire range of the energy release rate. The bainitic steel exhibits a higher rate of crack deceleration in the second stage, as indicated by the lower slope of the fatigue crack propagation kinetics curve in comparison with the pearlitic and manganese rail steels. This attests to the superior fatigue damage tolerance of the bainitic rail steel in comparison to pearlitic and austenitic manganese rail steels. Microstructural analysis of the three rail steels revealed that bainitic steel has a more intricate structure than AM and pearlitic steels. AM steel shows very few signs of being work hardened or toughened, which usually increases the mechanical properties of the material. As the number of alloying elements increase, the microstructure of the steel becomes more complex, resulting in the increase of mechanical properties and fatigue fracture resistance of bainitic rail steel.展开更多
The influence of applied temperatures on the creep rupture life of the third-generation low-cost single crystal(SX)superalloy with Pt-Al coating was evaluated.The creep damage was observed under the conditions of 1100...The influence of applied temperatures on the creep rupture life of the third-generation low-cost single crystal(SX)superalloy with Pt-Al coating was evaluated.The creep damage was observed under the conditions of 1100℃/137 MPa,1120℃/137 MPa,and 1140℃/137 MPa.Results show that the properties of bare superalloy outperform those of coated superalloy under all test conditions.The most significant reduction in creep life reaches 50%when the test condition is 1100℃/137 MPa.At higher temperatures(1120 and 1140℃),the crack propagation rate in Pt-Al coatings to SX superalloy substrate decreases,thereby reducing the degradation degree of mechanical properties.Instead of the penetration into SX substrate,tip oxidation and Al diffusion of the coating cracks cause the formation of oxides,therefore leading to the slow degradation in microstructures of the substrate beneath the coating.At 1100℃,however,the microstructure of coating/SX superalloy substrate degrades due to the Al internal diffusion.This diffusion mechanism promotes the formation of harmful topologically close packed phases around 1100℃.At 1120 and 1140℃,the dislocation of SX superalloy substrate beneath the coating is relatively unchanged,compared to that in the inner superalloy.In contrast,the dislocation network of the substrate beneath the coating becomes sparse,and the number of superdislocations cutting intoγ′phases increases at 1100℃.展开更多
When two contacting solid surfaces are tightly closed and invisible to the naked eye, the discontinuity is said to be microscopic regardless of whether its length is short or long. By this definition, it is not suffic...When two contacting solid surfaces are tightly closed and invisible to the naked eye, the discontinuity is said to be microscopic regardless of whether its length is short or long. By this definition, it is not sufficient to distinguish the difference between a micro- and macro-crack by using the length parameter. Microcracks in high strength metal alloys have been known to be sev- eral centimeters or longer. Considered in this work is a dual scale fatigue crack growth model where the main crack can be mi- cro or macro but there prevails an inherent microscopic tip region that is damaged depending on the irregularities of the micro- structure. This region is referred to as the "micro-tip" and can be simulated by a sharp wedge with different angles in addition to mixed boundary conditions. The combination is sufficient to model microscopic entities in the form of voids, inclusions, precipitations, interfaces, in addition to subgrain imperfections, or cluster of dislocations. This is accomplished by using the method of "singularity representation" such that closed form asymptotic solutions can be obtained for the development of fa- tigue crack growth rate relations with three parameters. They include: (1) the crack surface tightness o-* represented by Cro/Cr~ = 0.3-0.5 for short cracks in region I, and 0.1-0.2 for long cracks in region II, (2) the micro/macro material properties reflected by the shear modulus ratio/1" (=,L/micro/]-/macro varying between 2 and 5) and (3) the most sensitive parameter d* being the micro-tip characteristic length d* (=d/do) whose magnitude decreases in the direction of region I ---~II. The existing fatigue crack growth data for 2024-T3 and 7075-T6 aluminum sheets are used to reinterpret the two-parameter da/dN=C(AK)n relation where AK has now been re-derived for a microcrack with surfaces tightly in contact. The contact force will depend on the mean stress ~m or mean stress ratio R as the primary parameter and on the stress amplitude era as the secondary parameter.展开更多
Hot extrusion was conducted in the α+β phase region for promoting mechanical properties of Ti42Al9V0.3Y. The microstructures and tensile properties before and after hot extrusion were studied. The results show that ...Hot extrusion was conducted in the α+β phase region for promoting mechanical properties of Ti42Al9V0.3Y. The microstructures and tensile properties before and after hot extrusion were studied. The results show that the microstructure of the as-cast alloy mainly consists of massive γ phase in β matrix and the as-extruded alloy mainly consists of lamellar α2/γ, lamellar β/γ, and strip γ propagating from elongated β phase. In the as-cast alloy, the predominantly observed fracture mode is transgranular cleavage failure at room temperature and intergranular fracture at 650-750 °C. After hot extrusion, it transforms into transgranular cleavage-like failure, including translamellar cleavage and delamination. The excellent tensile properties of the as-extruded material are attributed to the obvious refined microstructure with broken YAl2 particles and the micro-crack shielding action of the TiAl lamellasome.展开更多
基金Projects(51071004,51101002)supported by the National Natural Science Foundation of ChinaProject(2011BAE22B01-3)supported by the National Science and Technology Supporting Plan during the 12th Five-Year Period,China
文摘Tensile test of the as-cast Mg-6Zn-2Er alloy was conducted at room temperature. The results indicate that the alloy is inclined to failure when the strain reaches 5.6%. The coarse secondary phases are responsible for the failure, especially for the Mg3Zn3Er2 phase (W-phase). It is indicated that the existence of the W-phase activates the stress concentrations due to the incapacity of W-phase for the load transfer, which results in the void at the inner of the W-phase. In comparison, the interface between the matrix and the secondary phase is stable. In conclusion, the characters of the secondary phases with respect to size, distribution, morphology and type, play an important role in the plastic deformation behavior of the alloy.
基金Project(2011CB605504)supported by the National Basic Research Program of ChinaProject(NCET-12-0153)supported by the Program of New Century Excellent Talents in UniversityProject(51274076)supported by the National Natural Science Foundation of China
文摘The nominal Ti44Al6Nb1.0Cr2.0V alloy was newly designed and prepared by vacuum consumable melting technique with the ingot sizes of d225 mm×320 mm. The results show that the average lamella colony size is 780-1830 μm. This as-cast alloy has a modified near lamellar(M-NL) structure that is composed of mainly larger(α2+γ) lamella colonies and smaller(B2+equiaxed γ) blocky morphology. It exhibits the moderate tensile properties at room temperature, in which the Region(5) yields the ultimate tensile strength(UTS) about 499 MPa and the elongation about 0.53%. The obvious brittle fracture characteristics and trans-granular interlamellar fracture are the predominant modes. After room temperature tensile testing, there are some <101] and a few 1/2<112] superdislocations in the γ phase. The as-cast microcrack is the main factor to deteriorate the tensile property, which results in the premature fracture, poor ductility and few dislocations. The addition of Nb, Cr and V can decrease stacking fault energy(SFE) obviously, which is helpful to enhancing the ductility of the alloy.
文摘Vickers indentation test was used to study the effects of mineral composition and microstructure on crack resistance of sintered ore, and the initiation and propagation of cracks in different minerals contained in sintered ore were examined. The results indicate that the microstructure of calcium ferrites is a major factor influencing crack resistance of sintered ore. Finer grain size of calcium ferrite will lead to higher cracking threshold and better crack resistance of sintered ore. The formation of calcium ferrite with fine grain size during sintering process is favorable for crack resistance of sintered ore.
文摘Microstructural analysis and fatigue crack propagation behavior of three types of rail steels, was performed. These are premium pearlitic, austenitic manganese (AM) and bainitic rail steels. Rectangular un-notched and notched test specimens were machined from railheads of each material using electrical discharge machining (EDM) and used for the mechanical properties and fatigue evaluation respectively. Bainitic steel has the highest yield strength, ultimate strength, and strain to failure as compared to both pearlitic and austenitic manganese steels. Fatigue studies showed that the crack speed for the bainitic steel is lower than that for the pearlitie and the AM steels over the entire range of the energy release rate. The bainitic steel exhibits a higher rate of crack deceleration in the second stage, as indicated by the lower slope of the fatigue crack propagation kinetics curve in comparison with the pearlitic and manganese rail steels. This attests to the superior fatigue damage tolerance of the bainitic rail steel in comparison to pearlitic and austenitic manganese rail steels. Microstructural analysis of the three rail steels revealed that bainitic steel has a more intricate structure than AM and pearlitic steels. AM steel shows very few signs of being work hardened or toughened, which usually increases the mechanical properties of the material. As the number of alloying elements increase, the microstructure of the steel becomes more complex, resulting in the increase of mechanical properties and fatigue fracture resistance of bainitic rail steel.
基金National Key Research and Development Program of China(2017YFA0700704)China Postdoctoral Science Foundation(2023M733570)+1 种基金Excellent Youth Foundation of Liaoning Province(2021-YQ-02)Science Center for Gas Turbine Project(P2021-A-Ⅳ-002-002)。
文摘The influence of applied temperatures on the creep rupture life of the third-generation low-cost single crystal(SX)superalloy with Pt-Al coating was evaluated.The creep damage was observed under the conditions of 1100℃/137 MPa,1120℃/137 MPa,and 1140℃/137 MPa.Results show that the properties of bare superalloy outperform those of coated superalloy under all test conditions.The most significant reduction in creep life reaches 50%when the test condition is 1100℃/137 MPa.At higher temperatures(1120 and 1140℃),the crack propagation rate in Pt-Al coatings to SX superalloy substrate decreases,thereby reducing the degradation degree of mechanical properties.Instead of the penetration into SX substrate,tip oxidation and Al diffusion of the coating cracks cause the formation of oxides,therefore leading to the slow degradation in microstructures of the substrate beneath the coating.At 1100℃,however,the microstructure of coating/SX superalloy substrate degrades due to the Al internal diffusion.This diffusion mechanism promotes the formation of harmful topologically close packed phases around 1100℃.At 1120 and 1140℃,the dislocation of SX superalloy substrate beneath the coating is relatively unchanged,compared to that in the inner superalloy.In contrast,the dislocation network of the substrate beneath the coating becomes sparse,and the number of superdislocations cutting intoγ′phases increases at 1100℃.
文摘When two contacting solid surfaces are tightly closed and invisible to the naked eye, the discontinuity is said to be microscopic regardless of whether its length is short or long. By this definition, it is not sufficient to distinguish the difference between a micro- and macro-crack by using the length parameter. Microcracks in high strength metal alloys have been known to be sev- eral centimeters or longer. Considered in this work is a dual scale fatigue crack growth model where the main crack can be mi- cro or macro but there prevails an inherent microscopic tip region that is damaged depending on the irregularities of the micro- structure. This region is referred to as the "micro-tip" and can be simulated by a sharp wedge with different angles in addition to mixed boundary conditions. The combination is sufficient to model microscopic entities in the form of voids, inclusions, precipitations, interfaces, in addition to subgrain imperfections, or cluster of dislocations. This is accomplished by using the method of "singularity representation" such that closed form asymptotic solutions can be obtained for the development of fa- tigue crack growth rate relations with three parameters. They include: (1) the crack surface tightness o-* represented by Cro/Cr~ = 0.3-0.5 for short cracks in region I, and 0.1-0.2 for long cracks in region II, (2) the micro/macro material properties reflected by the shear modulus ratio/1" (=,L/micro/]-/macro varying between 2 and 5) and (3) the most sensitive parameter d* being the micro-tip characteristic length d* (=d/do) whose magnitude decreases in the direction of region I ---~II. The existing fatigue crack growth data for 2024-T3 and 7075-T6 aluminum sheets are used to reinterpret the two-parameter da/dN=C(AK)n relation where AK has now been re-derived for a microcrack with surfaces tightly in contact. The contact force will depend on the mean stress ~m or mean stress ratio R as the primary parameter and on the stress amplitude era as the secondary parameter.
基金Project supported by the National Postdoctoral Foundation of Chinathe Youth Science and Technology Project of Harbin (No 2008RFQXG040),China
文摘Hot extrusion was conducted in the α+β phase region for promoting mechanical properties of Ti42Al9V0.3Y. The microstructures and tensile properties before and after hot extrusion were studied. The results show that the microstructure of the as-cast alloy mainly consists of massive γ phase in β matrix and the as-extruded alloy mainly consists of lamellar α2/γ, lamellar β/γ, and strip γ propagating from elongated β phase. In the as-cast alloy, the predominantly observed fracture mode is transgranular cleavage failure at room temperature and intergranular fracture at 650-750 °C. After hot extrusion, it transforms into transgranular cleavage-like failure, including translamellar cleavage and delamination. The excellent tensile properties of the as-extruded material are attributed to the obvious refined microstructure with broken YAl2 particles and the micro-crack shielding action of the TiAl lamellasome.