Synthesis of 2,6-pyridine Dimethyl Formate under Microwave Irradiation

An efficient synthesis of 2,6-pyridine dimethyl formate happened under the microwave irradiation is proposed. It is noteworthy that some factors influence the product yield such as time, temperature, ratio of reactants, and acidity which were discussed. The optimized quantity of 2,6-pyridine dimethyl acid is 10 mmol and methanol is 25 mmol. The yield is up to 95%-96% when using 2 mL 30% sulfuric acid. All products have been characterized by IR and 1H NMR.

班集体现代化:内涵、建构及实践探究

班集体是班主任工作的主阵地,班集体现代化是实现班主任现代化的关键要素,成功的班集体建设正是现代化班级发展的目标之一。文章将结合班本研究,从班集体现代化建设的内涵、建构及实践方面,就如何推动班集体现代化做一些探讨,以期为同行带来借鉴与启发。