The main problem in an efficient Zn（CH3COO）2/AC （AC-activated carbon） catalyst preparation is the achievement of uniform distribution of highly dispersed salt component on the activated carbon （AC） surface. The ...The main problem in an efficient Zn（CH3COO）2/AC （AC-activated carbon） catalyst preparation is the achievement of uniform distribution of highly dispersed salt component on the activated carbon （AC） surface. The solution of this problem is modification of the AC by hydrogen peroxide （H202） oxidation of the surface and treatment of AC with acetic acid as well as special methods of salt deposition and catalyst drying. The investigations of these ways of AC surface modification （treatment of AC with acetic acid and H2O2） have demonstrated the obtained AC to have both an increased adsorption capacity as to Zn（OAc）2 and optimum volumes of meso- and micro-pores as well as high catalyst activity in vinyl acetate （VA） synthesis. The characteristics of supports and catalysts were found out by benzene, water and acetic acid vapors adsorption. The distribution of the salt on the AC surface was studied by small-angle X-ray scattering （SAXS）, by scanning electron microscopy （SEM） and X-ray micro-analysis （XMA）. The catalysts were tested in vinyl acetate synthesis in flow-bed isothermal reactor by cyclic method at 175, 205 and 230℃.展开更多
This paper presents a method for determining the percentage of coarse aggregate in concrete specimens by image processing. The test pieces were produced with the aim of obtaining images of their cross sections through...This paper presents a method for determining the percentage of coarse aggregate in concrete specimens by image processing. The test pieces were produced with the aim of obtaining images of their cross sections through a scanner table. In order to increase the contrast between mortar and coarse aggregate the sliced surfaces were treated with the phenolphthale in solution. The images obtained in the scanner were processed in a program developed with MATLAB （matrix laboratory）. The average coarse aggregate in each section and the mean of coarse aggregate per test body were calculated. With the results, it was revealed that the method returned satisfying results when compared to the original trace of the concrete.展开更多
Three electrodeposited Fe-Ni,Fe-Co,and Fe-Ni-Co cores of thin film transformer are prepared on silicon(100) substrates,which are sputtered a 90 nm thick film of Cu acting as the seed layer.The core films consisting of...Three electrodeposited Fe-Ni,Fe-Co,and Fe-Ni-Co cores of thin film transformer are prepared on silicon(100) substrates,which are sputtered a 90 nm thick film of Cu acting as the seed layer.The core films consisting of Fe-Ni 20:80,Fe-Co 60:40 and Fe-Ni-Co 10:60:30,respectively,are deposited using direct current electrodeposition.The surface texture,electrical and magnetic properties are surveyed by scanning electron microscopy(SEM),superconducting quantum interference device(SQUID),etc.The wave transmission ability and efficiency of thin film transformer with these cores,inputting the sine wave,are compared.All the analyses indicate that FeNi alloy films display the optimal magnetic properties and excellent transformer performance.展开更多
The large-scale assembly and fabrication method for single-walled carbon nanotube(SWCNT) nano devices was implemented.Assembly of SWCNT field effect transistor(FET) was realized by floating potential dielectrophoresis...The large-scale assembly and fabrication method for single-walled carbon nanotube(SWCNT) nano devices was implemented.Assembly of SWCNT field effect transistor(FET) was realized by floating potential dielectrophoresis approach.The simulation of floating potential distribution of the chip was performed by comsol multiphysics coupling software.Six hundred devices were assembled on the area of less than one square centimeter.The fabricated devices were characterized by atomic force microscopy and scanning electron microscopy.The experimental results showed that large-scale assembly had been realized,and the success rate of ideal assembly for SWCNT FET had been assessed.展开更多
文摘The main problem in an efficient Zn（CH3COO）2/AC （AC-activated carbon） catalyst preparation is the achievement of uniform distribution of highly dispersed salt component on the activated carbon （AC） surface. The solution of this problem is modification of the AC by hydrogen peroxide （H202） oxidation of the surface and treatment of AC with acetic acid as well as special methods of salt deposition and catalyst drying. The investigations of these ways of AC surface modification （treatment of AC with acetic acid and H2O2） have demonstrated the obtained AC to have both an increased adsorption capacity as to Zn（OAc）2 and optimum volumes of meso- and micro-pores as well as high catalyst activity in vinyl acetate （VA） synthesis. The characteristics of supports and catalysts were found out by benzene, water and acetic acid vapors adsorption. The distribution of the salt on the AC surface was studied by small-angle X-ray scattering （SAXS）, by scanning electron microscopy （SEM） and X-ray micro-analysis （XMA）. The catalysts were tested in vinyl acetate synthesis in flow-bed isothermal reactor by cyclic method at 175, 205 and 230℃.
文摘This paper presents a method for determining the percentage of coarse aggregate in concrete specimens by image processing. The test pieces were produced with the aim of obtaining images of their cross sections through a scanner table. In order to increase the contrast between mortar and coarse aggregate the sliced surfaces were treated with the phenolphthale in solution. The images obtained in the scanner were processed in a program developed with MATLAB （matrix laboratory）. The average coarse aggregate in each section and the mean of coarse aggregate per test body were calculated. With the results, it was revealed that the method returned satisfying results when compared to the original trace of the concrete.
基金supported by the National Natural Science Foundation of China (Grant No. 60874101)
文摘Three electrodeposited Fe-Ni,Fe-Co,and Fe-Ni-Co cores of thin film transformer are prepared on silicon(100) substrates,which are sputtered a 90 nm thick film of Cu acting as the seed layer.The core films consisting of Fe-Ni 20:80,Fe-Co 60:40 and Fe-Ni-Co 10:60:30,respectively,are deposited using direct current electrodeposition.The surface texture,electrical and magnetic properties are surveyed by scanning electron microscopy(SEM),superconducting quantum interference device(SQUID),etc.The wave transmission ability and efficiency of thin film transformer with these cores,inputting the sine wave,are compared.All the analyses indicate that FeNi alloy films display the optimal magnetic properties and excellent transformer performance.
基金supported by the National Natural Science Foundation of China (Grant No. 51005230)China Postdoctoral Science Foundation(Grant No. 2012M520654)the Education Department of Liaoning Province Science and Technology Research Projects (Grant No. L2012213)
文摘The large-scale assembly and fabrication method for single-walled carbon nanotube(SWCNT) nano devices was implemented.Assembly of SWCNT field effect transistor(FET) was realized by floating potential dielectrophoresis approach.The simulation of floating potential distribution of the chip was performed by comsol multiphysics coupling software.Six hundred devices were assembled on the area of less than one square centimeter.The fabricated devices were characterized by atomic force microscopy and scanning electron microscopy.The experimental results showed that large-scale assembly had been realized,and the success rate of ideal assembly for SWCNT FET had been assessed.
