For the linear crack skeleton of railway bridges with irregular strike,it is difficult to accurately express the crack contour feature by using a single smoothing fitting algorithm.In order to improve the measurement ...For the linear crack skeleton of railway bridges with irregular strike,it is difficult to accurately express the crack contour feature by using a single smoothing fitting algorithm.In order to improve the measurement accuracy,a polynomial curve fitting was proposed,which used the calibration point of crack contour as the boundary point,and then put them all together to produce a continuous contour curve to achieve the crack length measurement.The method was tested by measuring the linar cracks with different shapes.It is shown that this proposed algorithm can not only solve the jagged problem generated in the crack skeleton extraction process,but also improve the crack length measurement accuracy.The relative deviation is less than 0.15,and the measurement accuracy is over 98.05%,which provides a more effective means for the crack length measurement in railway bridges.展开更多
The research on the application of X-ray diffraction in the quantitative analysis of Chinese medicines is rare. The main reason is that the technical problems related to the internal standard and the selection of quan...The research on the application of X-ray diffraction in the quantitative analysis of Chinese medicines is rare. The main reason is that the technical problems related to the internal standard and the selection of quantitative peaks are not well solved, and the accuracy and precision of the results are not satisfactory. This study employed the concept of mass absorption coefficient based on the internal standard method, and the full spectrum fitting and quantitative methods were used to solve the above technical problems. The sample was blended. the internal standard substance of zinc oxide was fully ground, and tablets were prepared by positive pressure method. Under certain instrumental conditions, the PXRD pattern was obtained by scanning. The percentage of gypsum fibrosum in Xiaokening tablet was obtained by quantitative analysis of full spectrum fitting internal standard by TOPAS software. The method was investigated by methodology. At the same time, the method was compared by ion chromatography, and SPSS software was used to make a significant t test on the results of the two methods. After the investigation, the average standard recovery rate of CaSO4-2H2O was 99.06%(RSD = 3.02%);and the recovery rate for simulated samples was 96.7%. The method had good specificity. After statistical analysis, there was no significant difference between the new PXRD method and the traditional method of ion chromatography.展开更多
基金National Defense Pre-Research Fund Project(No.060601)Wanqiao Education Fund Project(No.06010023)。
文摘For the linear crack skeleton of railway bridges with irregular strike,it is difficult to accurately express the crack contour feature by using a single smoothing fitting algorithm.In order to improve the measurement accuracy,a polynomial curve fitting was proposed,which used the calibration point of crack contour as the boundary point,and then put them all together to produce a continuous contour curve to achieve the crack length measurement.The method was tested by measuring the linar cracks with different shapes.It is shown that this proposed algorithm can not only solve the jagged problem generated in the crack skeleton extraction process,but also improve the crack length measurement accuracy.The relative deviation is less than 0.15,and the measurement accuracy is over 98.05%,which provides a more effective means for the crack length measurement in railway bridges.
文摘The research on the application of X-ray diffraction in the quantitative analysis of Chinese medicines is rare. The main reason is that the technical problems related to the internal standard and the selection of quantitative peaks are not well solved, and the accuracy and precision of the results are not satisfactory. This study employed the concept of mass absorption coefficient based on the internal standard method, and the full spectrum fitting and quantitative methods were used to solve the above technical problems. The sample was blended. the internal standard substance of zinc oxide was fully ground, and tablets were prepared by positive pressure method. Under certain instrumental conditions, the PXRD pattern was obtained by scanning. The percentage of gypsum fibrosum in Xiaokening tablet was obtained by quantitative analysis of full spectrum fitting internal standard by TOPAS software. The method was investigated by methodology. At the same time, the method was compared by ion chromatography, and SPSS software was used to make a significant t test on the results of the two methods. After the investigation, the average standard recovery rate of CaSO4-2H2O was 99.06%(RSD = 3.02%);and the recovery rate for simulated samples was 96.7%. The method had good specificity. After statistical analysis, there was no significant difference between the new PXRD method and the traditional method of ion chromatography.
