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不同产地大闸蟹风味表征及风味骨架成分差异
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作者 于明光 陈明昭 +2 位作者 宋焕禄 朱建设 邱曹华 《食品科学技术学报》 EI CAS CSCD 北大核心 2024年第5期135-147,共13页
大闸蟹以其鲜美的风味特点深受消费者喜爱。采用全二维气相色谱-嗅闻-质谱联用技术和液相色谱-二极管阵列检测器分析技术全面解析了不同产地大闸蟹中的风味物质,并结合主成分分析和正交偏最小二乘法判别分析探究了地域对大闸蟹风味骨架... 大闸蟹以其鲜美的风味特点深受消费者喜爱。采用全二维气相色谱-嗅闻-质谱联用技术和液相色谱-二极管阵列检测器分析技术全面解析了不同产地大闸蟹中的风味物质,并结合主成分分析和正交偏最小二乘法判别分析探究了地域对大闸蟹风味骨架成分的影响。研究结果表明:在来自5种不同产地的大闸蟹中共鉴定出68种气味化合物和19种滋味化合物,其中包括21种醛类、17种醇类、9种酮类、5种酸类、4种含氮化合物、3种酯类、4种芳香族类、5种其他类化合物及16种氨基酸和3种核苷酸。通过准确定量、气味和滋味活度值评估,确定了大闸蟹的风味骨架成分(在所有样品中的气味活度值或滋味活度值均≥1),包含16种气味和6种滋味化合物。结果表明,(E)-2-己烯醛、(E)-2-癸烯醛、芳樟醇、壬醛、己醛和1-辛烯-3-醇等6种气味化合物及精氨酸、丙氨酸和甘氨酸等3种滋味化合物可作为区分不同产地大闸蟹的指标性风味化合物。 展开更多
关键词 大闸蟹 气味成分 滋味成分 全二维气相色谱-嗅闻-质谱联用技术 指标化合物
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烟丝含水率对主流烟气CO等7种有害成分释放量的影响 被引量:22
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作者 刘志华 杨松 +4 位作者 王昆淼 何沛 李璠 陈永宽 缪明明 《烟草科技》 EI CAS 北大核心 2012年第1期29-33,共5页
为考察烟丝含水率对主流烟气CO等7种有害成分释放量的影响,采用3种饱和盐溶液制备了不同烟丝含水率的卷烟,分别收集3组卷烟的烟气总粒相物、测定主流烟气中CO等7种有害成分的释放量,并对卷烟的物理参数和固相燃烧温度进行了检测。结果表... 为考察烟丝含水率对主流烟气CO等7种有害成分释放量的影响,采用3种饱和盐溶液制备了不同烟丝含水率的卷烟,分别收集3组卷烟的烟气总粒相物、测定主流烟气中CO等7种有害成分的释放量,并对卷烟的物理参数和固相燃烧温度进行了检测。结果表明:①烟丝含水率对7种有害成分的释放量影响不尽相同,随着烟丝含水率的升高,卷烟主流烟气中氨(NH3)、4-(甲基亚硝胺基)-1-(3-吡啶基)-1-丁酮(NNK)、苯酚的释放量呈降低趋势,CO,苯并[a]芘(B[a]P)释放量呈升高趋势,氢氰酸(HCN)及巴豆醛的变化不明显;②烟丝含水率对卷烟的固相燃烧温度没有显著影响,但影响卷烟的燃烧速率(燃烧过程),进而影响了烟气成分的形成、转移和释放。 展开更多
关键词 卷烟 含水率 主流烟气 危害性指标化合物
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简易水处理活性炭的选择和应用方法 被引量:29
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作者 应维琪 常启刚 +1 位作者 张巍 蒋文新 《环境污染与防治》 CAS CSCD 北大核心 2005年第6期430-435,439,共7页
首先介绍活性炭性能测试与水处理活性炭选炭、吸附技术选择、工艺应用的关系,其次报导两个活性炭选用方面的改进方法。通过重新定义、整合、完善现有活性炭性能指标,建立了以酚值、碘值、亚甲基蓝、丹宁酸值为吸附性能指标的选炭方法。... 首先介绍活性炭性能测试与水处理活性炭选炭、吸附技术选择、工艺应用的关系,其次报导两个活性炭选用方面的改进方法。通过重新定义、整合、完善现有活性炭性能指标,建立了以酚值、碘值、亚甲基蓝、丹宁酸值为吸附性能指标的选炭方法。这四种指标化合物的分子量与直径覆盖了大多数有机污染物的范围,用此法可减少活性炭应用测试的炭型。在活性炭精选和吸附工艺应用研究中,用微型炭柱进行穿透实验可弥补缩小式传统型、小型炭柱的不足。相对于国外现用微型柱的实验方法,文中介绍的微型柱快速穿透(MCRB)方法的设备要求较低,操作简单,可以在国内大多数实验室中进行;通过对多种污染物质的实验结果,建立了MCRB方法的可信性和适用性。这两种新方法完善了活性炭水处理研究的实验体系,可降低其应用于水与污水处理的成本,有利于中国的环境保护。 展开更多
关键词 选炭 吸附容量 指标化合物 容量利用率 微型柱 快速穿透
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吐哈盆地台北凹陷侏罗系煤系源岩地球化学分类及意义 被引量:12
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作者 王志勇 孟仟祥 +3 位作者 王作栋 王晓华 杜宏宇 吕江陵 《沉积学报》 CAS CSCD 北大核心 2010年第6期1238-1243,共6页
烃源岩的沉积环境、母源输入与有机质性质有着密切联系,吐哈盆地台北凹陷不同层系、不同地区侏罗系煤系烃源岩由于其沉积环境、母源输入的不同,导致其地球化学指标差异;通过对源岩地球化学指标相关性分析表明,姥植比(Pr/Ph)是反映源岩... 烃源岩的沉积环境、母源输入与有机质性质有着密切联系,吐哈盆地台北凹陷不同层系、不同地区侏罗系煤系烃源岩由于其沉积环境、母源输入的不同,导致其地球化学指标差异;通过对源岩地球化学指标相关性分析表明,姥植比(Pr/Ph)是反映源岩沉积氧化还原环境和水体盐度的重要指标;C29ααα20R在C27~C29规则甾烷ααα20R中的相对含量也是反映沉积水体盐度的重要指标。同时发现源岩类型划分的主控指标是族组成中芳烃、沥青质组分含量及饱芳比、非沥比等四项指标,姥植比、伽马蜡烷指数为源岩类型划分的次控指标,据此将台北凹陷侏罗系煤系烃源岩划分为三类。 展开更多
关键词 吐哈盆地 煤系源岩 生物标志化合物指标 源岩类型
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Allium sativum Flavor Compounds as an Indicator for Garlic Identity and Quality Determination 被引量:1
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作者 Ruta Galoburda Karina Bodniece Thierry Talou 《Journal of Food Science and Engineering》 2013年第5期226-234,共9页
The objective of the study was to research the aroma profile of volatile compounds in garlic subspecies originating from Latvia, and compare them with the aroma composition of garlic grown in the region of Midi-Pyrene... The objective of the study was to research the aroma profile of volatile compounds in garlic subspecies originating from Latvia, and compare them with the aroma composition of garlic grown in the region of Midi-Pyrenees (France). It was established that hard-neck garlic tends to contain more diallyl disulfide (DADS), the main decomposition product of allicin. Compared to the hard-neck subspecies, the content of allyl mercaptan, one of the major compounds producing the strong odor detectable after ingestion of garlic, was significantly lower in the soft-neck garlic clones. The amount of cyclic compound 3-vinyl-1,2-dithiin differed considerably with higher contents in the soft-neck subspecies. The results also demonstrate the soft-neck garlic as a more suitable subspecies for long-term storage. In general, the results show no significant difference in the content of DADS and the total content of other flavor compounds between hard-neck and soft-neck garlic grown in the region of Midi-Pyrenees and Latvia. However, comparing garlic subspecies originating from France and Latvia by the content of allyl mercaptan, 1,2-dithiolane and 3-vinyl-1,2-dithiin, a considerable proportional difference of these volatiles was determined. Also, a significant difference was established in the content of DADS between the white garlic variety "Blanc de Lomagne" (France, region of Midi-Pyrenees) and white garlic grown in other countries. The results of this study suggest the suitability of solid phase microextraction (SPME) and gas chromatography (GC) methods for quality control of garlic originating from France. 展开更多
关键词 Allium sativum diallyl disulfide FLAVOR GARLIC IDENTITY
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Sonication for advanced drinking water treatment 被引量:1
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作者 张光明 魏希柱 +2 位作者 李相昆 张杰 豆子波 《Journal of Harbin Institute of Technology(New Series)》 EI CAS 2009年第1期16-20,共5页
This paper investigated the feasibility of sonication as an advanced treatment method for drinking water production and used comprehensive indexes of water quality to examine its efficiency. Results show that sonicati... This paper investigated the feasibility of sonication as an advanced treatment method for drinking water production and used comprehensive indexes of water quality to examine its efficiency. Results show that sonication significantly reduces the toxicity of water. Sonication with 5 W/L at 90 kHz lasting for 30 rain decreases the water SUVA and the disinfection byproduct formation potential (DBPFP) by 38.7% and 27. 2% respectively. Sonication also decreases the UV254 by more than 50% through destroying unsaturated chemical bonds. Higher sound intensity and higher frequency benefit the reduction of TOC and UV254. Besides, sonication significantly increases the affinity of organics with granular activated carbon ( GAC ) , and thus the hybrid sonication-GAC method reduces the water TOC, COD, UV254, and DBPFP by 78.3%, 69.4%, 75.7%, and 70.0% respectively. Therefore, sonication and the hybrid sonication-GAC metbod are proposed as advanced treatment methods for drinking water. 展开更多
关键词 sonieation drinking water advanced treatment DBPFP
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Physicochemical Parameters for Biological and Synthetic Surfactants Used as Detergents 被引量:1
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作者 Patricia C. Bernardes Emiliane A. Aratujo Marcia C. T. R. Vidigal Nelio J. Andrade Luis A. Minim Valeria P. R. Minim 《Journal of Food Science and Engineering》 2012年第7期359-366,共8页
Biological and synthetic surfactants were compared in terms of their ability to reduce interfacial tension, change the thermodynamic characteristics of a pre-conditioned surface, and to modify the rheological properti... Biological and synthetic surfactants were compared in terms of their ability to reduce interfacial tension, change the thermodynamic characteristics of a pre-conditioned surface, and to modify the rheological properties of their respective formulations at two different temperatures. Both classes of suffactants were able to reduce the inteffacial tension of their formulations to a similar level. However, the biosurfactants were more effective than the synthetics surfactants. Biosurfactants also altered the surface properties of stainless steel, rendering it hydrophilic. Microbial adhesion to stainless steel conditioned with biosurfactants was found to be thermodynamically unfavorable for all microbial strains tested. A linear relationship between shear stress and shear rate was obtained across a range of experimental conditions for all surfactant mixtures, indicating that all formulations behaved as Newtonian fluids. 展开更多
关键词 SURFACTANTS biosurfactants interfacial tension microbial adhesion stainless steel.
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