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SPME/GC-MS法分析柠檬草挥发气体成分 被引量:7
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作者 邓小勇 谷茂 +1 位作者 许伯球 谢小玉 《深圳职业技术学院学报》 CAS 2008年第2期36-40,共5页
利用固相微萃取SPME/GC-MS技术分析了柠檬草的挥发气体成分。结果表明:柠檬草中共鉴定出25种主要挥发性化合物,以碳氢化合物和醛类物为主,包括β-月桂稀(34.34%)、石竹烯(0.493%)、莰烯(0.646%)、D-柠檬烯(0.126%)、1R-α-蒎烯(0.73%)... 利用固相微萃取SPME/GC-MS技术分析了柠檬草的挥发气体成分。结果表明:柠檬草中共鉴定出25种主要挥发性化合物,以碳氢化合物和醛类物为主,包括β-月桂稀(34.34%)、石竹烯(0.493%)、莰烯(0.646%)、D-柠檬烯(0.126%)、1R-α-蒎烯(0.73%)、柠檬醛(26.5%)、3,7二甲基-2,6-辛二稀醛(26.63%)等。经过精制的柠檬草精油含有酮和烃类化合物,主要有:2-十一酮(0.606%)、2-甲基-5-(1-甲基乙基)环己酮(1.83%)、(1S)-6,6-二甲基-二乙基二环-[3,1,1]-庚烷,(0.34%)、1,4-双亚甲基-环已烷,(0.176%),β-丙基-环已基(0.1667%)。 展开更多
关键词 柠檬草 固相微萃取(SPME) 气相色谱/质谱联用(GC—MS) 挥发气体成分
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应用顶空固相微萃取-气相色谱/质谱法分析杧果叶片挥发性物质成分 被引量:1
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作者 黄志萍 陈发兴 《福建果树》 2011年第1期23-27,共5页
应用顶空固相微萃取法(HS-SPME)及气相色谱-质谱(GC/MSD)法进行本地种杧果叶片成分分析。结果共检测出68种挥发性成分,鉴定出其中的50个成分,含量占总挥发性组分的98.56%,其中主要成分为(n)-杜松萜烯(18.87%)、2,2,4,8-四甲基三环[5.3.1... 应用顶空固相微萃取法(HS-SPME)及气相色谱-质谱(GC/MSD)法进行本地种杧果叶片成分分析。结果共检测出68种挥发性成分,鉴定出其中的50个成分,含量占总挥发性组分的98.56%,其中主要成分为(n)-杜松萜烯(18.87%)、2,2,4,8-四甲基三环[5.3.1.0]8-十一烯(17.78%)、2,4,6-三甲基苯酚(12.94%)、,c-衣兰油烯(10.09%)、偄-杜松萜烯(-)-(8.14%)、香附子烯(5.64%)、(+)-香橙烯(4.17%)等。分析结果从对本地种杧果叶片挥发性成分功能角度肯定其作为行道树的价值功效。 展开更多
关键词 固相微萃取 气相色谱/质谱 本地种杧果 挥发气体成分
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Chemical Compositions of Volatile Oil from Fruiting Body of Armillaria luteo-virens 被引量:30
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作者 周劲松 熊辉岩 +2 位作者 杨春江 焦迎春 盛海彦 《Agricultural Science & Technology》 CAS 2008年第2期90-92,共3页
The chemical compositions of volatile oil from fruiting body of Armillaria luteo-virens in Qinghai Province were firstly analyzed with GC-MS and its relevant compositions were detected by calculating chromatographic p... The chemical compositions of volatile oil from fruiting body of Armillaria luteo-virens in Qinghai Province were firstly analyzed with GC-MS and its relevant compositions were detected by calculating chromatographic peak area with normalized method. 21 peaks were separated and 13 compositions were identified which were mainly unsaturated fatty acids, taking 97.1% of the total volatile oil. 展开更多
关键词 Armillaria luteo-rirens Volatile oil Chemical compositions GC-MS
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Influence of the post-fermentation by four Aspergillus strains on the aroma of pu-erh tea 被引量:5
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作者 叶静 王文光 +4 位作者 李军 郭晓宇 赵明波 姜勇 屠鹏飞 《Journal of Chinese Pharmaceutical Sciences》 CAS CSCD 2016年第4期284-290,共7页
Aroma is one of the most important factors for the flavor, taste, and quality of pu-erh tea, and the post-fermentation process has an important influence on the aroma of pu-erh tea. In the present study, the influence... Aroma is one of the most important factors for the flavor, taste, and quality of pu-erh tea, and the post-fermentation process has an important influence on the aroma of pu-erh tea. In the present study, the influence of fungi fermentation on the flavor of pu-erh tea was investigated and compared. Volatile compounds from pu-erh tea fermented by four Aspergillus strains, including A. niger, A. oryzae, /1. awamori, and A. glaueus, were extracted and analyzed using ultrasound-assisted extraction-dispersive liquid-liquid microextraction-gas chromatography-mass spectrometry (UAE-DLLME-GC-MS), and a total of 63 volatile compounds were identified. In comparison with the sun-dried green tea, fermented pu-erh tea contained high levels of methoxyphenolic compounds, such as 1,2,3-trimethoxybenzene, which was the most abundant one. Our results confirmed that the characteristic methoxyphenolic compounds were produced by the activity of Aspergillus during the post-fermentation process, and A. niger and A. awamori were the most important strains for the formation of aroma quality of pu-erh tea. 展开更多
关键词 Pu-erh tea ASPERGILLUS Solid-state fermentation Volatile compounds GC-MS
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