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高透光率聚醚砜树脂放料工艺研究
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作者 张登 高红军 +5 位作者 孙学科 王道波 陈锐斌 叶国滨 曹民 黄险波 《科学大众(科技创新)》 2018年第12期27-29,共3页
聚醚砜树脂的放料工艺对树脂透光率有显著影响。文章利用扫描电子显微镜、核磁共振氢谱和电感耦合等离子体光谱仪等系统研究了聚合结束后聚合溶液放料过程所需沉淀浴的温度和浓度等工艺条件对树脂粉末表面结构、溶剂和副产物残留等的影... 聚醚砜树脂的放料工艺对树脂透光率有显著影响。文章利用扫描电子显微镜、核磁共振氢谱和电感耦合等离子体光谱仪等系统研究了聚合结束后聚合溶液放料过程所需沉淀浴的温度和浓度等工艺条件对树脂粉末表面结构、溶剂和副产物残留等的影响,并利用透光率雾度测定仪评估了树脂的透光率。通过研究确定了高透光率、低溶剂残留的PES树脂的合适放料工艺,对PES的工业化生产具有较好的指导意义。 展开更多
关键词 聚醚砜 透光率 放料工艺
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Tailoring microstructure and mechanical properties of aluminum matrix composites reinforced with novel Al/CuFe multi-layered core-shell particles
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作者 Rashid ALI Fahad ALI +6 位作者 Aqib ZAHOOR Rub Nawaz SHAHID Naeem ul Haq TARIQ Zafar IQBAL Adnan Qayyum BUTT Saad ULLAH Hasan Bin AWAIS 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2022年第6期1822-1833,共12页
Aluminum matrix composites(AMCs), reinforced with novel pre-synthesized Al/Cu Fe multi-layered coreshell particles, were fabricated by different consolidation techniques to investigate their effect on microstructure a... Aluminum matrix composites(AMCs), reinforced with novel pre-synthesized Al/Cu Fe multi-layered coreshell particles, were fabricated by different consolidation techniques to investigate their effect on microstructure and mechanical properties. To synthesize multi-layered Al/Cu Fe core-shell particles, Cu and Fe layers were deposited on Al powder particles by galvanic replacement and electroless plating method, respectively. The core-shell powder and sintered compacts were characterized by using X-ray diffraction(XRD), scanning electron microscopy(SEM) equipped with energy dispersive spectroscopy(EDX), pycnometer, microhardness and compression tests. The results revealed that a higher extent of interfacial reactions, due to the transformation of the deposited layer into intermetallic phases in spark plasma sintered composite, resulted in high relative density(99.26%), microhardness(165 HV0.3) and strength(572 MPa). Further, the presence of un-transformed Cu in the shell structure of hot-pressed composite resulted in the highest fracture strain(20.4%). The obtained results provide stronger implications for tailoring the microstructure of AMCs through selecting appropriate sintering paths to control mechanical properties. 展开更多
关键词 core-shell reinforcement aluminum matrix composites electroless plating sintering techniques spark plasma sintering interfacial reaction
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