Crystals of CdSxSe1-x alloys have been grown from the vapour phase. Some of the physical properties, such as lattice parameters, crystal structure and x-rays data of CdSxSe1-x alloys were determined using x-ray diffra...Crystals of CdSxSe1-x alloys have been grown from the vapour phase. Some of the physical properties, such as lattice parameters, crystal structure and x-rays data of CdSxSe1-x alloys were determined using x-ray diffractometry. X-ray diffractometry has shown that CdS-CdSe mixed crystals had the wurtzite structure for all compositions between CdS and CdSe. The lattice parameters (both a and c) were found to show a linear dependence with composition. The dependence of the lattice parameters of a and c on composition can be expressed as: a(x) = 4.165 + 0.16x; c(x) = 6.713 + 0.27x. The variation of band gap with composition was determined for these samples from optical absorption measurements, which showed that the band gap varied smoothly and monotonically, but not linearly over the composition range typical results were found between 2.42-1.74 eV at room temperature.展开更多
Objective: The aim of our study was to investigate the impact of abdominal hypo-fraction irradiation on liver damage in rats so as to provide a reference for its clinical application. Methods: A total of 100 Wistar ra...Objective: The aim of our study was to investigate the impact of abdominal hypo-fraction irradiation on liver damage in rats so as to provide a reference for its clinical application. Methods: A total of 100 Wistar rats were equally randomized to five groups as control, 4 Gy, 6 Gy, 8 Gy and 12 Gy group, and the corresponding fractionated doses were offered. Liver functions were examined at the 2nd, 4th, 6th, 8th and 10th week after irradiation. Morphological changes were observed by HE staining. Expressions of Bcl-2 and Bax were examined by immunohistochemical technique. Results: In all irradiation groups, hepatocellular swell, degeneration, necrosis and even hepatic fibrosis could be seen. The differences of the liver coefficient, Glutamyl pyruvic transaminase (GPT), Glutamyl oxaloacetic transaminase (GOT) were significant among the groups and different time points (F = 11.833-781.972, F = 20.857-264.692, P < 0.001). Expressions of Bcl-2 and Bax were significantly different between each group (F = 211.607, 116.577; P < 0. 001), and between each time point (F = 54.083, 68.749; P < 0. 001). Conclusion: Compare with conventional fraction, abdominal hypo-fraction irradiation may cause radiation damage to rat liver, being dose-and-time dependent. Up-regulation of activating apoptosis protein Bax and down-regulation of inhibiting apoptosis protein Bcl-2 may involve in the process.展开更多
Voids are one of the major defects in ball grid array (BGA) solder joints due to a large amount of outgassing flux that gets entrapped during reflow. X-ray nondestructive machines are used to make voids visible ...Voids are one of the major defects in ball grid array (BGA) solder joints due to a large amount of outgassing flux that gets entrapped during reflow. X-ray nondestructive machines are used to make voids visible as lighter areas inside the solder joints in X-ray images for detection However, it has always been difficult to analyze this problem automatically because of some challenges such as noise, inconsistent lighting and void-like artifacts. This study realized accurate extraction and automatic a-nalysis of void defects in solder joints by adopting a technical proposal, in which Otsu algorithm was used to segment solder balls and void defects were extracted through opening and closing operations and top-hat transformation in mathematical mor-phology. Experimental results show that the technical proposal mentioned here has good robustness and can be applied in the detection of voids in BGA solder joints.展开更多
Thermogravimetric analysis and electrical resistivity were used to determine the hydration process of cement paste with rice husk ash(RHA)(0−15%)and water-cement ratio of 0.4 in this work.X-ray diffraction(XRD)method ...Thermogravimetric analysis and electrical resistivity were used to determine the hydration process of cement paste with rice husk ash(RHA)(0−15%)and water-cement ratio of 0.4 in this work.X-ray diffraction(XRD)method and scanning electron microscopy(SEM)were used to survey crystal composition and microstructures of specimens cured for 3 h,1 d,7 d and 28 d.Finally,electrical parameters(electrical resistance and AC impedance spectroscopy)of steel bars reinforced cement paste were investigated to study the effect of RHA on the corrosion resistance.Results showed that RHA could affect the cement hydration by hydration promotion and pozzolanic effect.The evaluation function for electrical resistivity and curing ages fitted well with linear increasing function.The addition of RHA higher than 5%demonstrated a decreasing role in the electrical resistivity of cement paste at earlier curing ages(3−7 d).Meanwhile,when at later curing ages(7−28 d)the result was the opposite.Moreover,RHA demonstrated positive effects on corrosion resistance of steel bars in cement paste.展开更多
The coefficient and dynamics of water diffusion in adhesive-graphite joints were calculated in-situ with energy dispersive X-ray (EDX) analysis, a method that is significantly simpler than elemental analysis. Water di...The coefficient and dynamics of water diffusion in adhesive-graphite joints were calculated in-situ with energy dispersive X-ray (EDX) analysis, a method that is significantly simpler than elemental analysis. Water diffusion coefficient and dynamics of adhesive-graphite joints treated by different surface treatment methods were also investigated. Calculation results indicated that the water diffusion rate in adhesive-graphite joints treated by sandpaper was higher than that treated by chemical oxidation or by silane couple agent. Also the durability of graphite joints treated by coupling agent is superior to that treated by chemical oxidation or sandpaper burnishing.展开更多
文摘Crystals of CdSxSe1-x alloys have been grown from the vapour phase. Some of the physical properties, such as lattice parameters, crystal structure and x-rays data of CdSxSe1-x alloys were determined using x-ray diffractometry. X-ray diffractometry has shown that CdS-CdSe mixed crystals had the wurtzite structure for all compositions between CdS and CdSe. The lattice parameters (both a and c) were found to show a linear dependence with composition. The dependence of the lattice parameters of a and c on composition can be expressed as: a(x) = 4.165 + 0.16x; c(x) = 6.713 + 0.27x. The variation of band gap with composition was determined for these samples from optical absorption measurements, which showed that the band gap varied smoothly and monotonically, but not linearly over the composition range typical results were found between 2.42-1.74 eV at room temperature.
文摘Objective: The aim of our study was to investigate the impact of abdominal hypo-fraction irradiation on liver damage in rats so as to provide a reference for its clinical application. Methods: A total of 100 Wistar rats were equally randomized to five groups as control, 4 Gy, 6 Gy, 8 Gy and 12 Gy group, and the corresponding fractionated doses were offered. Liver functions were examined at the 2nd, 4th, 6th, 8th and 10th week after irradiation. Morphological changes were observed by HE staining. Expressions of Bcl-2 and Bax were examined by immunohistochemical technique. Results: In all irradiation groups, hepatocellular swell, degeneration, necrosis and even hepatic fibrosis could be seen. The differences of the liver coefficient, Glutamyl pyruvic transaminase (GPT), Glutamyl oxaloacetic transaminase (GOT) were significant among the groups and different time points (F = 11.833-781.972, F = 20.857-264.692, P < 0.001). Expressions of Bcl-2 and Bax were significantly different between each group (F = 211.607, 116.577; P < 0. 001), and between each time point (F = 54.083, 68.749; P < 0. 001). Conclusion: Compare with conventional fraction, abdominal hypo-fraction irradiation may cause radiation damage to rat liver, being dose-and-time dependent. Up-regulation of activating apoptosis protein Bax and down-regulation of inhibiting apoptosis protein Bcl-2 may involve in the process.
基金National Science and Technology Major Project of the Ministry of Science And Technology of China(No.2013YQ240803)Shanxi Programs for Science and Technology Development(Nos.20140321010-02,201603D121040-1)Scientific and Technological Innovation Programs of Higher Education Institutions of Shanxi Province(No.2013063)
文摘Voids are one of the major defects in ball grid array (BGA) solder joints due to a large amount of outgassing flux that gets entrapped during reflow. X-ray nondestructive machines are used to make voids visible as lighter areas inside the solder joints in X-ray images for detection However, it has always been difficult to analyze this problem automatically because of some challenges such as noise, inconsistent lighting and void-like artifacts. This study realized accurate extraction and automatic a-nalysis of void defects in solder joints by adopting a technical proposal, in which Otsu algorithm was used to segment solder balls and void defects were extracted through opening and closing operations and top-hat transformation in mathematical mor-phology. Experimental results show that the technical proposal mentioned here has good robustness and can be applied in the detection of voids in BGA solder joints.
基金Projects(51808300,51778302)supported by the National Natural Science Foundation of ChinaProject supported by the K.C.Wong Magna Fund in Ningbo University,China。
文摘Thermogravimetric analysis and electrical resistivity were used to determine the hydration process of cement paste with rice husk ash(RHA)(0−15%)and water-cement ratio of 0.4 in this work.X-ray diffraction(XRD)method and scanning electron microscopy(SEM)were used to survey crystal composition and microstructures of specimens cured for 3 h,1 d,7 d and 28 d.Finally,electrical parameters(electrical resistance and AC impedance spectroscopy)of steel bars reinforced cement paste were investigated to study the effect of RHA on the corrosion resistance.Results showed that RHA could affect the cement hydration by hydration promotion and pozzolanic effect.The evaluation function for electrical resistivity and curing ages fitted well with linear increasing function.The addition of RHA higher than 5%demonstrated a decreasing role in the electrical resistivity of cement paste at earlier curing ages(3−7 d).Meanwhile,when at later curing ages(7−28 d)the result was the opposite.Moreover,RHA demonstrated positive effects on corrosion resistance of steel bars in cement paste.
文摘The coefficient and dynamics of water diffusion in adhesive-graphite joints were calculated in-situ with energy dispersive X-ray (EDX) analysis, a method that is significantly simpler than elemental analysis. Water diffusion coefficient and dynamics of adhesive-graphite joints treated by different surface treatment methods were also investigated. Calculation results indicated that the water diffusion rate in adhesive-graphite joints treated by sandpaper was higher than that treated by chemical oxidation or by silane couple agent. Also the durability of graphite joints treated by coupling agent is superior to that treated by chemical oxidation or sandpaper burnishing.