The microstructure and mechanical properties of alloy 617 B in the process of 5000 h aging at 750 °C were systematically investigated by means of SEM, TEM and mechanical analysis. M23C6 particles were dispersed i...The microstructure and mechanical properties of alloy 617 B in the process of 5000 h aging at 750 °C were systematically investigated by means of SEM, TEM and mechanical analysis. M23C6 particles were dispersed inside grains and distributed discontinuously along grain boundaries and γ′ phases were situated at intragranular sites in the process of aging. The size of precipitates increased with increasing aging time. Inter- and intra-granular carbide and γ′ phase particles inside grains resulted in the precipitation strengthening of this aged alloy, enhancing the strength and hardness. The aged alloy possessed good stabilities of hardness and strength during aging. An obvious decrease of the toughness of this aged alloy was due to γ′ phase particles limiting plastic deformation to the area nearby grain boundaries, resulting in the occurrence of crack along grain boundaries. Additionally, the intergranular cracks apparently led to a decrease in the toughness for this aged alloy due to carbide particles at grain boundaries. The toughness of this aged alloy was fairly stable possibly due to the unchanged distribution of the precipitates during aging.展开更多
The ultra high strength SiC particles (SiCp) reinforced Al-10%Zn-3.6%Mg-1.8%Cu-0.36%Zr-0.15% Ni composite was prepared by spray co-deposition. Microstructures of the extruded and different heat-treated bars were ana...The ultra high strength SiC particles (SiCp) reinforced Al-10%Zn-3.6%Mg-1.8%Cu-0.36%Zr-0.15% Ni composite was prepared by spray co-deposition. Microstructures of the extruded and different heat-treated bars were analyzed by transmission electron microscopy (TEM) and energy dispersive spectrometry (EDS). Grain size of the composites prepared by two-stage solution is smaller than that by single-stage solution. After single-stage solution aging treatment, fine precipitates of both η and AlZnMgCu-rich phase can be found both intragranularly and intergranularly. While after the two-stage solution, an amorphous Si-Cu-Al-O (5 nm) layer appears at the interface. The addition of Ni and Zr modified the influence of the two-stage solution and inhibited the growth of the 7090/SiCp composite grain size. Heat treatments can significantly improve the fracture toughness of the composite. The fracture toughness first decreases then increases with the elongation of the aging time.展开更多
A retrogression process was applied to AA7075alloy at180,240and320°C for1,30,50,70,90and120min.After the retrogression,aging treatment was reapplied with T6conditions(120°C,24h).The mechanical properties of ...A retrogression process was applied to AA7075alloy at180,240and320°C for1,30,50,70,90and120min.After the retrogression,aging treatment was reapplied with T6conditions(120°C,24h).The mechanical properties of aged samples were determined by V-Charpy and hardness tests and also,physical properties of samples were determined by electrical conductivity tests.Moreover,microstructural properties were characterized by light microscope and transmission electron microscope.The results show that the effects of the temperature and the duration of the retrogression and reagent on the impact toughness and hardness are related to the precipitates at the grain boundary.展开更多
The microstructure,mechanical properties and stress corrosion cracking(SCC)of 7136 aluminum alloy under T 6,T 79 and T 74 aging treatments were studied and the effects of microstructure on the mechanical properties an...The microstructure,mechanical properties and stress corrosion cracking(SCC)of 7136 aluminum alloy under T 6,T 79 and T 74 aging treatments were studied and the effects of microstructure on the mechanical properties and SCC were discussed.The results show that the ultimate tensile strength and yield strength of the aging 7136 alloys follow this sequence from high to low:T 6>T 79>pre-aging>T 74.For 7136 Al alloy after T 6 aging,the average diameter of the precipitates was(5.7±1.7)nm,and the diameter of 60.7%(number fraction)precipitates was 2−6 nm,leading to a good precipitation strengthening.The K_(IC)of T 74-aging alloy is 38.2 MPa·m^(1/2),which is 26.1%more than that of T 6-aging alloy and 17.5%more than that of T 79-aging alloy.The improved fracture toughness in T 74-aging alloy is mainly due to the reduction of the strength difference between intragranular and grain boundary.The SCC resistance of the aging 7136 alloys follows this sequence from high to low:T 79>T 74>T 6.After T 79 aging,the discontinuous grain boundary precipitates and narrow precipitate free zones were obtained in 7136 alloy,which was beneficial to SCC resistance.展开更多
针对航空发动机复合材料出口导向叶片RTM(Resin Transfer Molding,树脂传递模塑)成型工艺,开展了高韧性短时效树脂基体的工艺特性及低渗透率铺层结构预制体的渗透特性研究,并结合PAM-RTM软件对其RTM成型工艺方案进行了研究,获得了适用...针对航空发动机复合材料出口导向叶片RTM(Resin Transfer Molding,树脂传递模塑)成型工艺,开展了高韧性短时效树脂基体的工艺特性及低渗透率铺层结构预制体的渗透特性研究,并结合PAM-RTM软件对其RTM成型工艺方案进行了研究,获得了适用于高韧性短时效树脂/低渗透率铺层结构复合材料出口导向叶片的快速RTM成型工艺方法。展开更多
基金Project(2012AA050501)supported by the National High-tech Research and Development Program of ChinaProject(NY20110102)supported by the National Energy Applied Technology and Engineering Demonstration Program,China+1 种基金Project(2012CB724401)supported by the National Basic Research Program of ChinaProject(003)supported by CSEE Youth Science & Technology Innovation,China
文摘The microstructure and mechanical properties of alloy 617 B in the process of 5000 h aging at 750 °C were systematically investigated by means of SEM, TEM and mechanical analysis. M23C6 particles were dispersed inside grains and distributed discontinuously along grain boundaries and γ′ phases were situated at intragranular sites in the process of aging. The size of precipitates increased with increasing aging time. Inter- and intra-granular carbide and γ′ phase particles inside grains resulted in the precipitation strengthening of this aged alloy, enhancing the strength and hardness. The aged alloy possessed good stabilities of hardness and strength during aging. An obvious decrease of the toughness of this aged alloy was due to γ′ phase particles limiting plastic deformation to the area nearby grain boundaries, resulting in the occurrence of crack along grain boundaries. Additionally, the intergranular cracks apparently led to a decrease in the toughness for this aged alloy due to carbide particles at grain boundaries. The toughness of this aged alloy was fairly stable possibly due to the unchanged distribution of the precipitates during aging.
基金Project (02Gky2004) supported by Hunan Provincial Science and Technology Department, China
文摘The ultra high strength SiC particles (SiCp) reinforced Al-10%Zn-3.6%Mg-1.8%Cu-0.36%Zr-0.15% Ni composite was prepared by spray co-deposition. Microstructures of the extruded and different heat-treated bars were analyzed by transmission electron microscopy (TEM) and energy dispersive spectrometry (EDS). Grain size of the composites prepared by two-stage solution is smaller than that by single-stage solution. After single-stage solution aging treatment, fine precipitates of both η and AlZnMgCu-rich phase can be found both intragranularly and intergranularly. While after the two-stage solution, an amorphous Si-Cu-Al-O (5 nm) layer appears at the interface. The addition of Ni and Zr modified the influence of the two-stage solution and inhibited the growth of the 7090/SiCp composite grain size. Heat treatments can significantly improve the fracture toughness of the composite. The fracture toughness first decreases then increases with the elongation of the aging time.
基金supported by Yildiz Technical University Scientific Research Project Unit under Contract No:2016-07-02-DOP02
文摘A retrogression process was applied to AA7075alloy at180,240and320°C for1,30,50,70,90and120min.After the retrogression,aging treatment was reapplied with T6conditions(120°C,24h).The mechanical properties of aged samples were determined by V-Charpy and hardness tests and also,physical properties of samples were determined by electrical conductivity tests.Moreover,microstructural properties were characterized by light microscope and transmission electron microscope.The results show that the effects of the temperature and the duration of the retrogression and reagent on the impact toughness and hardness are related to the precipitates at the grain boundary.
基金Project(2017GK2261)supported by the Science and Technology Program of Hunan Province,ChinaProject(41423040204)supported by National Key Laboratory of Light Weight and High Strength Structural Materials Equipment Pre-research Laboratory Foundation,China。
文摘The microstructure,mechanical properties and stress corrosion cracking(SCC)of 7136 aluminum alloy under T 6,T 79 and T 74 aging treatments were studied and the effects of microstructure on the mechanical properties and SCC were discussed.The results show that the ultimate tensile strength and yield strength of the aging 7136 alloys follow this sequence from high to low:T 6>T 79>pre-aging>T 74.For 7136 Al alloy after T 6 aging,the average diameter of the precipitates was(5.7±1.7)nm,and the diameter of 60.7%(number fraction)precipitates was 2−6 nm,leading to a good precipitation strengthening.The K_(IC)of T 74-aging alloy is 38.2 MPa·m^(1/2),which is 26.1%more than that of T 6-aging alloy and 17.5%more than that of T 79-aging alloy.The improved fracture toughness in T 74-aging alloy is mainly due to the reduction of the strength difference between intragranular and grain boundary.The SCC resistance of the aging 7136 alloys follows this sequence from high to low:T 79>T 74>T 6.After T 79 aging,the discontinuous grain boundary precipitates and narrow precipitate free zones were obtained in 7136 alloy,which was beneficial to SCC resistance.
文摘针对航空发动机复合材料出口导向叶片RTM(Resin Transfer Molding,树脂传递模塑)成型工艺,开展了高韧性短时效树脂基体的工艺特性及低渗透率铺层结构预制体的渗透特性研究,并结合PAM-RTM软件对其RTM成型工艺方案进行了研究,获得了适用于高韧性短时效树脂/低渗透率铺层结构复合材料出口导向叶片的快速RTM成型工艺方法。