This paper describes an effective method for determining ciprofloxacin lactate. An excess of sodium tetraphenylboron was added to precipitate ciprofloxacin lactate in HAc-NaAc buffer solution (pH=4.0). After filtering...This paper describes an effective method for determining ciprofloxacin lactate. An excess of sodium tetraphenylboron was added to precipitate ciprofloxacin lactate in HAc-NaAc buffer solution (pH=4.0). After filtering off the precipitate, the excessive sodium tetraphenylboron in the filtrate was titrated with cetyltrimethylammonium bromide standard solution, with bromophenol blue as indicator. The method is simple and rapid, it has been applied to the determination of ciprofloxacin lactate raw material with satisfactory results. The recovery was between 99.66% and 100.2%, the relative error was less than ±0.40%. Experiments showed that the method gave the same results as the approach using nonaqueous titration (ChP).展开更多
To understand the formation mechanism of blue stragglers in open clusters, we conducted a photometric analysis for a blue straggler eclipsing binary in the old open cluster NGC 2141. By using the least square fitting ...To understand the formation mechanism of blue stragglers in open clusters, we conducted a photometric analysis for a blue straggler eclipsing binary in the old open cluster NGC 2141. By using the least square fitting of times of minima, we derived the ephemeris and redetermined the orbital period of this system to be 0.6227 d. We have also done a photometric analysis for light curve with the Wilson-Devinney Code （2003）. The photometric solutions reveal a semi-detached binary with the second- ary component filling its Roche lobe. The photometric mass ratio MJMI （secondary/primary） was determined to be 0.190_＋0.002 and the ratio of V-band luminosity L2/LI（V） is about 0.033_＋0.001, which indicates the secondary component is overluminous. Thus, this blue straggler likely results from a substantial mass exchange between these two components.展开更多
Hyperspectral remote sensing makes it possible to non-destructively monitor leaf chlorophyll content （LCC）. This study characterized the geometric patterns of the first derivative reflectance spectra in the red edge...Hyperspectral remote sensing makes it possible to non-destructively monitor leaf chlorophyll content （LCC）. This study characterized the geometric patterns of the first derivative reflectance spectra in the red edge region of rapeseed （Brassica napus L.） and wheat （Triticum aestivum L.） crops. The ratio of the red edge area less than 718 nm to the entire red edge area was negatively correlated with LCC. This finding allowed the construction of a new red edge param- eter, defined as red edge symmetry （RES）. Compared to the commonly used red edge parameters （red edge position, red edge amplitude, and red edge area）, RES was a better predictor of LCC. Furthermore, RES was easily calculated using the reflectance of red edge boundary wavebands at 675 and 755 nm （R675 and R755） and reflectance of red edge center wavelength at 718 nm （R718）, with the equation RES = （R71s - R675）/（R755 - R675）. In addition, RES was simulated effectively with wide wavebands from the airborne hyperspectral sensor AVIRIS and satellite hyperspectral sensor Hyperion. The close relationships between the simulated RES and LCC indicated a high feasibility of estimating LCC with simulated RES from AVIRIS and Hyperion data. This made RES readily applicable to common airborne and satellite hyperspectral data derived from AVIRIS and Hyperion sources, as well as ground-based spectral reflectance data.展开更多
文摘This paper describes an effective method for determining ciprofloxacin lactate. An excess of sodium tetraphenylboron was added to precipitate ciprofloxacin lactate in HAc-NaAc buffer solution (pH=4.0). After filtering off the precipitate, the excessive sodium tetraphenylboron in the filtrate was titrated with cetyltrimethylammonium bromide standard solution, with bromophenol blue as indicator. The method is simple and rapid, it has been applied to the determination of ciprofloxacin lactate raw material with satisfactory results. The recovery was between 99.66% and 100.2%, the relative error was less than ±0.40%. Experiments showed that the method gave the same results as the approach using nonaqueous titration (ChP).
基金supported by the National Natural Science Foundation of China (Grant Nos. 11033008 and 11103072)the Chinese Academy of Sciences (Grant No. KJCX2-YW-T24)the National Basic Research Program of China (Grant No. 2009CB824800)
文摘To understand the formation mechanism of blue stragglers in open clusters, we conducted a photometric analysis for a blue straggler eclipsing binary in the old open cluster NGC 2141. By using the least square fitting of times of minima, we derived the ephemeris and redetermined the orbital period of this system to be 0.6227 d. We have also done a photometric analysis for light curve with the Wilson-Devinney Code （2003）. The photometric solutions reveal a semi-detached binary with the second- ary component filling its Roche lobe. The photometric mass ratio MJMI （secondary/primary） was determined to be 0.190_＋0.002 and the ratio of V-band luminosity L2/LI（V） is about 0.033_＋0.001, which indicates the secondary component is overluminous. Thus, this blue straggler likely results from a substantial mass exchange between these two components.
基金Supported by the Program for New Century Excellent Talents in University of China(No.NCET-08-0797)the National Natural Science Foundation of China(No.30871448)+1 种基金the Natural Science Foundation of Jiangsu Province,China(No.BK2008330)the Program for the Creative Scholars of Jiangsu Province,China(No.BK20081479)
文摘Hyperspectral remote sensing makes it possible to non-destructively monitor leaf chlorophyll content （LCC）. This study characterized the geometric patterns of the first derivative reflectance spectra in the red edge region of rapeseed （Brassica napus L.） and wheat （Triticum aestivum L.） crops. The ratio of the red edge area less than 718 nm to the entire red edge area was negatively correlated with LCC. This finding allowed the construction of a new red edge param- eter, defined as red edge symmetry （RES）. Compared to the commonly used red edge parameters （red edge position, red edge amplitude, and red edge area）, RES was a better predictor of LCC. Furthermore, RES was easily calculated using the reflectance of red edge boundary wavebands at 675 and 755 nm （R675 and R755） and reflectance of red edge center wavelength at 718 nm （R718）, with the equation RES = （R71s - R675）/（R755 - R675）. In addition, RES was simulated effectively with wide wavebands from the airborne hyperspectral sensor AVIRIS and satellite hyperspectral sensor Hyperion. The close relationships between the simulated RES and LCC indicated a high feasibility of estimating LCC with simulated RES from AVIRIS and Hyperion data. This made RES readily applicable to common airborne and satellite hyperspectral data derived from AVIRIS and Hyperion sources, as well as ground-based spectral reflectance data.
