基于降噪设计的陶粒微观结构调控的试验

采用发泡法,在陶粒制作工艺中添加碳酸氢铵发泡剂,增加热处理程序。通过宏观试验和微观表征,控制发泡剂用量、升温速率、养护时间来调节陶粒的孔径、显孔率以及孔的有序性等微观结构,实现陶粒孔结构的可控,从而优化陶粒的吸声性能。研究表明:发泡剂的添加量越多、升温速率越高、增加热处理程序之前养护时间越短,所制备的陶粒显孔率越大、孔径越细小、孔排列的结构越有序均匀。当发泡剂的添加量为2.0 wt%、升温速率为20℃/min、热处理之前零养护时,可制备出最高显孔隙率为32.67%,平均孔径为0.31μm,孔结构有序均匀排列的多孔陶粒,并有效改善多孔材料在低频范围吸声性能;整个控制机理下所制备的多孔陶粒筒压强度都大于2.0 MPa,满足规范和使用要求。

Study on Preparation of Ceramic Material and Its Properties

This paper introduces the classification, properties and application of porous ceramic materials, reviewed preparation of porous ceramics. Taking fly ash and red mud as the main raw material to generate porous ceramics, the paper study the influence of different proportions of raw materials, sintering temperature, porosity of porous ceramic sample rate, bending strength, and microstructure. The results show that, fly ash and red mud proportioning and sintering temperature are the main factors that influence the structure and properties of samples. The4#sample is a kind of high porosity and high strength quality of porous ceramics.