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夕阳无悔方显红
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作者 阿俊 《党的生活(贵州)》 1999年第9期43-,共1页
关键词 显红 夕阳
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人体显红莫大意
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作者 田香 《家庭中医药》 2004年第1期57-57,共1页
脸红:有高血压的人容易面色 通红,看上去肤色很好。有高热的人, 面呈红赤。如果是危重病人,原来面 色苍白,突然之间面色红润,可能是病情恶化之兆,应予重视。 手掌红:健康人的手掌呈粉红色,但如果过红,尤其大拇指根部和小指根部下面鼓起... 脸红:有高血压的人容易面色 通红,看上去肤色很好。有高热的人, 面呈红赤。如果是危重病人,原来面 色苍白,突然之间面色红润,可能是病情恶化之兆,应予重视。 手掌红:健康人的手掌呈粉红色,但如果过红,尤其大拇指根部和小指根部下面鼓起的地方发红。 展开更多
关键词 人体显红 高血压 手掌 肝硬化 慢性肝炎
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Tc-99m-RBC核素显像对胃肠道出血定位诊断的评价 被引量:4
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作者 陈曼 张燕燕 《北京医科大学学报》 CSCD 1995年第1期68-68,79,共2页
Tc-99m-RBC核素显像对胃肠道出血定位诊断的评价北京医科大学第三医院核医学科陈曼,张燕燕对胃肠道出血患者准确找到出血部位是治疗的前提,近年来,我科用Te-99m体内标记红细胞法进行显像以确定胃肠道出血部位(1)... Tc-99m-RBC核素显像对胃肠道出血定位诊断的评价北京医科大学第三医院核医学科陈曼,张燕燕对胃肠道出血患者准确找到出血部位是治疗的前提,近年来,我科用Te-99m体内标记红细胞法进行显像以确定胃肠道出血部位(1),使许多用常规方法不能发现出血部位... 展开更多
关键词 胃肠道出血 定位诊断 锝99M 细胞核素
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Infrared microthermometry of fluid inclusion in sphalerite:A case study of the Xinqiao deposit in the Middle-Lower Yangtze metallogenic belt
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作者 Yangyang Wang Yilin Xiao 《中国科学技术大学学报》 CAS CSCD 北大核心 2024年第5期10-21,I0006,共13页
Infrared microthermometry allows direct measurement of fluid inclusions hosted in opaque ore minerals and can provide direct constraints on the evolution of ore-forming fluids.This study presents infrared microthermom... Infrared microthermometry allows direct measurement of fluid inclusions hosted in opaque ore minerals and can provide direct constraints on the evolution of ore-forming fluids.This study presents infrared microthermometry of spherite-hosted fluid inclusions from the Xinqiao deposit in the Middle-Lower Yangtze Metallogenic Belt and sheds new light on the ore genesis of the deposit.Considering that infrared light may lead to non-negligible temperature deviations during microthermometry,some tests were first conducted to ensure the accuracy of the microthermometric measurements.The measurement results indicated that using the lowest light intensity of the microscope and inserting an optical filter were effective in minimizing the possible temperature deviations of infrared microthermometry.All sphalerite-hosted fluid inclusions from the Xinqiao deposit were aqueous.They show homogenization temperature ranging from~200 to 350℃,but have two separate salinity groups(1.0 wt%-10 wt%and 15.1 wt%-19.2 wt%NaCl equivalent).The low-salinity group represents sedimentary exhalative(SEDEX)-associated fluids,whereas the high-salinity group results from modification by later magmatic hydrothermal fluids.Combined with published fluid inclusion data,the four-stage fluid evolution of the Xinqiao deposit was depicted.Furthermore,our data suggest that the Xinqiao deposit was formed by twostage metallogenic events including SEDEX and magmatic-hydrothermal mineralization. 展开更多
关键词 infrared microthermometry fluid inclusion SPHALERITE Xinqiao deposit
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明代婚礼服饰的艺术特征与影响因素 被引量:5
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作者 卞向阳 李梦珂 《服装学报》 CAS 2019年第6期531-537,共7页
明代婚服是中国古代汉民族礼仪服饰文化的集大成者,婚服的传承与演变过程见证着时代发展。依托明代历史文献资料与出土服饰实物,探寻明代婚礼服饰发展演变的历史根源;分析不同阶层男女婚礼服饰形制,并描绘出对应的婚服着装搭配图示;根... 明代婚服是中国古代汉民族礼仪服饰文化的集大成者,婚服的传承与演变过程见证着时代发展。依托明代历史文献资料与出土服饰实物,探寻明代婚礼服饰发展演变的历史根源;分析不同阶层男女婚礼服饰形制,并描绘出对应的婚服着装搭配图示;根据色彩、纹样、材质、工艺归纳明代婚礼服饰的艺术特征。研究认为,明代婚礼服饰艺术特征主要受到政治因素、经济态势、社会风尚与文化理念等因素的影响。研究结果为理清明代婚服形制的艺术特征提供可靠依据。 展开更多
关键词 明代 婚礼服饰 礼制规范 社会风尚
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Ultrastructure of Kupffer cells and hepatocytes in the Dubin-Johnson syndrome:A case report 被引量:1
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作者 Maria Elzbieta Sobaniec-Lotowska Dariusz Marek Lebensztein 《World Journal of Gastroenterology》 SCIE CAS CSCD 2006年第6期987-989,共3页
Ultrastructure of Kupffer cells and hepatocytes in liver bioptate was evaluated in a 17-year-old boy with Dubin -Johnson syndrome (D.1S). The liver tissue obtained by needle biopsy was fixed in glutaraldehyde and pa... Ultrastructure of Kupffer cells and hepatocytes in liver bioptate was evaluated in a 17-year-old boy with Dubin -Johnson syndrome (D.1S). The liver tissue obtained by needle biopsy was fixed in glutaraldehyde and paraformaldehyde and routinely processed for electron microscopic analysis. The ultrastructural examinations of liver bioptate revealed the accumulation of membranebound, electron-dense lysosomal granules within the cytoplasm of hepatocytes, characteristic of D.1S. They were located mainly in the vicinity of the biliary pole, and preferentially in the centrilobular region that corresponded to the pigment deposits seen under light microscope. The presence of the granules was accompanied by dilated elements of the granular endoplasmic reticulum and paracrystalline mitochondrial inclusions as well as dilation of the bile canaliculi. The changes in hepatocytes coexisted with marked stimulation and enhanced phagocytic activity of Kupffer cells. This was manifested in the accumulation of pigment deposits within their cytoplasm that corresponded to those observed in hepatocytes. Hyperactive pericentral Kupffer cells which are involved in the response to pigmentary material originating from disintegrated hepatocytes may play an essential role in the development of DJS. 展开更多
关键词 Liver biopsy Electron microscopic study Lysosomal granules Functional hyperbilirubinemia Dubin-Johnson syndrome
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The relationship between IR characteristic peak and microstructure of the glass used as optical fiber 被引量:4
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作者 段吉安 蔡国华 帅词俊 《Journal of Central South University of Technology》 2006年第3期238-241,共4页
Based on the harmonic vibration equation, the relationship between IR characteristic peak of fiberglass and Si-O-Si bond angle was deduced, and 1 100 cm^-1 characteristic peak was specifically studied. It is found tha... Based on the harmonic vibration equation, the relationship between IR characteristic peak of fiberglass and Si-O-Si bond angle was deduced, and 1 100 cm^-1 characteristic peak was specifically studied. It is found that 1 100 cm^-1 characteristic peak shifts to higher wave number when Si-O-Si bond angle increases. Taking fused biconical taper (FBT) coupler as an example, the microstructures of the fiber coupler manufactured at different draw- ing speeds were tested with micro infrared spectrum. According to the test results, it is found that the bond angle at the taper region is the largest, the one at the fused region is the second largest, and the one of bare fiber is the smal- lest. The characteristic peaks of fused-taper region shift to higher wave number when drawing speed increases. 展开更多
关键词 FIBERGLASS IR spectroscopic MICROSTRUCTURE
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Visualization of chromatin folding patterns in chicken erythrocytes by atomic force microscopy (AFM) 被引量:1
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作者 QIAN RUO LAN ZHENG XIA LIU +5 位作者 MEI YUN ZHOU HEN YUE XIE CHU JIANG ZHI JIANG YAN(Shanghai Institute of Cell Biology, Chinese Academy ofSciences, Shanghai 200031, China)LI MIN QIAN YI ZHANG JUN HU(Shanghai Institute of Nuclear Research, Chinese Academyof 《Cell Research》 SCIE CAS CSCD 1997年第2期143-150,共8页
The organization of the higher order structure of chromatin in chicken erythrocytes has been examined withtapping-mode scanning force microscopy under conditionsclose to their native environment. Reproducible highreso... The organization of the higher order structure of chromatin in chicken erythrocytes has been examined withtapping-mode scanning force microscopy under conditionsclose to their native environment. Reproducible highresolution AFM images of chromatin compaction at several levels can be demonstrated. An extended beads-on-astring (width of ~ 15-20nm, height of ~ 2-3nm for eachindividual nucleosome) can be consistently observed. Furthermore, superbeads (width of ~ 40nm, height of ~ 7nm)are demonstrated. Visualization of the solenoid conformation at the level of 30nm chromatin fiber is attained eitherby using AFM or by using electron microscopy. In addition, tightly coiled chromatin fibers (~ 50-60nm and ~90-110nm) can be revealed. Our data suggest that the chromatin in the interphase nucleus of chicken erythrocyte represents a high-order conformation and AFM provides useful high-resolution structural information concerning thefolding pattern of interphase chromatin fibers. 展开更多
关键词 The chromatin folding pattern chicken erythrocyte atomic force microscopy
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The structure of the nucleosome core particle of chromatin in chicken erythrocytes visualized by using atomicforce microscopy 被引量:2
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作者 ZHAO HUI YI ZHANG +4 位作者 SHU BING ZHANG CHUJIANG QI YE HE MIN QIAN LI RUO LANQIAN( Shanghai Institute of Cell Biology, Chinese Academyof Sciences, Shanghai 200031, China)( Shanghai Institute of Nuclear Research, ChineseAcademy of Sciences, Shanghai 201800, 《Cell Research》 SCIE CAS CSCD 1999年第4期255-260,共6页
The structure of the nuclosome core particle of chromatin in chicken erythrocytes has been examined by usingAFM. The 146 hp of DNA wrapped twice around the corehistone octamer are clearly visualized. Both the ends ofe... The structure of the nuclosome core particle of chromatin in chicken erythrocytes has been examined by usingAFM. The 146 hp of DNA wrapped twice around the corehistone octamer are clearly visualized. Both the ends ofentry/exit of linker DNA are also demonstrated. The dimension of the nucleosome core particles is- 1-4 um inheight and ~13-22 um in width. In addition, superbeads(width of - 48-57 urn, beight of-2-3 nm) are occasionallyrevealed, two turns of DNA around the core particles arealso detected. 展开更多
关键词 Nucleosome core particle chicken erythrocytes atomic force microscopy.
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New Records of Freeliving Marine Nematodes from Hong Kong,China 被引量:3
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作者 ZHOU Hong, ZHANG ZhinanCollege of Marine Life Sciences, Ocean University of China, Qingdao 266003, P.R.China 《Journal of Ocean University of Qingdao》 2003年第2期177-184,共8页
Six species of new records collected from intertidal mangrove/non-mangrove and subtidal cave sediments during a mangrove ecological study (1998-2001) and a marine cave expedition (2002) in Hong Kong waters are redescr... Six species of new records collected from intertidal mangrove/non-mangrove and subtidal cave sediments during a mangrove ecological study (1998-2001) and a marine cave expedition (2002) in Hong Kong waters are redescribed. These include two enoplids: Anoplostoma viviparum in Anoplostomatidae and Trissonchulus janetae in Ironidae, two chromadorids:Paracomesoma dubium and Actarjania splendens in Comesomatidae, and two monhysterids: Parodontophora marina and Parodontophora c.f. danker in Axonolaimidae. Five of them are the first records from China. Ecological and taxonomic remarks are provided and discussed in comparison with the original descriptions. 展开更多
关键词 freeliving marine nematodes new records Hong Kong China
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Electrophoretic Deposition of TiO2/Nb2O5 Composite Electrode Thin Films for Photovoltaic Application 被引量:1
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作者 John Njagi Nguu Bernard Odhiambo Aduda Francis Wanjala Nyongesa Robinson Juma Musembi 《Journal of Energy and Power Engineering》 2014年第4期757-764,共8页
Nano sized powders of TiO2 (titanium dioxide) and Nb2O5 (Niobium (V) oxide) were used to fabricate TiO2/Nb2O5 composites thin films by EPD (electrophoretic deposition) technique. The metal oxide powders, toget... Nano sized powders of TiO2 (titanium dioxide) and Nb2O5 (Niobium (V) oxide) were used to fabricate TiO2/Nb2O5 composites thin films by EPD (electrophoretic deposition) technique. The metal oxide powders, together with magnesium nitrate hexahydrate pellets, were suspended in propan-2-ol inside an EPD cell. The electrodes, placed 1.2 cm apart, were partially immersed in the suspension and a DC potential applied across them. Key EPD process parameters, which include applied DC electric field, deposition time and solid concentration in suspension, were optimized through visual inspection and from UV-Vis-NIR spectrophotometer spectra. The highest (55%) transmittance was obtained for films with deposition time of 90 s, powder concentration of 0.01 g/40 mL, and 35 V DC (direct current) voltage. XRD micrographs confirmed that TiO2 and Nb2O5 particles were presented in the composite film. SEM (scanning electron microscope) micrographs of the composite electrode thin films showed that porous films of high quality with well controlled morphology were deposited by using the EPD technique. 展开更多
关键词 Electrophoretic deposition TiO2/Nb2O5 composite electrode thin films.
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Changes in organic structure and mineral phases transformation of coal during heat treatment on laboratory scale 被引量:8
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作者 Vivek Mishra Mamta Sharma +1 位作者 Sanchita Chakravarty Amit Banerjee 《International Journal of Coal Science & Technology》 EI 2016年第4期418-428,共11页
Structural changes due to coalification and oxidation influence the coal quality, geochemically and petrologically. Understanding of the coal structures helps to predict the behaviour of coal at various processes. The... Structural changes due to coalification and oxidation influence the coal quality, geochemically and petrologically. Understanding of the coal structures helps to predict the behaviour of coal at various processes. The objective of this paper is to study the changes in organic structure and mineral phase transformation during combustion. Different density fractions were generated and then heated at different temperatures from 200 to 1000 ℃. Petrography, Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD) were carried out on all the density fractions aimed to accomplish this objective. Here, through petrography, it was observed that the vitrinite and liptinite macerals disappear at higher temperature while porous inertinite is seen. The inertinite structure is exposed which is assumed by the presence of -OH and C-O-C stretches with the aromatic nucleus (CH) and three to four adjacent H from FTIR spectra. Moreover, it can be concluded that aliphatic groups get collapsed at high temperature. In case of inorganic matter, through XRD and FTIR, it is also revealed that with increasing temperature, clay minerals converted into elemental oxides. Hence, this study is suggesting that the structures of coal are altered by the degree of contact metamorphism. 展开更多
关键词 COAL Heat treatment Oxidation PETROGRAPHY FTIR XRD
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Hydrothermal Synthesis of Rhombus-like SmCO3OH Microplates and Its Photoluminescence Property Doped with Eu^3+ 被引量:1
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作者 尹小斌 张悠金 +1 位作者 方志勇 徐振宇 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2010年第1期102-106,I0002,共6页
Rhombus-like SmCO3OH microplates with the edge lengths ranging from 5 μm to 10 μm and the thickness about 1.5 μm were synthesized through a simple hydrothermal method using urea as the precipitance. The structure a... Rhombus-like SmCO3OH microplates with the edge lengths ranging from 5 μm to 10 μm and the thickness about 1.5 μm were synthesized through a simple hydrothermal method using urea as the precipitance. The structure and properties of the rhombus-like SmCO3OH microplates were characterized by X-ray diffraction, field-emission scanning electron microscopy, Fourier transform infrared spectroscopy, and X-ray photoelectron spectroscopy. The optical property of the rhombus-like SmCO3OH microplates doped with Eu^3+ was investigated by photoluminescence. A broad and strong emission band at 677 nm was obtained, which can be contributed to producing light conversion film. 展开更多
关键词 SmCO3OH Hydrothermal method PHOTOLUMINESCENCE
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A Survey of Translation of Robert Bums' "A Red, Red Rose" in China
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作者 LI Zheng-shuan 《Journal of Literature and Art Studies》 2016年第4期325-339,共15页
Robert Burns wrote about 700 poems and songs. But the first poem that was translated into Chinese is "A Red, Red Rose". It was collected into a book compiled in 1908 which was published in 1911. It was retranslated ... Robert Burns wrote about 700 poems and songs. But the first poem that was translated into Chinese is "A Red, Red Rose". It was collected into a book compiled in 1908 which was published in 1911. It was retranslated many times at different times, mostly by people who were both poets and translators at the same time. And almost all the translators were famous poets such as Su Manshu, Yuan Shuipai, Wang Zuoliang, Yuan Kejia, and Guo Moruo. These translators had their own unique taste and typical features. This article will present a survey of translation history and at the same time give some comments on different versions. 展开更多
关键词 Robert Bums "A Red Red Rose" translation into Chinese
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Microstructure and microwave dielectric properties of CaO-B_2O_3-SiO_2 glass ceramics with various B_2O_3 contents 被引量:8
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作者 韦鹏飞 周洪庆 +2 位作者 朱海奎 戴斌 王杰 《Journal of Central South University》 SCIE EI CAS 2011年第5期1359-1364,共6页
The effects of B2O3 addition on both the sintering behavior and microwave dielectric properties of CaO-B2O3-SiO2 (CBS) glass ceramics were investigated by Fourier transform infrared spectroscopy (FTIR), X-ray diff... The effects of B2O3 addition on both the sintering behavior and microwave dielectric properties of CaO-B2O3-SiO2 (CBS) glass ceramics were investigated by Fourier transform infrared spectroscopy (FTIR), X-ray diffractometry (XRD) and scanning electron microscopy (SEM). The results show that the increasing amount of B203 causes the increase of the contents of [BO3], [BO4] and [SiO4], which deduces the increase of CaB204 and a-SiO2 and the decrease of CaSiO3 correspondingly. No new phase is observed throughout the entire experiments. A bulk density of 2.54 g/cm3, a thermal expansion coefficient value of 11.95× 10-6 ℃-1 (20-500℃), a dielectric constant er value of 6.42 and a dielectric loss tanδ value of 0.000 9 (measured at 9.7 GHz) are obtained for CBS glass ceramics containing 35%-B203 (mass fraction) sintered at 850 ℃ for 15 min. 展开更多
关键词 CAO-B2O3-SIO2 B2O3 content Fourier transform infrared spectroscopy MICROSTRUCTURE dielectric properties
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Polyhydroxyl-aluminum pillaring improved adsorption capacities of Pb^(2+) and Cd^(2+) onto diatomite 被引量:5
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作者 朱健 王平 +1 位作者 雷明婧 张伟丽 《Journal of Central South University》 SCIE EI CAS 2014年第6期2359-2365,共7页
In order to greatly improve adsorption capacity, the diatomite was pillared by polyhydroxyl-aluminum.A series of adsorption tests were conducted to obtain the optimum condition for pillared diatomite synthesis. The sc... In order to greatly improve adsorption capacity, the diatomite was pillared by polyhydroxyl-aluminum.A series of adsorption tests were conducted to obtain the optimum condition for pillared diatomite synthesis. The scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), surface area and porosity analyzer and micro-electrophoresis were used to determine pore structure and surface property.The pillared diatomite attaining the optimal adsorption densities (qe) of Pb^2+ and Cd^2+ was synthesized with the following conditions: Addition of pillaring solution containing Al3+-oligomers with a concentration range of 0.1-0.2 mol/L to a suspension containing Na+-diatomite to obtain the required Al/diatomite ratio of 10 mmol/g; synthesis temperature of 80 ℃ for 120 min; aging at a temperature of 105 ℃ for 16 h. The adsorption capacities of Pb^2+ and Cd^2+ on pillared diatomite increase by 23.79% and 27.36% compared with natural diatomite, respectively. The surface property of pillared diatomite is more favorable for ion adsorption than natural diatomite. The result suggests that diatomite can be modified by pillaring with polyhydroxyl-aluminum to improve its adsorption properties greatly. 展开更多
关键词 DIATOMITE PILLARING polyhydroxyl-aluminum synthesis ADSORPTION Pb^2+ Cd^2+
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Synthesis and Antimicrobial Activity of Heterocyclic Compounds Containing Chromene Ring
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作者 Enaiat K. Mohamed Wesam S. Shehab 《Journal of Chemistry and Chemical Engineering》 2010年第10期26-32,共7页
Synthesis of some new compounds containing chromene ring are described in this work. They were synthesized in moderate to good yield, started with Condensation of 7-hydroxy-4-methylcoumarin (1) with ethyl bromoaceta... Synthesis of some new compounds containing chromene ring are described in this work. They were synthesized in moderate to good yield, started with Condensation of 7-hydroxy-4-methylcoumarin (1) with ethyl bromoacetate furnishes ethyl-2-(4-methyl-2-oxo-2H-chromen-7-yloxy) acetate (2). The structures of all the new compounds were confirmed using IR, 1H-NMR spectra and micro analysis, selected members of the synthesized compound were screened for antimicrobial activity. They have shown a wide range of activity from one completely inactive compound to medium active ones. 展开更多
关键词 CHROMENE THIAZOLIDINE Oxazolotriazole derivatives antimicrobial activity
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A novel synthesis of LiFePO_4/C from Fe_2O_3 without extra carbon or carbon-containing reductant 被引量:5
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作者 肖政伟 胡国荣 《Journal of Central South University》 SCIE EI CAS 2014年第6期2143-2149,共7页
A novel synthesis of LiFePO4/C from Fe2O3 with no extra carbon or carbon-containing reductant was introduced: Fe2O3 (+NH4H2PO4)→Fe2P2O7(+Li2CO3+glucose)→LiFePO4/C. X-ray diffractometry (XRD), Fourier trans... A novel synthesis of LiFePO4/C from Fe2O3 with no extra carbon or carbon-containing reductant was introduced: Fe2O3 (+NH4H2PO4)→Fe2P2O7(+Li2CO3+glucose)→LiFePO4/C. X-ray diffractometry (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) were utilized to characterize relevant products obtained in the synthetic procedure. The reaction of Fe2P2O7 and Li2CO3 was investigated by thermo-gravimetric and differential thermal analysis (TGA-DTA). Fe2O3 is completely reduced to Fe2P2O7 by NH4H2PO4 at 700 ℃ and Fe2P2O7 fully reacts with Li2CO3 to form LiFePO4 in the temperature range of 663.4-890 ℃. The primary particles of LiFePO4/C samples prepared at 670, 700 and 750 ℃ respectively exhibit uniform morphology and narrow size distribution, 0.5-3 μm for those obtained at 670 and 700 ℃ and 0.5-5 μm for those obtained at 750 ℃. LiFePO4/C (carbon content of 5.49%, mass fraction) made at 670 ℃ shows an appreciable average capacity of 153.2 mA·h/g at 0.1C in the first 50 cycles. 展开更多
关键词 lithium ion phosphate ferric oxide ferrous pyrophosphate lithium ion cells
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In-situ Synthesis of ZSM-5 Zeolite from Metakaolin/Spinel and Its Catalytic Performance on Methanol Conversion 被引量:4
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作者 Liu Ye Yu Xianbo +2 位作者 Qin Lei Wang Jingdai Yang Yongrong (Department of Chemical and Biochemical Engineering,Zhejiang University,Hangzhou 310027) 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2010年第1期23-28,共6页
ZSM-5 zeolite was in-situ synthesized from metakaolin or s alumina sources, respectively. The ZSM-5 zeolite was characterized pinel by incorporating additional silica and by X-ray diffractometry (XRD), scanning elec... ZSM-5 zeolite was in-situ synthesized from metakaolin or s alumina sources, respectively. The ZSM-5 zeolite was characterized pinel by incorporating additional silica and by X-ray diffractometry (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) spectroscopy and N2 adsorption measurement. This supported zeolite was tested on the methanol to propylene (MTP) processes. Experimental results showed that the ZSM-5 zeolite exhibited high selectivity for propylene. The yield of propylene on ZSM-5 zeolite made from metakaolin was increased by 17.73%, while that on ZSM-5 zeolite made from spinel was raised by 9.90%, compared to that achieved with the commercial ZSM-5 zeolite. The significant increase in propylene production is probably due to the distinctive morphology of the ZSM-5 zeolite, which possessed a rough external surface covered with sphere-like particles and distribution of small crystals sized at around 400--500 nm. This morphology could help to generate more crystal defects so that more active centers could be exposed to the reaction mixture. In addition, the zeolite product had a gradient pore distribution and many medium Brǒnsted acid sites, both of which might also contribute to the increased propylene production. 展开更多
关键词 METAKAOLIN SPINEL in-situ synthesis of ZSM-5 methanol to propylene (MTP)
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Enzymatic saccharification of cellulose using an ionic liquid [Amim] [COOH] pretreatment
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作者 LIU Zhen XIA Chi DAI Hui WANG Jian-ji 《Journal of Energy and Power Engineering》 2009年第9期49-53,共5页
In this study we used l-allyl-3-methyl imidazole formate ([Amim][COOH]) as ionic liquid to pre-treat the cellulose and determined the rate of polymerization and enzymatic hydrolysis. The results showed that pretreat... In this study we used l-allyl-3-methyl imidazole formate ([Amim][COOH]) as ionic liquid to pre-treat the cellulose and determined the rate of polymerization and enzymatic hydrolysis. The results showed that pretreatment with ([Amim][COOH]) significantly decreased the cellulose polymerization. As the pretreatment temperature went up, the enzymatic hydrolysis rate was first increased and then decreased The maximal enzymatic hydrolysis rate was achieved when the pretreatment temperature was 90 ℃. Under the ultrasonic condition, the initial rate of enzmatic hydrolysis for the ionic liquid-treated cellulose was up to 11.10 gL-1h-1, which was 33% increase compared to the untreated cellulose. Scanning Electronic Microscopy (SEM) and Fourier Transform Infrared-Raman Spectroscop (FT-IR) analysis showed that ionic liquidtreated cellulose started to depolymerize. In addition, the cr3'stallinity of the cellulose was significantly decreased after pretreatment with ionic liquid. 展开更多
关键词 ionic liquid cellulose: pretreatment: enzymatic hydrolysis: ultrasonic
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