Aim To establish a HPLC method for the separation of the enantiomers of zolmitriptan. Methods The separations were performed on Chiralcel OJ column with hexane-ethanol-diethylamine（85：15：0.2） as mobile phase at a ...Aim To establish a HPLC method for the separation of the enantiomers of zolmitriptan. Methods The separations were performed on Chiralcel OJ column with hexane-ethanol-diethylamine（85：15：0.2） as mobile phase at a flow rate of 0.8 mL·min^-1 and detecttion wavelength of 227 nm at 35 ℃. Several related parameters for separation were studied. Results Baseline separation （Rs 〉 1.5） was easily obtained in the case, and the R-isomer impurity in zolmitriptan was determined. Conclusion The method developed in this study has been successfully applied for quality-control purposes.展开更多
The principles of the SINS/DVL integrated navigation system are introduced, and the compass status accuracy is compared. When the heading is changed, the dead reckoning algorithm using the heading information of the S...The principles of the SINS/DVL integrated navigation system are introduced, and the compass status accuracy is compared. When the heading is changed, the dead reckoning algorithm using the heading information of the SINS (Strapdown inertial navigation systems) and DVL (doppler velocity log) is adopted to substitute the SINS/DVL integrated system. The simulation results show that the method can improve the accuracy of integrated navigation system when AUV (autonomous underwater vehicle) is in motion.展开更多
Application of Balanced Scorecard （BSC） is not so successful in China in the past few years. This paper is to represent how the company Sichuan Ertan Industrial Corporation （SEICO）, design performance evaluation s...Application of Balanced Scorecard （BSC） is not so successful in China in the past few years. This paper is to represent how the company Sichuan Ertan Industrial Corporation （SEICO）, design performance evaluation system to improve its efficiency and effectiveness and satisfy customers＇ needs with the help of BSC principles and methodology. It is found from this case study that the key steps to design performance evaluation system are to： （1） link strategy and performance measurements at company-level; （2） decompose them into all the members in all the units at all the levels of that company; and （3） tie them to an incentive plan. Those steps have not been detailed in publications by Kaplan and Norton.展开更多
Experimental results of remote laser measurement of a time structure of a pulse waves are resulted. Occurrence of the pulse waves are connected with the rhythmic reduction of a myocardittm. Speed of pulse wave＇s prop...Experimental results of remote laser measurement of a time structure of a pulse waves are resulted. Occurrence of the pulse waves are connected with the rhythmic reduction of a myocardittm. Speed of pulse wave＇s propagation does not depend on speed of current of blood, it is defined by diameter of a vessel, by its walls thickness, by elasticity of a vessel, and also by rheological properties of blood. Measurement of parameters of pulse waves is important tbr definition of a condition of cardiovascular system. Ways of measurement of characteristics of pulse waves used now （acoustic, electric, optical） are contact. In some cases, for example, in clinics on treatment of burns and so forth, the question of remote measurement of processes hemodynamics by use of methods of laser sotmding is rather actual. The results described in work have shown outlook of development of laser methods of diagnostics for present purposes. The measurement technique used by authors is based on use of longitudinal Doppler effect which essence consists in change of frequency or length of a wave of radiation at reflection from moving surface. For smoothing the measured signal （clearing from noise） the program developed by authors on the basis of the wavelet-analysis was used. Experimental measurements are shown, that the laser method allows to register distinctly structure of pulse waves which is characterized by two peaks. The results of remote laser measurement of a time structure of a pulse waves confirm the assumption made on the basis of general-theoretical physical positions, that characteristics of pulse waves can be registered on the Doppler effect basis.展开更多
This paper investigates the distribution of intercarrier interference （ICI） in multiple-input multiple-output orthogonal frequency division multiplexing （MIMO-OFDM） systems based on the geometrical one-ring model....This paper investigates the distribution of intercarrier interference （ICI） in multiple-input multiple-output orthogonal frequency division multiplexing （MIMO-OFDM） systems based on the geometrical one-ring model. Using the spatial and temporal correlation of a geometrical one-ring model, a close-formed expression of intercarrier interference due to the Doppler effect caused by the movement of receiver is derived under the isotropic scattering conditions and non-isotropic scattering conditions. The analytical results are verified by Monte Carlo simulations. We use the generated channels to investigate MIMO-OFDM intercarrier interference under various channel parameters. It can be shown that more than 95% oflCI power comes from five neighboring subcarriers.展开更多
文摘Aim To establish a HPLC method for the separation of the enantiomers of zolmitriptan. Methods The separations were performed on Chiralcel OJ column with hexane-ethanol-diethylamine（85：15：0.2） as mobile phase at a flow rate of 0.8 mL·min^-1 and detecttion wavelength of 227 nm at 35 ℃. Several related parameters for separation were studied. Results Baseline separation （Rs 〉 1.5） was easily obtained in the case, and the R-isomer impurity in zolmitriptan was determined. Conclusion The method developed in this study has been successfully applied for quality-control purposes.
文摘The principles of the SINS/DVL integrated navigation system are introduced, and the compass status accuracy is compared. When the heading is changed, the dead reckoning algorithm using the heading information of the SINS (Strapdown inertial navigation systems) and DVL (doppler velocity log) is adopted to substitute the SINS/DVL integrated system. The simulation results show that the method can improve the accuracy of integrated navigation system when AUV (autonomous underwater vehicle) is in motion.
文摘Application of Balanced Scorecard （BSC） is not so successful in China in the past few years. This paper is to represent how the company Sichuan Ertan Industrial Corporation （SEICO）, design performance evaluation system to improve its efficiency and effectiveness and satisfy customers＇ needs with the help of BSC principles and methodology. It is found from this case study that the key steps to design performance evaluation system are to： （1） link strategy and performance measurements at company-level; （2） decompose them into all the members in all the units at all the levels of that company; and （3） tie them to an incentive plan. Those steps have not been detailed in publications by Kaplan and Norton.
文摘Experimental results of remote laser measurement of a time structure of a pulse waves are resulted. Occurrence of the pulse waves are connected with the rhythmic reduction of a myocardittm. Speed of pulse wave＇s propagation does not depend on speed of current of blood, it is defined by diameter of a vessel, by its walls thickness, by elasticity of a vessel, and also by rheological properties of blood. Measurement of parameters of pulse waves is important tbr definition of a condition of cardiovascular system. Ways of measurement of characteristics of pulse waves used now （acoustic, electric, optical） are contact. In some cases, for example, in clinics on treatment of burns and so forth, the question of remote measurement of processes hemodynamics by use of methods of laser sotmding is rather actual. The results described in work have shown outlook of development of laser methods of diagnostics for present purposes. The measurement technique used by authors is based on use of longitudinal Doppler effect which essence consists in change of frequency or length of a wave of radiation at reflection from moving surface. For smoothing the measured signal （clearing from noise） the program developed by authors on the basis of the wavelet-analysis was used. Experimental measurements are shown, that the laser method allows to register distinctly structure of pulse waves which is characterized by two peaks. The results of remote laser measurement of a time structure of a pulse waves confirm the assumption made on the basis of general-theoretical physical positions, that characteristics of pulse waves can be registered on the Doppler effect basis.
文摘This paper investigates the distribution of intercarrier interference （ICI） in multiple-input multiple-output orthogonal frequency division multiplexing （MIMO-OFDM） systems based on the geometrical one-ring model. Using the spatial and temporal correlation of a geometrical one-ring model, a close-formed expression of intercarrier interference due to the Doppler effect caused by the movement of receiver is derived under the isotropic scattering conditions and non-isotropic scattering conditions. The analytical results are verified by Monte Carlo simulations. We use the generated channels to investigate MIMO-OFDM intercarrier interference under various channel parameters. It can be shown that more than 95% oflCI power comes from five neighboring subcarriers.
