The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show t...The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show that the quench sensitivity of 6063 alloy is lower than that of 6061 or 6082 alloy,and the critical temperature ranges from 300 to 410℃ with the nose temperature of about 360℃.From TEM analysis,heterogeneous precipitate β-Mg2Si is prior to nucleate on the(AlxFeySiz) dispersoids in the critical temperature range,and grows up most rapidly at the nose temperature of 360℃.The heterogeneous precipitation leads to a low concentration of solute,which consequently reduces the amount of the strengthening phase β'' after aging.In the large-scale industrial production of 6063 alloy,the cooling rate during quenching should be enhanced as high as possible in the quenching sensitive temperature range(410-300℃) to suppress the heterogeneous precipitation to get optimal mechanical properties,and it should be slowed down properly from the solution temperature to 410℃ and below 300℃ to reduce the residual stress.展开更多
The post buckling strength of web plate of I section plate girders is considered to resist the shear force in many other countries code for design of steel structures,while it has not been considered in the Chinese ...The post buckling strength of web plate of I section plate girders is considered to resist the shear force in many other countries code for design of steel structures,while it has not been considered in the Chinese code GB J17-88.For the code revising,some important conclusions have been drawn through the theoretical analysis and experimental research of the post buckling strength of web plate of I section plate girders.展开更多
The gradient image is always sensitive to noise in image detail enhancement. To overcome this shortage, an improved detail enhancement algorithm based on difference curvature and contrast field is proposed. F...The gradient image is always sensitive to noise in image detail enhancement. To overcome this shortage, an improved detail enhancement algorithm based on difference curvature and contrast field is proposed. Firstly, the difference curvature is utilized to determine the amplification coefficient instead of the gradient. This new amplification function of the difference curvature takes more neighboring points into account, it is therefore not sensitive to noise. Secondly, the contrast field is nonlinearly amplified according to the new amplification coefficient. And then, with the enhanced contrast field, we construct the energy functional. Finally, the enhanced image is reconstructed by the variational method. Experimental results of standard testing image and industrial X-ray image show that the proposed algorithm can perform well on increasing contrast and sharpening edges of images while suppressing noise at the same time.展开更多
A new composite structure based on aluminum foam sandwich and fiber metal laminate was proposed. A layer of glass fiber was provided at the interface between the metal panel and the aluminum foam core in this composit...A new composite structure based on aluminum foam sandwich and fiber metal laminate was proposed. A layer of glass fiber was provided at the interface between the metal panel and the aluminum foam core in this composite structure, using adhesive technology to bond the materials together by organic glue in the sequence of metal panel, glass fiber, aluminum foam core, glass fiber and metal panel. The experimental results show that the new composite structure has an improved comprehensive performance compared with the traditional aluminum foam sandwiches. The optimized parameters for the fabrication of the new aluminum foam composite structure with best bending strength were obtained. The epoxy resin and low porosity aluminum foams are preferred, the thickness of aluminum sheets should be at least 1.5 mm, and the type of glass fiber has little effect on the bending strength. The main failure modes of the new composite structures with two types of glues were discussed.展开更多
A good quality, high yield, slow mature and middle season Japonica rice variety, Nanjing 9108 and its parents Guandong 194 and Wuxiangjing 14,were taken as the materials for the study. The growth and photosynthetic ch...A good quality, high yield, slow mature and middle season Japonica rice variety, Nanjing 9108 and its parents Guandong 194 and Wuxiangjing 14,were taken as the materials for the study. The growth and photosynthetic characteristics of the rice plants at the post-flowering stage were compared and the rice yield components were examined at harvest. The results showed that as compared with Wuxiangjing 14, the per plant yield of Nanjing 9108 was 7.70% higher, and much higher than that of Guandong194. The large total grain per plant and heavy grain weigh of Nanjing 9108 were the important structure basis for its yield. Further analysis o the growth indicators showed that Nanjing 9108 had a large leaf area of upper three green leaves area and a smaller leaf base angle in the third leaf from the bottom blades, which helped get a higher photosynthetic capacity in groups. On the14 thday after flowering, Nanjing 9108 had similar value of net photosynthetic rate(Pn) to that of Wuxianjing 14, but lower than that of Guandong 194. Viewing from the parameters obtained from light response of photosynthesis on the modified model of rectangular hyperbola, Pn of Nanjing 9108 was more aptated to be saturated by light intensity and sensitive to photoinhibition. On the whole, Nanjing 9108 with high yield mainly resulted from its good plant type, grain structure and higher photosynthetic capacity in groups. Further improving its photosynthetic capacity o single leaf in Nanjing 9108 would be an important way for its super high yield po tential in the future.展开更多
Si/Al composites with different Si contents for electronic packaging were prepared by spark plasma sintering (SPS) technique. Properties of the composites were investigated, including density, thermal conductivity, ...Si/Al composites with different Si contents for electronic packaging were prepared by spark plasma sintering (SPS) technique. Properties of the composites were investigated, including density, thermal conductivity, coefficient of thermal expansion and flexural strength. The effects of the Si content on microstructure and thermal and mechanical properties of the composites were studied. The results show that the Si/Al composites consist of Si and Al components and Al uniformly distributes among Si grains. The relative density of the Si/Al composites gradually increases with the decrease of Si content and reaches 98.0% when the Si content is 50%. The thermal conductivity, the coefficient of thermal expansion and the flexural strength of the composite all decrease with the increase of the Si content, and an optimal matching of them is obtained when the Si content is 60%(volume fraction).展开更多
Equal channel angular pressing(ECAP)is one of the most effective processes to produce ultra-fine grain(UFG)and nanocrystalline(NC)materials.Because the commercially pure titanium exhibits excellent biocompatibility pr...Equal channel angular pressing(ECAP)is one of the most effective processes to produce ultra-fine grain(UFG)and nanocrystalline(NC)materials.Because the commercially pure titanium exhibits excellent biocompatibility properties,it has a significant potential to be utilized as an implant material.The low static and dynamic strengths of the pure titanium are one of the weaknesses of this material.This defect can be removed by applying the ECAP process on the pure titanium.In this work,the commercially pure titanium Grade2(CP-Ti of Grade2)was pressed at room temperature by the ECAP process via a channel angle of135°for3passes.The microstructural analysis and mechanical tests such as tensile test,hardness test,three-point bending test and Charpy impact test were all carried out on the ECAPed CP-Ti through3passes.The microstructural evolution reveals that by applying the ECAP process,coarse grain(CG)structure develops to UFG/NC structure.Moreover,the results of the mechanical tests show that the process significantly increases the yield and ultimate tensile strengths,bending strength,hardness and fracture toughness of the commercially pure titanium so that it can be used as a replacement for metallic alloys used as biomaterials.展开更多
To obtain porous alumina ceramic with high strength,a novel gelcasting system based on 2-hydroxyethyl methacrylate(HEMA)dissolved in tert-butyl alcohol(TBA)was developed.The polymerization of the HEMA-TBA gelcasting s...To obtain porous alumina ceramic with high strength,a novel gelcasting system based on 2-hydroxyethyl methacrylate(HEMA)dissolved in tert-butyl alcohol(TBA)was developed.The polymerization of the HEMA-TBA gelcasting system,the thermal behavior of obtained green body,and the microstructures and mechanical properties of the sintered bodies were investigated by rheometer,TG-DSC,SEM and bending strength testing,respectively.The results show that,(1)10 mg/mL of the initiator(benzoyl peroxide)is the optimal amount for polymerization of this gelscasting system at 25 ℃;(2)The alumina suspension of the HEMA-TBA gelcasting system showing shear-thinning behavior is sufficiently low for gelcasting process;(3)The bending strength of porous alumina ceramic samples,whose porosities range from 42% to 56%,is from(8±0.5)to(91±4.5)MPa.展开更多
A positioning volume ellipsoid method is proposed to represent tumor volume in the workspace of a high-intensity-focused ultrasound (HIFU) surgery platform during the platform's positioning motion. To this simplif...A positioning volume ellipsoid method is proposed to represent tumor volume in the workspace of a high-intensity-focused ultrasound (HIFU) surgery platform during the platform's positioning motion. To this simplified tumor model, a nearest neighbor search method is used to determine intermediate configuration and goal configuration, which the treatment head and ultrasound focus must pass in their localization to target volume. Based on the decided configurations, the continuity condition of combined Bezier curve in Euclidean space and De Casteljau algorithm on Lie group SO(3) are integrated to construct a combined Bezier positioning path of C2 continuity at junctional configuration, and an illustration of different positioning path planning is analyzed based on a liver tumor case.展开更多
Aiming at developing novel microwave-transparent ceramics with low dielectric loss, high thermal conductivity and high strength, Si3Na-AIN (30%, mass fraction) composite ceramics with La203 as sintering additive wer...Aiming at developing novel microwave-transparent ceramics with low dielectric loss, high thermal conductivity and high strength, Si3Na-AIN (30%, mass fraction) composite ceramics with La203 as sintering additive were prepared by hot-pressing at 1 800 ℃ and subsequently annealed at 1 450 ℃ and 1 850 ℃ for 2 h and 4 h, respectively. The materials were characterized by XRD and SEM. The effect of annealing process on the phase composition, sintering performance, microstructure, bending strength, dielectric loss and thermal conductivity of the materials was investigated. The results showed that both annealing at 1 850 ℃ and 1 450 ℃ promoted the phase transformation of α-Si3N4 to β-Si3N4. After annealing at 1 850 ℃, grain growth to a certain extent occurred in the materials. Especially, the elongated β-Si3N4 grains showed a slight increase in diameter from 0.2 μm to 0.6 μm approximately and a decrease in aspect ratio. As a result, as the annealing time increased to 4 h, the bending strength declined from 456 MPa to 390 MPa, whereas the dielectric loss decreased to 2.15× 10^-3 and the thermal conductivity increased to 16.3 W/(m.K) gradually. When annealed at 1 450 ℃, increasing the annealing time to 4 h significantly promoted the crystallization of glassy phase to La2Si6N803 phase in the materials, which led to the increase in bending strength to 619 MPa and thermal conductivity to 15.9 W/(m·K), respectively, and simultaneously the decrease in dielectric loss to 1.53× 10^-3.展开更多
One of the key problems by diffusion-rolling bonding with small reduction for carbon steel plates is the bonding assistant coat. Abonding assitant coat used below 850℃ was developed. It contained copper as basic elem...One of the key problems by diffusion-rolling bonding with small reduction for carbon steel plates is the bonding assistant coat. Abonding assitant coat used below 850℃ was developed. It contained copper as basic element and zinc as main alloy element. Other small elements and rear metals were added to decrease the melting point and to obtain a better clouding and bigh plasticity. Based on the theory of brazing and transient liquid diffusion welding, two carbon steel plates were rolled with small reduction by using self-made bonding assistant coat. Temperature, pressure and holding time are the main technology parameters for controlling the process of diffusion-rolling. The results show that the bonding strength is the greatest when the bonding temperature is 830℃, holding time is 3 min and the reduction rate is 9%.展开更多
This paper reports investigation conducted to study the fatigue performance of steel fibre reinforced concrete (SFRC) containing fibres of mixed aspect ratio. An extensive experimental program was conducted in which 9...This paper reports investigation conducted to study the fatigue performance of steel fibre reinforced concrete (SFRC) containing fibres of mixed aspect ratio. An extensive experimental program was conducted in which 90 flexural fatigue tests were carried out at different stress levels on size 500 mm×100 mm×100 mm SFRC specimens respectively containing 1.0%, 1.5% and 2.0% volume fraction of fibres. About 36 static flexural tests were also conducted to determine the static flexural strength prior to fatigue testing. Each volume fraction of fibres incorporated corrugated mixed steel fibres of size 0.6 mm×2.0 mm×25 mm and 0.6 mm×2.0 mm×50 mm in ratio 50:50 by weight. The results are presented both as S-N relationships, with the maximum fatigue stress expressed as a percentage of the strength under static loading, and as relationships between actually applied fatigue stress and number of loading cycles to failure. Two-million-cycle fatigue strengths of SFRC containing different volume fractions of mixed fibres were obtained and compared with plain concrete.展开更多
Zirconia/stainless steel (ZrO2/SUS316L) functionally graded materials (FGMs) were fabricated by tape casting and laminating. Microstructures of FGMs were observed by optical microscope. Fracture behavior of FGMs in di...Zirconia/stainless steel (ZrO2/SUS316L) functionally graded materials (FGMs) were fabricated by tape casting and laminating. Microstructures of FGMs were observed by optical microscope. Fracture behavior of FGMs in different loading modes and influences of different gradient changes on flexural strength were investigated. The results show that ZrO2/ SUS316L FGMs with graded components at interlayers are obtained after they are sintered in vacuum and pressureless condition at 1 350 ℃. TheⅠ?Ⅱ mixed mode crack creates in composite layer and grows to both sides zigzag while loading on ZrO2 layer. Flexural strengths are 496.4,421.7 and 387.5 MPa when gradient changes are 10%,15% and 20%,but flexural strengths of the corresponding fracture layers are 387.1,334.6 and 282.3 MPa since cracks of FGMs are affected by three-dimensional stress,respectively. The cracks are generated in ZrO2 layer and extend to SUS316L layer while loading is added on SUS316L layer,flexural strength does not change with the graded components and keeps consistent basically.展开更多
Ni-Cr/h-BN self-lubricating composities were prepared by powder metallurgy (P/M) method.The effects of hexagonal boron nitride (h-BN) content on the mechanical and tribological properties of the Ni-Cr/h-BN composites ...Ni-Cr/h-BN self-lubricating composities were prepared by powder metallurgy (P/M) method.The effects of hexagonal boron nitride (h-BN) content on the mechanical and tribological properties of the Ni-Cr/h-BN composites were investigated.The corresponding frictional models were established to analyze the formation of the lubricant h-BN films on the surfaces of the Ni-Cr/h-BN composites.The results show that,when the content of h-BN increases from 5% to 15% (mass fraction),the bending strength of the Ni-Cr/h-BN composite decreases from 96.670 MPa to 17.319 MPa,and the hardness (HB) decreases from 33 to 14.The friction coefficient of the Ni-Cr/h-BN composite decreases firstly from 0.385 to 0.216,and then increases to 0.284,while the wear rate decreases firstly from 4.14×10-9 kg/(N·m) to 1.35×10-9 kg/(N·m),then increases to 2.36×10-9 kg/(N·m).The best comprehensive mechanical and tribological properties can be obtained between 10% and 12% h-BN addition.展开更多
Ni Fe2O4 ceramics were prepared in different sintering atmospheres. The phase compositions, microstructures and mechanical properties were studied. The results show that the stoichiometric compound Ni Fe2O4 cannot be ...Ni Fe2O4 ceramics were prepared in different sintering atmospheres. The phase compositions, microstructures and mechanical properties were studied. The results show that the stoichiometric compound Ni Fe2O4 cannot be obtained in vacuum or atmospheres with oxygen contents of 2×10-5, 2×10-4 and 2×10-3, respectively. All the samples sintered in above-mentioned atmospheres contain phases of Ni Fe2O4 and Ni O. With increasing oxygen content, Ni Fe2O4 content in the ceramic increases, while Ni O content appears a contrary trend. In vacuum, Ni Fe2O4 ceramic has average grain size of 3.94 μm, and bending strength of85.12 MPa. The changes of the phase composition and mechanical properties of Ni Fe2O4 based cermets are mainly caused by the alteration of their properties of Ni Fe2O4 ceramic.展开更多
This study was undertaken to determine the bending strength properties of off-cut Yellow Meranti wood by applying the finger jointed techniques. The finger orientations that were used in this study are vertical and ho...This study was undertaken to determine the bending strength properties of off-cut Yellow Meranti wood by applying the finger jointed techniques. The finger orientations that were used in this study are vertical and horizontal finger orientation. Specimens were bonded with PVAc (polyvinyl acetate). The bending strength properties were determined by the three point and four point bending test method. The results show that vertical finger orientation has the higher mean of modulus of rupture and the modulus of elasticity value of 24.49 MPa (28.91 MPa) and 8,814 MPa (11,668 MPa) respectively. However, the tested specimen properties did not meet the minimum strength of the solid (control) specimens.展开更多
文摘The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show that the quench sensitivity of 6063 alloy is lower than that of 6061 or 6082 alloy,and the critical temperature ranges from 300 to 410℃ with the nose temperature of about 360℃.From TEM analysis,heterogeneous precipitate β-Mg2Si is prior to nucleate on the(AlxFeySiz) dispersoids in the critical temperature range,and grows up most rapidly at the nose temperature of 360℃.The heterogeneous precipitation leads to a low concentration of solute,which consequently reduces the amount of the strengthening phase β'' after aging.In the large-scale industrial production of 6063 alloy,the cooling rate during quenching should be enhanced as high as possible in the quenching sensitive temperature range(410-300℃) to suppress the heterogeneous precipitation to get optimal mechanical properties,and it should be slowed down properly from the solution temperature to 410℃ and below 300℃ to reduce the residual stress.
文摘The post buckling strength of web plate of I section plate girders is considered to resist the shear force in many other countries code for design of steel structures,while it has not been considered in the Chinese code GB J17-88.For the code revising,some important conclusions have been drawn through the theoretical analysis and experimental research of the post buckling strength of web plate of I section plate girders.
基金National Natural Science Foundation of China(No.61271357)International S&T Cooperation Program of Shanxi Province(No.2013081035)
文摘The gradient image is always sensitive to noise in image detail enhancement. To overcome this shortage, an improved detail enhancement algorithm based on difference curvature and contrast field is proposed. Firstly, the difference curvature is utilized to determine the amplification coefficient instead of the gradient. This new amplification function of the difference curvature takes more neighboring points into account, it is therefore not sensitive to noise. Secondly, the contrast field is nonlinearly amplified according to the new amplification coefficient. And then, with the enhanced contrast field, we construct the energy functional. Finally, the enhanced image is reconstructed by the variational method. Experimental results of standard testing image and industrial X-ray image show that the proposed algorithm can perform well on increasing contrast and sharpening edges of images while suppressing noise at the same time.
基金Project(SS2015AA031101)supported by the National High-tech R&D Program of China
文摘A new composite structure based on aluminum foam sandwich and fiber metal laminate was proposed. A layer of glass fiber was provided at the interface between the metal panel and the aluminum foam core in this composite structure, using adhesive technology to bond the materials together by organic glue in the sequence of metal panel, glass fiber, aluminum foam core, glass fiber and metal panel. The experimental results show that the new composite structure has an improved comprehensive performance compared with the traditional aluminum foam sandwiches. The optimized parameters for the fabrication of the new aluminum foam composite structure with best bending strength were obtained. The epoxy resin and low porosity aluminum foams are preferred, the thickness of aluminum sheets should be at least 1.5 mm, and the type of glass fiber has little effect on the bending strength. The main failure modes of the new composite structures with two types of glues were discussed.
基金Supported by National Natural Scientific Fund Program(31371554)Jiangsu Innovation Fund(CX[(12)1003])+1 种基金Major National Program of Genetic Modified Food(2014ZX-08001-004-001-009)Jiangsu Natural Scientific Fund(BK20130708)~~
文摘A good quality, high yield, slow mature and middle season Japonica rice variety, Nanjing 9108 and its parents Guandong 194 and Wuxiangjing 14,were taken as the materials for the study. The growth and photosynthetic characteristics of the rice plants at the post-flowering stage were compared and the rice yield components were examined at harvest. The results showed that as compared with Wuxiangjing 14, the per plant yield of Nanjing 9108 was 7.70% higher, and much higher than that of Guandong194. The large total grain per plant and heavy grain weigh of Nanjing 9108 were the important structure basis for its yield. Further analysis o the growth indicators showed that Nanjing 9108 had a large leaf area of upper three green leaves area and a smaller leaf base angle in the third leaf from the bottom blades, which helped get a higher photosynthetic capacity in groups. On the14 thday after flowering, Nanjing 9108 had similar value of net photosynthetic rate(Pn) to that of Wuxianjing 14, but lower than that of Guandong 194. Viewing from the parameters obtained from light response of photosynthesis on the modified model of rectangular hyperbola, Pn of Nanjing 9108 was more aptated to be saturated by light intensity and sensitive to photoinhibition. On the whole, Nanjing 9108 with high yield mainly resulted from its good plant type, grain structure and higher photosynthetic capacity in groups. Further improving its photosynthetic capacity o single leaf in Nanjing 9108 would be an important way for its super high yield po tential in the future.
基金Project (51374039) supported by the National Natural Science Foundation of ChinaProject (613135) supported by National Security Basic Research Program of China
文摘Si/Al composites with different Si contents for electronic packaging were prepared by spark plasma sintering (SPS) technique. Properties of the composites were investigated, including density, thermal conductivity, coefficient of thermal expansion and flexural strength. The effects of the Si content on microstructure and thermal and mechanical properties of the composites were studied. The results show that the Si/Al composites consist of Si and Al components and Al uniformly distributes among Si grains. The relative density of the Si/Al composites gradually increases with the decrease of Si content and reaches 98.0% when the Si content is 50%. The thermal conductivity, the coefficient of thermal expansion and the flexural strength of the composite all decrease with the increase of the Si content, and an optimal matching of them is obtained when the Si content is 60%(volume fraction).
文摘Equal channel angular pressing(ECAP)is one of the most effective processes to produce ultra-fine grain(UFG)and nanocrystalline(NC)materials.Because the commercially pure titanium exhibits excellent biocompatibility properties,it has a significant potential to be utilized as an implant material.The low static and dynamic strengths of the pure titanium are one of the weaknesses of this material.This defect can be removed by applying the ECAP process on the pure titanium.In this work,the commercially pure titanium Grade2(CP-Ti of Grade2)was pressed at room temperature by the ECAP process via a channel angle of135°for3passes.The microstructural analysis and mechanical tests such as tensile test,hardness test,three-point bending test and Charpy impact test were all carried out on the ECAPed CP-Ti through3passes.The microstructural evolution reveals that by applying the ECAP process,coarse grain(CG)structure develops to UFG/NC structure.Moreover,the results of the mechanical tests show that the process significantly increases the yield and ultimate tensile strengths,bending strength,hardness and fracture toughness of the commercially pure titanium so that it can be used as a replacement for metallic alloys used as biomaterials.
基金Project(51202296) supported by the National Natural Science Foundation of China
文摘To obtain porous alumina ceramic with high strength,a novel gelcasting system based on 2-hydroxyethyl methacrylate(HEMA)dissolved in tert-butyl alcohol(TBA)was developed.The polymerization of the HEMA-TBA gelcasting system,the thermal behavior of obtained green body,and the microstructures and mechanical properties of the sintered bodies were investigated by rheometer,TG-DSC,SEM and bending strength testing,respectively.The results show that,(1)10 mg/mL of the initiator(benzoyl peroxide)is the optimal amount for polymerization of this gelscasting system at 25 ℃;(2)The alumina suspension of the HEMA-TBA gelcasting system showing shear-thinning behavior is sufficiently low for gelcasting process;(3)The bending strength of porous alumina ceramic samples,whose porosities range from 42% to 56%,is from(8±0.5)to(91±4.5)MPa.
基金TheDevelopingFoundationofShanghaiScienceandTechnologyCommittee (No .9944 190 2 7) .
文摘A positioning volume ellipsoid method is proposed to represent tumor volume in the workspace of a high-intensity-focused ultrasound (HIFU) surgery platform during the platform's positioning motion. To this simplified tumor model, a nearest neighbor search method is used to determine intermediate configuration and goal configuration, which the treatment head and ultrasound focus must pass in their localization to target volume. Based on the decided configurations, the continuity condition of combined Bezier curve in Euclidean space and De Casteljau algorithm on Lie group SO(3) are integrated to construct a combined Bezier positioning path of C2 continuity at junctional configuration, and an illustration of different positioning path planning is analyzed based on a liver tumor case.
基金Project(50872052) supported by the National Natural Science Foundation of ChinaProject(2009AA05Z313) supported by the National High Technology Research and Development Program of ChinaProject supported by the Commission of Science,Technology and Industry for National Defence,China
文摘Aiming at developing novel microwave-transparent ceramics with low dielectric loss, high thermal conductivity and high strength, Si3Na-AIN (30%, mass fraction) composite ceramics with La203 as sintering additive were prepared by hot-pressing at 1 800 ℃ and subsequently annealed at 1 450 ℃ and 1 850 ℃ for 2 h and 4 h, respectively. The materials were characterized by XRD and SEM. The effect of annealing process on the phase composition, sintering performance, microstructure, bending strength, dielectric loss and thermal conductivity of the materials was investigated. The results showed that both annealing at 1 850 ℃ and 1 450 ℃ promoted the phase transformation of α-Si3N4 to β-Si3N4. After annealing at 1 850 ℃, grain growth to a certain extent occurred in the materials. Especially, the elongated β-Si3N4 grains showed a slight increase in diameter from 0.2 μm to 0.6 μm approximately and a decrease in aspect ratio. As a result, as the annealing time increased to 4 h, the bending strength declined from 456 MPa to 390 MPa, whereas the dielectric loss decreased to 2.15× 10^-3 and the thermal conductivity increased to 16.3 W/(m.K) gradually. When annealed at 1 450 ℃, increasing the annealing time to 4 h significantly promoted the crystallization of glassy phase to La2Si6N803 phase in the materials, which led to the increase in bending strength to 619 MPa and thermal conductivity to 15.9 W/(m·K), respectively, and simultaneously the decrease in dielectric loss to 1.53× 10^-3.
文摘One of the key problems by diffusion-rolling bonding with small reduction for carbon steel plates is the bonding assistant coat. Abonding assitant coat used below 850℃ was developed. It contained copper as basic element and zinc as main alloy element. Other small elements and rear metals were added to decrease the melting point and to obtain a better clouding and bigh plasticity. Based on the theory of brazing and transient liquid diffusion welding, two carbon steel plates were rolled with small reduction by using self-made bonding assistant coat. Temperature, pressure and holding time are the main technology parameters for controlling the process of diffusion-rolling. The results show that the bonding strength is the greatest when the bonding temperature is 830℃, holding time is 3 min and the reduction rate is 9%.
基金Project supported by the Indian Council for Cultural Relations,India
文摘This paper reports investigation conducted to study the fatigue performance of steel fibre reinforced concrete (SFRC) containing fibres of mixed aspect ratio. An extensive experimental program was conducted in which 90 flexural fatigue tests were carried out at different stress levels on size 500 mm×100 mm×100 mm SFRC specimens respectively containing 1.0%, 1.5% and 2.0% volume fraction of fibres. About 36 static flexural tests were also conducted to determine the static flexural strength prior to fatigue testing. Each volume fraction of fibres incorporated corrugated mixed steel fibres of size 0.6 mm×2.0 mm×25 mm and 0.6 mm×2.0 mm×50 mm in ratio 50:50 by weight. The results are presented both as S-N relationships, with the maximum fatigue stress expressed as a percentage of the strength under static loading, and as relationships between actually applied fatigue stress and number of loading cycles to failure. Two-million-cycle fatigue strengths of SFRC containing different volume fractions of mixed fibres were obtained and compared with plain concrete.
基金Project (2007K06-13) supported by the Science and Technique Research and Development Program of Shaanxi Province, China
文摘Zirconia/stainless steel (ZrO2/SUS316L) functionally graded materials (FGMs) were fabricated by tape casting and laminating. Microstructures of FGMs were observed by optical microscope. Fracture behavior of FGMs in different loading modes and influences of different gradient changes on flexural strength were investigated. The results show that ZrO2/ SUS316L FGMs with graded components at interlayers are obtained after they are sintered in vacuum and pressureless condition at 1 350 ℃. TheⅠ?Ⅱ mixed mode crack creates in composite layer and grows to both sides zigzag while loading on ZrO2 layer. Flexural strengths are 496.4,421.7 and 387.5 MPa when gradient changes are 10%,15% and 20%,but flexural strengths of the corresponding fracture layers are 387.1,334.6 and 282.3 MPa since cracks of FGMs are affected by three-dimensional stress,respectively. The cracks are generated in ZrO2 layer and extend to SUS316L layer while loading is added on SUS316L layer,flexural strength does not change with the graded components and keeps consistent basically.
基金Project(MKPT-03-182) supported by the Ministry of Science and Technology of China
文摘Ni-Cr/h-BN self-lubricating composities were prepared by powder metallurgy (P/M) method.The effects of hexagonal boron nitride (h-BN) content on the mechanical and tribological properties of the Ni-Cr/h-BN composites were investigated.The corresponding frictional models were established to analyze the formation of the lubricant h-BN films on the surfaces of the Ni-Cr/h-BN composites.The results show that,when the content of h-BN increases from 5% to 15% (mass fraction),the bending strength of the Ni-Cr/h-BN composite decreases from 96.670 MPa to 17.319 MPa,and the hardness (HB) decreases from 33 to 14.The friction coefficient of the Ni-Cr/h-BN composite decreases firstly from 0.385 to 0.216,and then increases to 0.284,while the wear rate decreases firstly from 4.14×10-9 kg/(N·m) to 1.35×10-9 kg/(N·m),then increases to 2.36×10-9 kg/(N·m).The best comprehensive mechanical and tribological properties can be obtained between 10% and 12% h-BN addition.
基金Project(2008AA030503)supported by the National High Technology Research and Development Program of ChinaProject(51474238)supported by the National Natural Science Foundation of China
文摘Ni Fe2O4 ceramics were prepared in different sintering atmospheres. The phase compositions, microstructures and mechanical properties were studied. The results show that the stoichiometric compound Ni Fe2O4 cannot be obtained in vacuum or atmospheres with oxygen contents of 2×10-5, 2×10-4 and 2×10-3, respectively. All the samples sintered in above-mentioned atmospheres contain phases of Ni Fe2O4 and Ni O. With increasing oxygen content, Ni Fe2O4 content in the ceramic increases, while Ni O content appears a contrary trend. In vacuum, Ni Fe2O4 ceramic has average grain size of 3.94 μm, and bending strength of85.12 MPa. The changes of the phase composition and mechanical properties of Ni Fe2O4 based cermets are mainly caused by the alteration of their properties of Ni Fe2O4 ceramic.
文摘This study was undertaken to determine the bending strength properties of off-cut Yellow Meranti wood by applying the finger jointed techniques. The finger orientations that were used in this study are vertical and horizontal finger orientation. Specimens were bonded with PVAc (polyvinyl acetate). The bending strength properties were determined by the three point and four point bending test method. The results show that vertical finger orientation has the higher mean of modulus of rupture and the modulus of elasticity value of 24.49 MPa (28.91 MPa) and 8,814 MPa (11,668 MPa) respectively. However, the tested specimen properties did not meet the minimum strength of the solid (control) specimens.