采用高效液相色谱-串联质谱(HPLC-MS/MS)技术研究了新型反相分配和强阳离子交换固相萃取柱的性能,确定了该新型固相萃取柱的最佳p H值、最佳流速、最大吸附容量及饱和吸附容量。研究了新型固相萃取柱对三聚氰胺在不同起始浓度下的吸附...采用高效液相色谱-串联质谱(HPLC-MS/MS)技术研究了新型反相分配和强阳离子交换固相萃取柱的性能,确定了该新型固相萃取柱的最佳p H值、最佳流速、最大吸附容量及饱和吸附容量。研究了新型固相萃取柱对三聚氰胺在不同起始浓度下的吸附动力学和不同温度下的吸附热力学性能,并对吸附等温线数据进行了拟合。结果显示:该新型固相萃取柱的最佳吸附p H值为5.0,最佳流速为1.0 m L/min,最佳洗脱体积为1.0 m L,最大吸附量为900μg。30℃下该萃取柱的饱和吸附容量为81.45μg/mg。该吸附过程符合准二级动力学吸附模型,吸附等温线符合Langmuir吸附模型,且该过程为自发进行的吸热反应。展开更多
The thermal behavior of a thick transversely isotropic FGM rectangular plate was investigated within the scope of three-dimensional elasticity. Noticing many FGMs may have temperature-dependent properties, the materia...The thermal behavior of a thick transversely isotropic FGM rectangular plate was investigated within the scope of three-dimensional elasticity. Noticing many FGMs may have temperature-dependent properties, the material constants were further considered as functions of temperature. A solution method based on state-space formulations with a laminate approximate model was proposed. For a thin plate, the method was clarified by comparison with the thin plate theory. The influences of material inhomogeneity and temperature-dependent characteristics were finally discussed through numerical examples.展开更多
This paper is an analysis of a sourcebook using Neuro-Linguistic Programming technique. The main objective is to determine the effectiveness of the sourcebook in teaching English as a second language. Specifically, it...This paper is an analysis of a sourcebook using Neuro-Linguistic Programming technique. The main objective is to determine the effectiveness of the sourcebook in teaching English as a second language. Specifically, it aimed to know the visual materials, aural presentations, and semi-abstract thoughts that would encourage the learners to actively participate in classroom discussions; the methods to be adapted; and the steps involved in the preparation of the sourcebook. It was found that most student-respondents strongly react to pictures, to feelings and sensations, and to ideas. The sourcebook must be prepared in the form of a content-based instructional material. It must include drills that would give ample approaches to develop among the learners good sense of collaborative learning, integrative global language proficiency, and contextual communicative competence in meaningful situations. Moreover, the sourcebook must use both print and non-print teaching aids as supporting materials.展开更多
There has been a strong interest in the use of Phase Change Materials (PCMs) for the transient thermal abatement of high powered microprocessor.This paper presents a set of transient computational analysis for selecte...There has been a strong interest in the use of Phase Change Materials (PCMs) for the transient thermal abatement of high powered microprocessor.This paper presents a set of transient computational analysis for selected IC packages with the purpose of calibrating the merits of PCM in different configurations.The transient analysis of high powered microprocessors with heat sinks was performed as a benchmark for comparison with the same microprocessors fitted with PCM in the following configurations:a) PCM imbedded into the finned region of the heat sink,b) PCM mounted between the microprocessor and heat sink,c) sealed PCM underfill to the microprocessor and d) PCM fitted to the underside of the printed circuit board directly beneath the microprocessor.The analysis was performed using a commercial CFD tool together with an approximation to the phase change mechanism using the slope method.Results indicate the merit of each configuration.展开更多
文摘采用高效液相色谱-串联质谱(HPLC-MS/MS)技术研究了新型反相分配和强阳离子交换固相萃取柱的性能,确定了该新型固相萃取柱的最佳p H值、最佳流速、最大吸附容量及饱和吸附容量。研究了新型固相萃取柱对三聚氰胺在不同起始浓度下的吸附动力学和不同温度下的吸附热力学性能,并对吸附等温线数据进行了拟合。结果显示:该新型固相萃取柱的最佳吸附p H值为5.0,最佳流速为1.0 m L/min,最佳洗脱体积为1.0 m L,最大吸附量为900μg。30℃下该萃取柱的饱和吸附容量为81.45μg/mg。该吸附过程符合准二级动力学吸附模型,吸附等温线符合Langmuir吸附模型,且该过程为自发进行的吸热反应。
文摘The thermal behavior of a thick transversely isotropic FGM rectangular plate was investigated within the scope of three-dimensional elasticity. Noticing many FGMs may have temperature-dependent properties, the material constants were further considered as functions of temperature. A solution method based on state-space formulations with a laminate approximate model was proposed. For a thin plate, the method was clarified by comparison with the thin plate theory. The influences of material inhomogeneity and temperature-dependent characteristics were finally discussed through numerical examples.
文摘This paper is an analysis of a sourcebook using Neuro-Linguistic Programming technique. The main objective is to determine the effectiveness of the sourcebook in teaching English as a second language. Specifically, it aimed to know the visual materials, aural presentations, and semi-abstract thoughts that would encourage the learners to actively participate in classroom discussions; the methods to be adapted; and the steps involved in the preparation of the sourcebook. It was found that most student-respondents strongly react to pictures, to feelings and sensations, and to ideas. The sourcebook must be prepared in the form of a content-based instructional material. It must include drills that would give ample approaches to develop among the learners good sense of collaborative learning, integrative global language proficiency, and contextual communicative competence in meaningful situations. Moreover, the sourcebook must use both print and non-print teaching aids as supporting materials.
文摘There has been a strong interest in the use of Phase Change Materials (PCMs) for the transient thermal abatement of high powered microprocessor.This paper presents a set of transient computational analysis for selected IC packages with the purpose of calibrating the merits of PCM in different configurations.The transient analysis of high powered microprocessors with heat sinks was performed as a benchmark for comparison with the same microprocessors fitted with PCM in the following configurations:a) PCM imbedded into the finned region of the heat sink,b) PCM mounted between the microprocessor and heat sink,c) sealed PCM underfill to the microprocessor and d) PCM fitted to the underside of the printed circuit board directly beneath the microprocessor.The analysis was performed using a commercial CFD tool together with an approximation to the phase change mechanism using the slope method.Results indicate the merit of each configuration.
