Betulin, which is a medicinal pentacyclic triterpene, is abundant in the bark of white birch (Betula platyphlly). The bark of birch was collected at Tayuan Forest Farm of Jiagedaqi, Heilongjiang Province in September ...Betulin, which is a medicinal pentacyclic triterpene, is abundant in the bark of white birch (Betula platyphlly). The bark of birch was collected at Tayuan Forest Farm of Jiagedaqi, Heilongjiang Province in September 2000. Supercritical fluid extraction (SFE) that is a new separation technology has been used for the processing pharmaceutical and natural products. In this paper, the extraction of betulin from the bark of birch by supercritical CO2 extraction was studied. The authors investigated and analyzed a few parameters such as modifier dosage, extraction pressure and extraction temperature. The optimal extrac-tion conditions showed that the modifier dosage used for per gram bark powder was 1.5 mL, the extraction pressure was at 20 Mpa, and the extraction temperature was at 55 C. The velocity of flow of liquid CO2 was at 10 kg/h. The pressure and tem-perature in separation vessel were at 5.5 Mpa and 50 C, respectively.展开更多
A heated air circulation standard curing barn was used for baking tobacco leaves, and the effects of different yellowing conditions during the baking process on contents of neutral aroma components and smoking quality...A heated air circulation standard curing barn was used for baking tobacco leaves, and the effects of different yellowing conditions during the baking process on contents of neutral aroma components and smoking quality of upper leaves were studied by setting different yellowing time and color-fixing time. The results showed that during the baking process, only by prolonging the yellowing time by 24 h on the basis of control, the content of every kind of neutral aroma components in- creased obviously and the content of solanone increased by nearly 2.20 times. It was unfavorable for the degradation and accumulation of aroma components when only prolonging color-fixing time by 24 h. Prolonging both yellowing time and color- fixing time by 24 h mainly promoted the accumulation of chlorophyll degradation product neophytadiene, which increased by 33.24%, while the degradation and ac- cumulation of some aroma components were inhibited, indicating that only prolonging the yellowing time by 24 h could promote the accumulation of various kinds of neu- tral aroma components and improve the quality of tobacco leaves. The regression models were established of neutral aroma components in the first and second prin- cipal components to total aroma content, which were y=x+0.053 47 (R^2=0.919 7) and y=x+0.147 5 (R^2=0.698 4), respectively, and they were verified to be feasible.展开更多
[Objective] The aim was to analyze sugar components in fermented rice wine by ion chromatography. [Method] The optimal condition for chromatography system of sugar analysis was selected by measuring sugars in fermente...[Objective] The aim was to analyze sugar components in fermented rice wine by ion chromatography. [Method] The optimal condition for chromatography system of sugar analysis was selected by measuring sugars in fermented rice wine with ion chromatography and pulsed amperometric detection. [Result] The optimal measurement conditions were as follows: Leacheate (Leachate), consisting of NaOH and CH3COONa, was eluted by gradient concentrations, with column temperature at 35 ℃ and flow rate at 0.4 ml/min. In the condition, sugars in rice wine were ana- lyzed and the results showed that the method is featured by low detection limit, good repetition and high recovery rate. [Conclusion] The research establishes and determines the approaches and optimum conditions for sugar analysis in rice wine by ion chromatography and pulsed amperometric detection, providing references for advancement of research on quality improvement of fermented rice wine.展开更多
In this paper, we define a new class of biased linear estimators of the vector of unknown parameters in the deficient_rank linear model based on the spectral decomposition expression of the best linear minimun bias es...In this paper, we define a new class of biased linear estimators of the vector of unknown parameters in the deficient_rank linear model based on the spectral decomposition expression of the best linear minimun bias estimator. Some important properties are discussed. By appropriate choices of bias parameters, we construct many interested and useful biased linear estimators, which are the extension of ordinary biased linear estimators in the full_rank linear model to the deficient_rank linear model. At last, we give a numerical example in geodetic adjustment.展开更多
Conventional shot-gather migration uses a cross-correlation imaging condition proposed by Clarebout (1971), which cannot preserve imaging amplitudes. The deconvolution imaging condition can improve the imaging ampli...Conventional shot-gather migration uses a cross-correlation imaging condition proposed by Clarebout (1971), which cannot preserve imaging amplitudes. The deconvolution imaging condition can improve the imaging amplitude and compensate for illumination. However, the deconvolution imaging condition introduces instability issues. The least-squares imaging condition first computes the sum of the cross-correlation of the forward and backward wavefields over all frequencies and sources, and then divides the result by the total energy of the forward wavefield. Therefore, the least-squares imaging condition is more stable than the classic imaging condition. However, the least-squares imaging condition cannot provide accurate results in areas where the illumination is very poor and unbalanced. To stabilize the least-squares imaging condition and balance the imaging amplitude, we propose a novel imaging condition with structure constraints that is based on the least-squares imaging condition. Our novel imaging condition uses a plane wave construction that constrains the imaging result to be smooth along geological structure boundaries in the inversion frame. The proposed imaging condition improves the stability of the imaging condition and balances the imaging amplitude. The proposed condition is applied to two examples, the horizontal layered model and the Sigsbee 2A model. These tests show that, in comparison to the damped least-squares imaging condition, the stabilized least-squares imaging condition with structure constraints improves illumination stability and balance, makes events more consecutive, adjusts the amplitude of the depth layers where the illumination is poor and unbalanced, suppresses imaging artifacts, and is conducive to amplitude preserving imaging of deep layers.展开更多
Olivine phenocryst compositions and whole-rock chemical compositions are used to identify primitive picrite basalts from the early part of flood basalt successions in the western part of the Emeishan large igneous pro...Olivine phenocryst compositions and whole-rock chemical compositions are used to identify primitive picrite basalts from the early part of flood basalt successions in the western part of the Emeishan large igneous province (ELIP), southwestern China. The Fo contents of olivine phenocrysts of komatiites with MgO-21.79 wt% range from 85.2% to 91.4%. The composition of unerupted parental melts is calculated from the compositions of the most Fo-rich olivine phenocrysts. These melts had -22 wt% MgO, and originated in mantle with a potential temperature of -1600℃ and at about 4.2 GPa pressure, supporting the conclusion that the generation of ELIP can be attributed to melting of a plume head beginning at -138 km depth.展开更多
Two-dimensional tidal open boundary conditions of the M2 constituent in the Bohai and Yellow Seas(BYS) have been estimated by assimilating T/P altimeter data.During inversion,independent point(IP) strategy was used,in...Two-dimensional tidal open boundary conditions of the M2 constituent in the Bohai and Yellow Seas(BYS) have been estimated by assimilating T/P altimeter data.During inversion,independent point(IP) strategy was used,in which several IPs on the open boundary is assumed,values at these IPs can be optimized with an adjoint method,and those at other grid points are determined by linearly interpolating the values at IPs.The reasonability and feasibility of the model are tested by ideal twin experiments.In the practical experiment(PE) after assimilation,the cost function may reach 1% or less of its initial value.Mean absolute errors in amplitude and phase can be less than 5 cm and 5°,respectively,and the obtained co-chart can show the character of the M2 constituent in the BYS.The results of the PE indicate that using only two IPs on the open boundary can yield better simulated results.展开更多
Various conditions were investigated in detail for the novel organic template-free static hydrothermal synthesis of SUZ-4 zeolite in the presence of seeds. The obtained samples were characterized by XRD (X-ray diffra...Various conditions were investigated in detail for the novel organic template-free static hydrothermal synthesis of SUZ-4 zeolite in the presence of seeds. The obtained samples were characterized by XRD (X-ray diffraction), SEM (scanning electron microscope), TG (thermal gravimetric analysis), ICP (inductively coupling plasma) elemental analysis, nitrogen sorption isotherm and surface area. The results show that pure SUZ-4 zeolites with high crystallinity are obtained in a broad window of synthesis conditions: seed mass concentration 0.2%-2%, SIO2/A1203 molar ratio 21 25, KOH/SiO2 molar ratio 0.33 0.43, H20/SiO2 molar ratio 7.14-38.1, aging time 24 h, crystallization temperature 160℃, and crystallization time 6-10 d. Also, crystallinity and size of the rod-like SUZ-4 zeolite crystals are found to alter with the conditions.展开更多
Unconditionally secure signature is an important part of quantum cryptography. Usually, a signature scheme only provides an environment for a single signer. Nevertheless, in real applications, many signers may collabo...Unconditionally secure signature is an important part of quantum cryptography. Usually, a signature scheme only provides an environment for a single signer. Nevertheless, in real applications, many signers may collaboratively send a message to the verifier and convince the verifier that the message is actually transmitted by them. In this paper, we give a scalable arbitrated signature protocol of classical proved to be secure even with a compromised arbitrator. messages with multi-signers. Its security is analyzed and proved to be secure even with a compromised arbitrator.展开更多
By using a degree-day based distributed hydrological model, regimes of glacial runoff from the Koxkar glacier during 2007-2011 are simulated, and variations and characteristics of major hydrological components are dis...By using a degree-day based distributed hydrological model, regimes of glacial runoff from the Koxkar glacier during 2007-2011 are simulated, and variations and characteristics of major hydrological components are discussed. The results show that the meltwater runoff contributes 67.4%, of the proglacial discharge, out of which snowmelt, clean ice melting, buried-ice ablation and ice-cliff backwasting account for 22.4%, 21.9%, 17.9% and 5.3% of the total melt runoff, respectively. Rainfall runoff is significant in mid-latitude glacierized mountain areas like Tianshan and Karakorum. In the Koxkar glacier catchment, about 11.5% of stream water is initiated from liquid precipitation. Spatial distributions for each glacial runoff component reveal the importance of climatic gradients, local topography and morphology on glacial runoff generation, and temporal variations of these components is closely related to the annual cycle of catchment meteorology and glacier storage. Four stages are recognized in the seasonal variations of glacier storage, reflecting changes in meltwater yields, meteorological conditions and drainage systems in the annual hydrological cycle.展开更多
Fish sauce is a kind of condiments processed from fish. The L9(34) orthogonal tests have been carried out to inspect the effects of technological conditions for fermentation on the comprehensive quality of fish sauc...Fish sauce is a kind of condiments processed from fish. The L9(34) orthogonal tests have been carried out to inspect the effects of technological conditions for fermentation on the comprehensive quality of fish sauce. The conditions of the orthogonal tests are following: the fermentation temperature takes values of 35℃, 40℃ and 45℃, the percentage of Koji values of 40%, 20% and 10% and the percentage of salt values of 10%, 14% and 18%. The obtained experimental results indicate that fermentation temperature plays an important role in the improvement of sauce quality. The optimal technological conditions for sauce fermentation are of 10% salt, 45℃ and 40% koji mixed. The composition of fish sauce processed from offal of silver carp-surimi processing under the above-mentioned conditions and two commercial products have been analyzed. The results show that fish sauce processed from fish offal is nutritious and delicious. It is suggested that the fermentation of fish sauce is a potential and promising pathway to make full use of freshwater fish resources and offal in fish processing. In this study, fuzzy theory and analytic hierarchy process have been applied and the quality evaluation has been established by the combination of physico-chemical indices and sensory evaluation. The comprehensive evaluation has been taken to reflect the optimal factors for the process of sauce fermentation. The quality indexes for fish sauce contain sensory evaluation, amino nitrogen, total nitrogen, specific gravity, volatile basic nitrogen, salt concentration, brown index and acidity, represented by y1, y2, y3, y4, y5, y6, y7, y8, and y9, respectively. They form a group U= {y1, y2, y3, y4, y5, y6, y7, y8, y9,}. Using the fuzzy functions, the values of all these factors are transformed into fuzzy degrees of single factor, i.e. numerical values between 0 and 1. The fuzzy degrees of single factor in several samples are made up a matrix R. Following that, a weight of each index can be determined in the comprehensive evaluation. In the analytic hierarchy process, the weight can be obtained by the cross comparison between two different factors. The results show that the weights (W) of sensory evaluation, amino nitrogen, total nitrogen, specific gravity, volatile basic nitrogen, salt concentration, brown index and acidity are 0.356, 0.189, 0.107, 0.054, 0.097, 0.063, 0.061 and 0.073 respectively. Finally the aggregated fuzzy degree (B) of different samples is computed by B=W·R, which can be taken as the final result of comprehensive evaluation. The larger this value is, the higher the quality of sauce product would be.展开更多
High enzymatic activity is required for laccase applications.Central composite design (CCD)-based response surface methodology (RSM) can effectively increase the enzymatic activity of Pleurotus ostreatus P40 in li...High enzymatic activity is required for laccase applications.Central composite design (CCD)-based response surface methodology (RSM) can effectively increase the enzymatic activity of Pleurotus ostreatus P40 in liquid substrate fermentation.Initial screening of the nutritional components was performed using a Plackett-Burman design.The variables,namely,bran,bagasse,Tween 80,and yeast extract,were found to have statistically significant effects on laccase activity.These variables were further optimized using CCD-based RSM.Optimal concentrations for the maximum laccase activity were 8.144 2 g/L bran,50 g/L bagasse,0.424 1 mL/L Tween 80,and 2.832 5 g/L yeast extract.Under optimized conditions,the maximum measured laccase activity reached 96 480 U/L,which was close to the predicted value (104 830 U/L) by RSM.Therefore,RSM can be used to optimize culture components for laccase activity from Pieurotus ostreatus P40.展开更多
Model integration is an important section of the model management research area. The paper puts forward a formalization representation of model, and presents some concepts, such as the compound model re- lation, the c...Model integration is an important section of the model management research area. The paper puts forward a formalization representation of model, and presents some concepts, such as the compound model re- lation, the composite model and so on. Additionally, the existence of model integration is also analyzed in de- tail and several sufficient conditions are proved.展开更多
The influence of solvent (in its gaseous state) on the stability of crystallized organic compounds was investigated. Through two examples of studies on the solid/vapour equilibria made in our lab, several behaviors we...The influence of solvent (in its gaseous state) on the stability of crystallized organic compounds was investigated. Through two examples of studies on the solid/vapour equilibria made in our lab, several behaviors were highlighted: (i) a new hydrated phase (thermodynamically stable) of an active pharmaceutical ingredient (API) was detected after the recrystallization starting from a deliquescent state, (ii) a spontaneous resolution of a hydrated racemic compound towards an anhydrous conglomerate can occur during the desolvation under the precise conditions of temperature and humidity. This study illustrates that knowledge about solid/vapour equilibrium is a crucial step during the complete characterization of solid organic compounds.展开更多
Based on theoretical analysis, similarity simulation tests, numerical simulation analysis and field observations, we analyzed rock collapse and rules of fraction evolution of overlying rocks and studied the rules in c...Based on theoretical analysis, similarity simulation tests, numerical simulation analysis and field observations, we analyzed rock collapse and rules of fraction evolution of overlying rocks and studied the rules in controlling the effect of an extremely thick igneous rock, found above a main mining coal seam in an area prone to coal mine disasters in the Haizi Coal Mine. The results show that this igneous rock, called a "main key stratum", will not subside nor break for a long time, causing lower fractures and bed separations not to close. The presence of igneous rock plays an important role in rock bursts, mine floods, gas outburst and surface subsidence in coal mines. By analyzing the rules in controlling the effect of this igneous rock, we provide useful references for safety and high efficiency mining in coal mines under special geological conditions.展开更多
文摘Betulin, which is a medicinal pentacyclic triterpene, is abundant in the bark of white birch (Betula platyphlly). The bark of birch was collected at Tayuan Forest Farm of Jiagedaqi, Heilongjiang Province in September 2000. Supercritical fluid extraction (SFE) that is a new separation technology has been used for the processing pharmaceutical and natural products. In this paper, the extraction of betulin from the bark of birch by supercritical CO2 extraction was studied. The authors investigated and analyzed a few parameters such as modifier dosage, extraction pressure and extraction temperature. The optimal extrac-tion conditions showed that the modifier dosage used for per gram bark powder was 1.5 mL, the extraction pressure was at 20 Mpa, and the extraction temperature was at 55 C. The velocity of flow of liquid CO2 was at 10 kg/h. The pressure and tem-perature in separation vessel were at 5.5 Mpa and 50 C, respectively.
基金Supported by Major Special Project of Strong-flavor Characteristic High-quality Tobacco Development of China National Tobacco Company(110201101001 TS-01)China Tobacco Project of Jilin Province(JY2013001)~~
文摘A heated air circulation standard curing barn was used for baking tobacco leaves, and the effects of different yellowing conditions during the baking process on contents of neutral aroma components and smoking quality of upper leaves were studied by setting different yellowing time and color-fixing time. The results showed that during the baking process, only by prolonging the yellowing time by 24 h on the basis of control, the content of every kind of neutral aroma components in- creased obviously and the content of solanone increased by nearly 2.20 times. It was unfavorable for the degradation and accumulation of aroma components when only prolonging color-fixing time by 24 h. Prolonging both yellowing time and color- fixing time by 24 h mainly promoted the accumulation of chlorophyll degradation product neophytadiene, which increased by 33.24%, while the degradation and ac- cumulation of some aroma components were inhibited, indicating that only prolonging the yellowing time by 24 h could promote the accumulation of various kinds of neu- tral aroma components and improve the quality of tobacco leaves. The regression models were established of neutral aroma components in the first and second prin- cipal components to total aroma content, which were y=x+0.053 47 (R^2=0.919 7) and y=x+0.147 5 (R^2=0.698 4), respectively, and they were verified to be feasible.
基金Supported by Changsha Key Project in Hunan Province(K1005007-21)~~
文摘[Objective] The aim was to analyze sugar components in fermented rice wine by ion chromatography. [Method] The optimal condition for chromatography system of sugar analysis was selected by measuring sugars in fermented rice wine with ion chromatography and pulsed amperometric detection. [Result] The optimal measurement conditions were as follows: Leacheate (Leachate), consisting of NaOH and CH3COONa, was eluted by gradient concentrations, with column temperature at 35 ℃ and flow rate at 0.4 ml/min. In the condition, sugars in rice wine were ana- lyzed and the results showed that the method is featured by low detection limit, good repetition and high recovery rate. [Conclusion] The research establishes and determines the approaches and optimum conditions for sugar analysis in rice wine by ion chromatography and pulsed amperometric detection, providing references for advancement of research on quality improvement of fermented rice wine.
文摘In this paper, we define a new class of biased linear estimators of the vector of unknown parameters in the deficient_rank linear model based on the spectral decomposition expression of the best linear minimun bias estimator. Some important properties are discussed. By appropriate choices of bias parameters, we construct many interested and useful biased linear estimators, which are the extension of ordinary biased linear estimators in the full_rank linear model to the deficient_rank linear model. At last, we give a numerical example in geodetic adjustment.
基金financially supported by Important National Science and Technology Specific Projects of China(Grant No. 2011ZX05023-005-005)
文摘Conventional shot-gather migration uses a cross-correlation imaging condition proposed by Clarebout (1971), which cannot preserve imaging amplitudes. The deconvolution imaging condition can improve the imaging amplitude and compensate for illumination. However, the deconvolution imaging condition introduces instability issues. The least-squares imaging condition first computes the sum of the cross-correlation of the forward and backward wavefields over all frequencies and sources, and then divides the result by the total energy of the forward wavefield. Therefore, the least-squares imaging condition is more stable than the classic imaging condition. However, the least-squares imaging condition cannot provide accurate results in areas where the illumination is very poor and unbalanced. To stabilize the least-squares imaging condition and balance the imaging amplitude, we propose a novel imaging condition with structure constraints that is based on the least-squares imaging condition. Our novel imaging condition uses a plane wave construction that constrains the imaging result to be smooth along geological structure boundaries in the inversion frame. The proposed imaging condition improves the stability of the imaging condition and balances the imaging amplitude. The proposed condition is applied to two examples, the horizontal layered model and the Sigsbee 2A model. These tests show that, in comparison to the damped least-squares imaging condition, the stabilized least-squares imaging condition with structure constraints improves illumination stability and balance, makes events more consecutive, adjusts the amplitude of the depth layers where the illumination is poor and unbalanced, suppresses imaging artifacts, and is conducive to amplitude preserving imaging of deep layers.
文摘Olivine phenocryst compositions and whole-rock chemical compositions are used to identify primitive picrite basalts from the early part of flood basalt successions in the western part of the Emeishan large igneous province (ELIP), southwestern China. The Fo contents of olivine phenocrysts of komatiites with MgO-21.79 wt% range from 85.2% to 91.4%. The composition of unerupted parental melts is calculated from the compositions of the most Fo-rich olivine phenocrysts. These melts had -22 wt% MgO, and originated in mantle with a potential temperature of -1600℃ and at about 4.2 GPa pressure, supporting the conclusion that the generation of ELIP can be attributed to melting of a plume head beginning at -138 km depth.
基金Supported by the State Ministry of Science and Technology of China (Nos.2007AA09Z118,2008AA09A402)the National Natural Science Foundation of China(No.41076006)the Ministry of Education's 111 Project(No.B07036)
文摘Two-dimensional tidal open boundary conditions of the M2 constituent in the Bohai and Yellow Seas(BYS) have been estimated by assimilating T/P altimeter data.During inversion,independent point(IP) strategy was used,in which several IPs on the open boundary is assumed,values at these IPs can be optimized with an adjoint method,and those at other grid points are determined by linearly interpolating the values at IPs.The reasonability and feasibility of the model are tested by ideal twin experiments.In the practical experiment(PE) after assimilation,the cost function may reach 1% or less of its initial value.Mean absolute errors in amplitude and phase can be less than 5 cm and 5°,respectively,and the obtained co-chart can show the character of the M2 constituent in the BYS.The results of the PE indicate that using only two IPs on the open boundary can yield better simulated results.
基金Supported by the National Natural Science Foundation of China(20976084,21101094,21136005)
文摘Various conditions were investigated in detail for the novel organic template-free static hydrothermal synthesis of SUZ-4 zeolite in the presence of seeds. The obtained samples were characterized by XRD (X-ray diffraction), SEM (scanning electron microscope), TG (thermal gravimetric analysis), ICP (inductively coupling plasma) elemental analysis, nitrogen sorption isotherm and surface area. The results show that pure SUZ-4 zeolites with high crystallinity are obtained in a broad window of synthesis conditions: seed mass concentration 0.2%-2%, SIO2/A1203 molar ratio 21 25, KOH/SiO2 molar ratio 0.33 0.43, H20/SiO2 molar ratio 7.14-38.1, aging time 24 h, crystallization temperature 160℃, and crystallization time 6-10 d. Also, crystallinity and size of the rod-like SUZ-4 zeolite crystals are found to alter with the conditions.
基金Supported by the National High-Tech Research,Development Plan of China under Grant Nos.2006AA01Z440,2009AA012441,2009AA012437National Basic Research Program of China (973 Program 2007CB311100)+4 种基金the National Natural Science Foundation of China under Grant Nos.60873191 and 60821001Specialized Research Fund for the Doctoral Program of Higher Education under Grant Nos.20091103120014,20090005110010Beijing Natural Science Foundation under Grant Nos.1093015,1102004the Scientific Research Common Program of Beijing Municipal Commission of Education under Grant No.KM200810005004the ISN Open Foundation
文摘Unconditionally secure signature is an important part of quantum cryptography. Usually, a signature scheme only provides an environment for a single signer. Nevertheless, in real applications, many signers may collaboratively send a message to the verifier and convince the verifier that the message is actually transmitted by them. In this paper, we give a scalable arbitrated signature protocol of classical proved to be secure even with a compromised arbitrator. messages with multi-signers. Its security is analyzed and proved to be secure even with a compromised arbitrator.
基金supported by the Knowledge Innovation Program of the Chinese Academy of Sciences under Grant No. KZCX2-YW-GJ04National Nature Science Foundation of China (NSFC) under Grant Nos. 41130641 and 41271078
文摘By using a degree-day based distributed hydrological model, regimes of glacial runoff from the Koxkar glacier during 2007-2011 are simulated, and variations and characteristics of major hydrological components are discussed. The results show that the meltwater runoff contributes 67.4%, of the proglacial discharge, out of which snowmelt, clean ice melting, buried-ice ablation and ice-cliff backwasting account for 22.4%, 21.9%, 17.9% and 5.3% of the total melt runoff, respectively. Rainfall runoff is significant in mid-latitude glacierized mountain areas like Tianshan and Karakorum. In the Koxkar glacier catchment, about 11.5% of stream water is initiated from liquid precipitation. Spatial distributions for each glacial runoff component reveal the importance of climatic gradients, local topography and morphology on glacial runoff generation, and temporal variations of these components is closely related to the annual cycle of catchment meteorology and glacier storage. Four stages are recognized in the seasonal variations of glacier storage, reflecting changes in meltwater yields, meteorological conditions and drainage systems in the annual hydrological cycle.
文摘Fish sauce is a kind of condiments processed from fish. The L9(34) orthogonal tests have been carried out to inspect the effects of technological conditions for fermentation on the comprehensive quality of fish sauce. The conditions of the orthogonal tests are following: the fermentation temperature takes values of 35℃, 40℃ and 45℃, the percentage of Koji values of 40%, 20% and 10% and the percentage of salt values of 10%, 14% and 18%. The obtained experimental results indicate that fermentation temperature plays an important role in the improvement of sauce quality. The optimal technological conditions for sauce fermentation are of 10% salt, 45℃ and 40% koji mixed. The composition of fish sauce processed from offal of silver carp-surimi processing under the above-mentioned conditions and two commercial products have been analyzed. The results show that fish sauce processed from fish offal is nutritious and delicious. It is suggested that the fermentation of fish sauce is a potential and promising pathway to make full use of freshwater fish resources and offal in fish processing. In this study, fuzzy theory and analytic hierarchy process have been applied and the quality evaluation has been established by the combination of physico-chemical indices and sensory evaluation. The comprehensive evaluation has been taken to reflect the optimal factors for the process of sauce fermentation. The quality indexes for fish sauce contain sensory evaluation, amino nitrogen, total nitrogen, specific gravity, volatile basic nitrogen, salt concentration, brown index and acidity, represented by y1, y2, y3, y4, y5, y6, y7, y8, and y9, respectively. They form a group U= {y1, y2, y3, y4, y5, y6, y7, y8, y9,}. Using the fuzzy functions, the values of all these factors are transformed into fuzzy degrees of single factor, i.e. numerical values between 0 and 1. The fuzzy degrees of single factor in several samples are made up a matrix R. Following that, a weight of each index can be determined in the comprehensive evaluation. In the analytic hierarchy process, the weight can be obtained by the cross comparison between two different factors. The results show that the weights (W) of sensory evaluation, amino nitrogen, total nitrogen, specific gravity, volatile basic nitrogen, salt concentration, brown index and acidity are 0.356, 0.189, 0.107, 0.054, 0.097, 0.063, 0.061 and 0.073 respectively. Finally the aggregated fuzzy degree (B) of different samples is computed by B=W·R, which can be taken as the final result of comprehensive evaluation. The larger this value is, the higher the quality of sauce product would be.
基金National Science&Technology Pillar Program of China(No.2012BAC02B04)National Natural Science Foundation of China(No.41201306)
文摘High enzymatic activity is required for laccase applications.Central composite design (CCD)-based response surface methodology (RSM) can effectively increase the enzymatic activity of Pleurotus ostreatus P40 in liquid substrate fermentation.Initial screening of the nutritional components was performed using a Plackett-Burman design.The variables,namely,bran,bagasse,Tween 80,and yeast extract,were found to have statistically significant effects on laccase activity.These variables were further optimized using CCD-based RSM.Optimal concentrations for the maximum laccase activity were 8.144 2 g/L bran,50 g/L bagasse,0.424 1 mL/L Tween 80,and 2.832 5 g/L yeast extract.Under optimized conditions,the maximum measured laccase activity reached 96 480 U/L,which was close to the predicted value (104 830 U/L) by RSM.Therefore,RSM can be used to optimize culture components for laccase activity from Pieurotus ostreatus P40.
基金Supported by the National Natural Science Foundationof China (No.60474041).
文摘Model integration is an important section of the model management research area. The paper puts forward a formalization representation of model, and presents some concepts, such as the compound model re- lation, the composite model and so on. Additionally, the existence of model integration is also analyzed in de- tail and several sufficient conditions are proved.
文摘The influence of solvent (in its gaseous state) on the stability of crystallized organic compounds was investigated. Through two examples of studies on the solid/vapour equilibria made in our lab, several behaviors were highlighted: (i) a new hydrated phase (thermodynamically stable) of an active pharmaceutical ingredient (API) was detected after the recrystallization starting from a deliquescent state, (ii) a spontaneous resolution of a hydrated racemic compound towards an anhydrous conglomerate can occur during the desolvation under the precise conditions of temperature and humidity. This study illustrates that knowledge about solid/vapour equilibrium is a crucial step during the complete characterization of solid organic compounds.
基金the National Basic Research Program of China (No.2005CB221503)the National Natural Science Foundation of China (Nos.70533050 and 50674089)+1 种基金the National Foundation for the Youth of China (No.50904068)the Research Fund for the Youth of China University of Mining & Technology (No.OY091223)
文摘Based on theoretical analysis, similarity simulation tests, numerical simulation analysis and field observations, we analyzed rock collapse and rules of fraction evolution of overlying rocks and studied the rules in controlling the effect of an extremely thick igneous rock, found above a main mining coal seam in an area prone to coal mine disasters in the Haizi Coal Mine. The results show that this igneous rock, called a "main key stratum", will not subside nor break for a long time, causing lower fractures and bed separations not to close. The presence of igneous rock plays an important role in rock bursts, mine floods, gas outburst and surface subsidence in coal mines. By analyzing the rules in controlling the effect of this igneous rock, we provide useful references for safety and high efficiency mining in coal mines under special geological conditions.