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高效液相色谱-串联质谱法测定松树木材中阿维菌素的残留量
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作者 王奕升 张铮钰 +5 位作者 徐勇 周杨 吴兰鑫 王真 张红艳 吴学民 《中南农业科技》 2023年第5期64-66,共3页
建立高效液相色谱-串联质谱法测定松树木材中阿维菌素残留量的检测方法,旨在为阿维菌素防治松树害虫对环境的影响研究提供参考。木屑样品以乙腈作为提取溶剂,经振荡提取后C18分散固相萃取净化,离心后上清液经有机系滤膜过滤后在液相色谱... 建立高效液相色谱-串联质谱法测定松树木材中阿维菌素残留量的检测方法,旨在为阿维菌素防治松树害虫对环境的影响研究提供参考。木屑样品以乙腈作为提取溶剂,经振荡提取后C18分散固相萃取净化,离心后上清液经有机系滤膜过滤后在液相色谱-串联质谱正离子多反应监测模式下进行检测。结果表明,阿维菌素在0.005~1.000 mg/L线性关系良好,线性决定系数为0.9976;添加浓度为0.1、1.0、5.0 mg/kg时,平均回收率在77%~86%,相对标准偏差在2.0%~8.0%,方法定量限为0.1 mg/kg。该方法样品前处理操作简便快捷、灵敏度高、准确度高,可以用于测定松树木材中阿维菌素的残留量。 展开更多
关键词 高效液相色谱-串联质谱法 阿维菌素 松树木材 农药残留
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Study on Wood Drying Properties under Vacuum-floating Pressure
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作者 ZHANGBiguang YISonghn CHANGJianmin LIXianjun 《Chinese Forestry Science and Technology》 2004年第4期65-71,共7页
Using Masson pine as specimens, when drying mediums are overheated steam and hot-air respectively, preheating characteristics of wood under vacuum-floating pressure drying are discussed by measurement of internal temp... Using Masson pine as specimens, when drying mediums are overheated steam and hot-air respectively, preheating characteristics of wood under vacuum-floating pressure drying are discussed by measurement of internal temperature field and variation of moisture content during period of preheating. The relationship between drying medium conditions and drying rate of wood reveals that, firstly, compared with process of air-drying, time needed to be preheated under vacuum-floating decreased dramatically, meanwhile,the magnitude of condensation on the surface is relatively larger. Secondly, drying rate of wood under vacuum-floating pressure increases coupled with temperature of medium, reduction of absolute pressure,and raise of fluctuation rate of pressure. The sequence of factors contribution to drying rate is listed as following: temperature of medium (t) > fluctuation rate of pressure (f)> absolute pressure (p). 展开更多
关键词 wood drying vacuum-floating pressure PREHEATING CHARACTERISTICS
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