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高效液相色谱同时测定桂生汤中毛蕊花糖苷和桂皮醛的含量 被引量:2
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作者 刘丹 于丽红 +1 位作者 王颖 牛军 《中南药学》 CAS 2019年第11期1903-1905,共3页
目的建立高效液相色谱法同时测定桂生汤中毛蕊花糖苷和桂皮醛的含量。方法样品经微孔滤膜过滤后直接进样,色谱柱为Agilent ZORBAX Eclipse XDB-C18柱(4.6 mm×250 mm,5μm),以乙腈(A)-0.05%磷酸(B)为流动相梯度洗脱,流速1.0 mL·... 目的建立高效液相色谱法同时测定桂生汤中毛蕊花糖苷和桂皮醛的含量。方法样品经微孔滤膜过滤后直接进样,色谱柱为Agilent ZORBAX Eclipse XDB-C18柱(4.6 mm×250 mm,5μm),以乙腈(A)-0.05%磷酸(B)为流动相梯度洗脱,流速1.0 mL·min^-1,检测波长290 nm,柱温25℃。结果毛蕊花糖苷线性范围为0.010~0.242 mg·mL^-1,桂皮醛线性范围为0.020~0.494 mg·mL^-1,分离度良好。结论该方法简便可靠,专属性强,为桂生汤的进一步制剂研究提供了含量测定方法。 展开更多
关键词 桂生汤 桂皮醛 毛蕊花糖苷 高效液相色谱法
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Research Progress on Classical Prescriptions in Treating Mammary Glands Hyperplasia
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作者 Xin Jjiang Zhenliang Wang 《Chinese Medicine and Natural Products》 2022年第2期55-59,共5页
According to Zhongjing Zhang's academic thought,gynecological diseases mostly result from deficiency,accumulated cold,and qi stagnation,so the treatment of gynecological miscellaneous diseases should take qi and b... According to Zhongjing Zhang's academic thought,gynecological diseases mostly result from deficiency,accumulated cold,and qi stagnation,so the treatment of gynecological miscellaneous diseases should take qi and blood as the general principle,and focus on the liver.The pathogenesis of mammary glands hyperplasia(MGH)is liver and kidney deficiency,disharmony of the thoroughfare vessel and the conception vessel,the causes of which are emotional imbalance,liver qi depression,and failure of transportation due to spleen deficiency.The superficial causes include qi stagnation,phlegm coagulation,and blood stasis,which are mainly related to the liver,spleen,kidney,the thoroughfare vessel,and the conception vessel.In clinical treatment of MGH,Xiaochaihu Decoction or Sini Powder can be used for qi stagnation syndrome,Xiao Xianxiong Decoction for phlegm coagulation syndrome,Guizhi Fuling Pill or Dahuang Zhechong Pill for spleen deficiency syndrome,and Wenjing Decoction for the deficiency-cold syndrome. 展开更多
关键词 mammary glands hyperplasia Sini Powder Xiao Xianxiong Decoction Guizhi Fuling Pill Dahuang Zhechong Pill Xiao jianzhong Decoction Wenjing Decoction Yanghe Decoction
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