基金supported by the Science and Technology Projects of General Administration of Quality Supervision,Inspection and Quarantine of the People’s Republic of China ( 2011QK321,2012QK065, 2012104016-4, 2012KJ018 )research project of Guangdong provincial department of science and technology( 2014A040401046)Administration of quality and technology supervision of Guangdong Province and Guangzhou city ( No. 2015PT01, 2014CT04,2012KJ18)