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气相色谱-质谱法测定榴莲果肉中的香气成分
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作者 盖爽 邹宇新 +2 位作者 武越 尹伟懿 徐敏 《分析化学进展》 2017年第4期222-227,共6页
以榴莲果肉为试材,采用同时蒸馏萃取法提取其香气成分,采用气相色谱-质谱联用技术对含有榴莲香气成分进行分析,分离出了65个峰,经质谱分析、NIST05.L标准谱图检索,确定了榴莲香气成分的化学成分。从结果看出,榴莲果肉的主要芳香成分为... 以榴莲果肉为试材,采用同时蒸馏萃取法提取其香气成分,采用气相色谱-质谱联用技术对含有榴莲香气成分进行分析,分离出了65个峰,经质谱分析、NIST05.L标准谱图检索,确定了榴莲香气成分的化学成分。从结果看出,榴莲果肉的主要芳香成分为酯、酮、醇、烃类。研究结果可为榴莲在贮藏、食品加工、营养分析等领域开发利用提供参考。 展开更多
关键词 气相色谱-质谱法(GC-MS) 香气成分 榴莲果肉 同时蒸馏萃取
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Analysis of Aroma Volatile Profile of Philippine Durian Pulp (Durio zibethinus Rumph, ex Murray) Using HS-SPME Coupled with GC-MS
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作者 Princess Tiffany G. Dantes John S. Maninang +4 位作者 Arnold R. Elepano Hiroshi Gemma Sumiko Sugaya Engelbert K. Peralta Linda B. Mabesa 《Journal of Food Science and Engineering》 2014年第3期155-159,共5页
Durian (Durio zibethinus Rumph. ex Murray) is an exotic tropical fruit known for its excellent flavor and strong distinctive aroma. Volatiles of durian pulp from different cultivars in Thailand, Malaysia and Indones... Durian (Durio zibethinus Rumph. ex Murray) is an exotic tropical fruit known for its excellent flavor and strong distinctive aroma. Volatiles of durian pulp from different cultivars in Thailand, Malaysia and Indonesia were already reported. However, no study of volatiles from Philippine "Puyat" durian is available. "Puyat" is the most preferred by consumers in the Philippines due to its firm flesh with sweet and buttery taste. Aroma volatile compounds were analyzed by headspace solid phase microextraction (HS-SPME) method and gas chromatography-mass spectrometry (GC-MS). Volatiles were extracted for 1 h using 65 μm PDM/DVB SPME fiber and separated by DB-WAX capillary column (30 m × 0.25 mm id × 0.25 μm film thickness). Durian pulp produced 22 volatiles composed of 15 esters, six sulfurs and one thioacetal. Ethyl propanoate, ethyl octanoate, propyl propanoate, ethyl 2-methyl butanoate and diethyl disulfide were the major compounds identified. These compounds were also reported to be the most abundant in durian cultivars of other countries. Results of this study can then be used for future development of postharvest technologies to control the production of volatiles from Philippine durian pulp. 展开更多
关键词 DURIAN SPME GC-MS volatile compounds.
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