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微波-亚临界水萃取底泥中两种多氯联苯的研究 被引量:5
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作者 黄卫红 李勇 +1 位作者 杨岚钦 黄婷婷 《中国环境监测》 CAS CSCD 北大核心 2010年第5期15-18,共4页
微波亚临界水萃取模拟土样中的2,3-二氯联苯和3,3′-二氯联苯,用气相色谱进行分析。与亚临界水萃取方法相比,该法缩短了萃取时间,分析物的萃取回收率有所提高。对微波亚临界水的萃取条件进行优化,确定了最佳萃取条件为时间20min、温度... 微波亚临界水萃取模拟土样中的2,3-二氯联苯和3,3′-二氯联苯,用气相色谱进行分析。与亚临界水萃取方法相比,该法缩短了萃取时间,分析物的萃取回收率有所提高。对微波亚临界水的萃取条件进行优化,确定了最佳萃取条件为时间20min、温度区段为210℃~225℃。方法对长江镇江段内江的底泥中的多氯联苯进行分析,测定结果与索氏提取-GC分析结果吻合,且不受底泥中腐殖质等有机物影响。 展开更多
关键词 微波亚临界水萃取 模拟土样 2 3-二氯联苯 3 3′-二氯联苯 气相色谱
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Experimental study on simulation test instrument and its penetration performance of soil infiltration clogging
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作者 LU Jinzhi YANG Zhishuang LI Pengfei 《Global Geology》 2016年第3期182-186,共5页
The three-dimensional seepage simulation test device for siltation dam foundation soil is a multifunctional penetration instrument which is designed for the simulation of infiltration clogging,seepage damage,and dam s... The three-dimensional seepage simulation test device for siltation dam foundation soil is a multifunctional penetration instrument which is designed for the simulation of infiltration clogging,seepage damage,and dam seepage and so on. This device is different from the traditional instruments for the rock and soil permeability. In order to verify the practicability of the device,the authors collected the soil samples for laboratory penetration test,observed the seepage damage phenomenon,and obtained the dynamic change curve of permeability coefficient and isopotential map of water pressure. At the same time,the Geostudio finite element software is used to simulate the steady seepage of the test device. By contrast of the isopotential maps between simulation and actual water pressures,it is found that they are approximately the same. It is proved that the test data of the device is scientific and reliable,reaching the results of the test and design purposes. The instrument can be used in many aspects of experimental study on soil seepage. 展开更多
关键词 SEEPAGE numerical simulation penetration performance soil infiltration clogging
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