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正交函数光谱法测定复方普鲁卡因注射液的含量 被引量:4
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作者 李炜清 黄心一 《华西药学杂志》 CAS CSCD 北大核心 2000年第6期460-461,共2页
目的 :测定复方普鲁卡因注射液中普鲁卡因的含量。方法 :使用正交函数分光光度法。结果 :盐酸普鲁卡因的平均回收率为 10 0 .0 4% ,RSD为 0 .15 % (n =6 )。结论 :样品不经分离直接测定 ,结果准确 ,可用于普鲁卡因制剂的快速质量检验。
关键词 复方普鲁卡因注射液 含量测定 函数光谱
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正交函数光谱法测定珠贝定喘丸中的氨茶碱 被引量:3
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作者 黄诺嘉 张幼扬 《中成药》 CAS CSCD 北大核心 1991年第8期15-16,共2页
改进珠贝定喘丸中氨茶碱含量测定的方法,不需繁复的提取分离即可排除共存物质的干扰。方法简单快速,节约溶剂和时间,准确度和精密度均能符合制剂分析的要求。
关键词 珠贝定喘丸 氨茶碱 函数光谱
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正交函数光谱法测定栀芩清热液中黄芩甙的含量 被引量:3
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作者 黄诺嘉 吕红 《广东药学》 1997年第1期19-21,18,共4页
采用正交函数光谱法测定中药复方制剂栀芩清热液中黄芩甙的含量,可较好的排除其它成分的干扰,方法简便,快速,准确.
关键词 函数光谱 黄芩甙 栀芩清热液 含量测定
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差示-正交函数光谱法测定扑感敏胶囊中氨基比林含量
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作者 于治国 侯晓虹 +2 位作者 姜玲 赵冬梅 陈明明 《西北药学杂志》 CAS 1994年第6期245-248,共4页
采用差示-正交函数光谱法测定扑感敏胶囊中氨基比林的含量。本法以0.05mol/L硫酸溶液为参比液,0.1mol/L氢氧化钠溶液为样品液,以二次正交多项式系数(P2)为定量信息,分别在六个波长点下(N=6,=6mm,m... 采用差示-正交函数光谱法测定扑感敏胶囊中氨基比林的含量。本法以0.05mol/L硫酸溶液为参比液,0.1mol/L氢氧化钠溶液为样品液,以二次正交多项式系数(P2)为定量信息,分别在六个波长点下(N=6,=6mm,m=270.4mm)测定。测得平均回收率为100.1±0.23%(n=9)。 展开更多
关键词 函数光谱 扑感敏胶囊 氨基比林
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正交函数光谱法测定哮喘合剂中氨茶碱的含量
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作者 陈勇川 谢本琴 《华西药学杂志》 CAS CSCD 北大核心 1998年第4期275-276,共2页
采用正交函数光谱法测定了哮喘合剂中氨茶碱的含量,该法适合医院制剂的快速分析。
关键词 函数光谱 氨茶碱 哮喘合剂
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微波溶解—氢化物发生原子荧光光谱法测定氟石中的砷和汞 被引量:9
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作者 曾泽 蒋维旗 谢琰 《检验检疫科学》 2008年第6期32-34,共3页
研究了用微波溶解试样、氢化物发生原子荧光光谱法测定氟石中砷和汞的方法。探讨了试样的溶解条件、测定仪器条件、砷浓度过高时的预警与处理、硼氢化钾还原剂浓度对汞测定的影响及优化等。方法检出限0.076ng/mL(As),0.007ng/mL(Hg),线... 研究了用微波溶解试样、氢化物发生原子荧光光谱法测定氟石中砷和汞的方法。探讨了试样的溶解条件、测定仪器条件、砷浓度过高时的预警与处理、硼氢化钾还原剂浓度对汞测定的影响及优化等。方法检出限0.076ng/mL(As),0.007ng/mL(Hg),线性范围3.6~36ng/mL(As),0.2~1.2ng/mL(Hg),回收率105.4%~110.2%(As),100.3%~103.2%(Hg)。 展开更多
关键词 微波溶解 氟石 氢化物发生原子荧光光谱 扩增试验法
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珠贝定喘丸中氨茶碱含量均匀度测定方法研究 被引量:1
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作者 黄诺嘉 《中国药房》 CAS CSCD 2003年第10期622-623,共2页
目的 :建立珠贝定喘丸中氨茶碱含量均匀度的测定方法。方法 :采用正交函数光谱法。结果 :含量均匀度A +1 80S=7 7~12 2 ,均在限度范围内。结论 :本方法简便、准确 。
关键词 珠贝定喘丸 氨茶碱 函数光谱 含量均匀度
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清喉咽合剂中黄芩苷不同定量方法对比研究 被引量:1
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作者 张银竹 张娜娜 +1 位作者 张振巍 石磊 《中国药师》 CAS 2014年第2期215-217,共3页
目的:对比不同分析方法对清喉咽合剂中黄芩苷含量测定的影响。方法:采用高效液相色谱法和正交函数光谱法对清喉咽合剂中黄芩苷进行含量测定。结果:正交函数光谱法黄芩苷在0.045—0.225mg·ml-1范围内正交系数与浓度C之间呈现... 目的:对比不同分析方法对清喉咽合剂中黄芩苷含量测定的影响。方法:采用高效液相色谱法和正交函数光谱法对清喉咽合剂中黄芩苷进行含量测定。结果:正交函数光谱法黄芩苷在0.045—0.225mg·ml-1范围内正交系数与浓度C之间呈现较好的线性关系,回归方程|P2|=0.0917C-0.0059(r=0.9999);正交函数光谱法与HPLC法测定结果比较,差异无统计学意义(P〉0.05)。结论:正交函数光谱法简便、快速、准确,检测成本低,可以对中药制剂中主要活性成分进行快速、准确的定量检测。 展开更多
关键词 清喉咽合剂 黄芩苷 函数光谱 高效液相色谱法
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Background correction in near-infrared spectra of plant extracts by orthogonal signal correction 被引量:1
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作者 瞿海斌 欧丹林 程翼宇 《Journal of Zhejiang University-Science B(Biomedicine & Biotechnology)》 SCIE EI CAS CSCD 2005年第8期838-843,共6页
In near-infrared (NIR) analysis of plant extracts, excessive background often exists in near-infrared spectra. The detection of active constituents is difficult because of excessive background, and correction of this ... In near-infrared (NIR) analysis of plant extracts, excessive background often exists in near-infrared spectra. The detection of active constituents is difficult because of excessive background, and correction of this problem remains difficult. In this work, the orthogonal signal correction (OSC) method was used to correct excessive background. The method was also compared with several classical background correction methods, such as offset correction, multiplicative scatter correction (MSC), standard normal variate (SNV) transformation, de-trending (DT), first derivative, second derivative and wavelet methods. A simulated dataset and a real NIR spectral dataset were used to test the efficiency of different background correction methods. The results showed that OSC is the only effective method for correcting excessive background. 展开更多
关键词 Background correction Plant extracts Orthogonal signal correction Near-infrared spectroscopy
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Performance analysis and code recognition for dual N-ary orthogonal hybrid modulation systems
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作者 乔晓强 Zhao Hangsheng Cai Yueming 《High Technology Letters》 EI CAS 2008年第2期113-117,共5页
A dual N-ary orthogonal hybrid modulation system is introduced in this paper, which can increase the data rate greatly compared with conventional N-ary orthogonal spread spectrum system, so it can be used for high rat... A dual N-ary orthogonal hybrid modulation system is introduced in this paper, which can increase the data rate greatly compared with conventional N-ary orthogonal spread spectrum system, so it can be used for high rate data communication. Then, three code recognition algorithms are presented for dual N-ary orthogonal hybrid modulation system and the analytic bit error rate (BER) performance of the system in additive white Gaussian noise (AWGN) and fiat Rayleigh fading channel is derived. Finally, the computer simulation of the system with three code recognition algorithms is performed, which shows that the simplified maximum a posteriori (MAP) algorithm is the best for the system with a compromise between the performance and the complexity. 展开更多
关键词 code recognition N-ary orthogonal spread spectrum hybrid modulation MAP (maxi-mum a posteriori) algorithm
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THE STUDY OF A BOCC M-ARY SPREAD SPECTRUM SCHEME
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作者 Chu Zhenyong Ying Xiaofan +1 位作者 Tian Hongxin Yi Kechu 《Journal of Electronics(China)》 2005年第5期449-457,共9页
M-ary spread spectrum technique has been found wide applications in wireless communications, but it needs too many orthogonal spreading codes and its despreading/demodulation is quite complex computationally, which li... M-ary spread spectrum technique has been found wide applications in wireless communications, but it needs too many orthogonal spreading codes and its despreading/demodulation is quite complex computationally, which limit its wider applications. This paper proposes a novel scheme for Code Division Multiple Access (CDMA) communication systems based on M-ary spread spectrum, where only one prototype spreading code is assigned to each user and the codes for different users are orthogonal or quasi-orthogonal with each other. The M spreading codes of each user to represent K bits data are generated by circularly shifting the assigned code and reversing its polarity. The spreading codes generated like that are called as BiOrthogonal Cyclic Codes (BOCCs). At the receiver of the system, a transform domain matched-filter implemented by means of Fast Fourier Transform (FFT) is employed to despread and demodulate the received signals, which has very low computational complexity. The results of simulation experiments and bit-error performance analysis show that the proposed scheme is practical and very useful in many cases. 展开更多
关键词 M-ary spread spectrum BiOrthogonal Cyclic Codes (BOCCs) Satellite communication Transform domain processing
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Aerosol Type Identification Using PARASOL Multichannel Polarized Data 被引量:2
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作者 FAN Xue-Hua CHEN Hong-Bin 《Atmospheric and Oceanic Science Letters》 CSCD 2014年第3期224-229,共6页
PARASOL(Polarization & Anisotropy of Reflectances for Atmospheric Sciences coupled with Observations from a Lidar) multi-channel and multi-directional polarized data for different aerosol types were compared.The P... PARASOL(Polarization & Anisotropy of Reflectances for Atmospheric Sciences coupled with Observations from a Lidar) multi-channel and multi-directional polarized data for different aerosol types were compared.The PARASOL polarized radiance data at 490 nm,670 nm,and 865 nm increased with aerosol optical thickness(AOT) for fine-mode aerosols;however,the polarized radiances at 490 nm and 670 nm decreased as AOT increased for coarse dust aerosols.Thus,the variation of the polarized radiance with AOT can be used to identify fine or coarse particle-dominated aerosols.Polarized radiances at three wavelengths for fine-and coarse-mode aerosols were analyzed and fitted by linear regression.The slope of the line for 670 nm and 490 nm wavelength pairs is less than 0.35 for dust aerosols.However,the value for fine-mode aerosols is greater than 0.60.The Support Vector Machine method(SVM) based on 12 vector features was used to discriminate clear sky,coarse dust aerosols,fine-mode aerosols,and cloud.Two cases were given and validated by AErosol RObotic NETwork(AERONET) measurements,MODIS(Moderate Resolution Imaging Spectroradiometer) FMF(Fine Mode Fraction at 550 nm) images,PARASOL RGB(Red Green Blue) images,and CALIOP(Cloud-Aerosol Lidar with Orthogonal Polarization) VFM(Vertical Feature Mask) data. 展开更多
关键词 aerosol typePARASOLpolarized data support vector machine
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