To study the effect of annealing temperature on the joints between magnesium and aluminum alloys, and improve the properties of bonding layers, composite plates of magnesium alloy(AZ31 B) and aluminum alloy(6061) ...To study the effect of annealing temperature on the joints between magnesium and aluminum alloys, and improve the properties of bonding layers, composite plates of magnesium alloy(AZ31 B) and aluminum alloy(6061) were welded using the vacuum diffusion bonding method. The composite specimens were continuously annealed in an electrical furnace under the protection of argon gas. The microstructures were then observed using scanning electron microscopy. X-ray diffractometry was used to investigate the residual stresses in the specimens. The elemental distribution was analyzed with an electron probe micro analyzer. The tensile strength and hardness were also measured. Results show that the diffusion layers become wide as the heat treatment temperature increases, and the residual stress of the specimen is at a minimum and tensile strength is the largest when being annealed at 250 ℃. Therefore, 250 ℃ is the most appropriate annealing temperature.展开更多
Curvature method was used to measure the residual stress and substrate straining tensile test was carried out to study the debonding behavior of TiO2 nanotube film. The results indicate that the internal residual stre...Curvature method was used to measure the residual stress and substrate straining tensile test was carried out to study the debonding behavior of TiO2 nanotube film. The results indicate that the internal residual stress is -54 MPa. The strains of debonding initiation of TiO2 nanotube films without annealing, with 250 °C annealing and with 400 °C annealing are 2.6%, 5.1% and 8.6%, respectively, and the average radii of the debonding patches with debonding initiation are 27.5, 17.1 and 19.4 μm, respectively. The true critical debonding stresses of TiO2 nanotube films without annealing, with 250 °C annealing and with 400 °C annealing can be estimated as 220.4, 394.5 and 627.9 MPa, respectively. Interfacial shear lag model is modified and polynomial fitting equation of the interfacial shear strength of TiO2 nanotube film is demonstrated under debonding conditions. The modification and polynomial fitting are reliable since good agreement of the interfacial shear strengths after fitting is obtained compared with those results from the crack density analysis.展开更多
Single Ni-P and Ni-Mo-P coatings as well as duplex Ni-P/Ni-Mo-P coatings with the same compositions were prepared by electroless plating.The residual stresses of the coatings on the surface and cross sections were mea...Single Ni-P and Ni-Mo-P coatings as well as duplex Ni-P/Ni-Mo-P coatings with the same compositions were prepared by electroless plating.The residual stresses of the coatings on the surface and cross sections were measured by nanoindentation and AFM analysis,and the corrosion behaviour of the coatings in10%HCl solution was evaluated by electrochemical methods,to establish the correlation between the residual stresses and corrosion behaviour of the coatings.The results showed that the single Ni-P and duplex Ni-P/Ni-Mo-P coatings presented residual compressive stresses of241and206MPa respectively,while the single Ni-Mo-P coating exhibited a residual tensile stress of257MPa.The residual compressive stress impeded the growth of the pre-existing porosity in the coatings,protecting the integrity of the coating.The duplex Ni-P/Ni-Mo-P coatings had better corrosion resistance than their respective single coating.In addition,the stress states affect the corrosive form of coatings.展开更多
Diamond films were deposited on high-speed steel substrates by hot filament chemical vapor deposition (HFCVD) method. To minimize the early formation of graphite and to enhance the diamond film adhesion, a WC-Co coa...Diamond films were deposited on high-speed steel substrates by hot filament chemical vapor deposition (HFCVD) method. To minimize the early formation of graphite and to enhance the diamond film adhesion, a WC-Co coating was used as an interlayer on the steel substrates by high velocity oxy-fuel spraying. The effects of methane content on nucleation, quality, residual stress and adhesion of diamond films were investigated. The results indicate that the increasing methane content leads to the increase in nucleation density, residual stress, the degradation of quality and adhesion of diamond films. Diamond films deposited on high-speed steel (HSS) substrate with a WC-Co interlayer exhibit high nucleation density and good adhesion under the condition of the methane content initially set to be a higher value (4%, volume fraction) for 30 min, and then reduced to 2% for subsequent growth at pressure of 3 kPa and substrate temperature of 800 ℃.展开更多
A structure of gradient hard coatings( Ti,TiN,TiCN and TiAlN) is designed,and residual stress is simulated by a finite element method with ANSYS. The influence of the realistic situation including load and temperature...A structure of gradient hard coatings( Ti,TiN,TiCN and TiAlN) is designed,and residual stress is simulated by a finite element method with ANSYS. The influence of the realistic situation including load and temperature on the residual stress of the coatings is investigated. Simulated results show that the realistic situation strongly affects the residual stress. To be specific,i) The main residual stress concentrates on the coatings prepared on YG8 substrate,and the residual stress and its gradient of the coatings are bigger than that of the substrate; ii) TiAlN and TiCN coatings have better resistance compression than that of TiN coatings in the same condition; iii) The improved multilayer structure of the gradient hard coatings produces weaker residual stress but higher anti-pressure of the substrate.展开更多
Although plating is a necessary process for SMT components, it alters the magnetic characteristics and inductance level of Ni-Cu-Zn ferrite components. The results of this work show that the following three factors in...Although plating is a necessary process for SMT components, it alters the magnetic characteristics and inductance level of Ni-Cu-Zn ferrite components. The results of this work show that the following three factors in plating affect these components, and the effects are different for Ni- and Sn-plating: (1) Plating layers exert stresses and react with the residual stress of components to change the inductance level, and the effect of the tin layer is greater than that of the nickel one; (2) The plating current induces a magnetic field inside the components directly and indirectly, and this remains as remanence inside the components and reduces the inductance level, and the effect level of Ni-plating is greater than that of Sn-plating; (3) The plating solution corrodes the interface of the termination and ferrite core of the components to release the residual stress, and causes an increase in inductance, and the effect of Sn-plating is greater than that of Ni-plating. In addition, the inductance level is the result of the net effect of these three factors, and if the sintering temperature is increased to change in the type of residual stress, the net effect will be changed.展开更多
Silicon-based planar neuroprobes are composed of silicon substrate,conducting layer,and insulation layers of SiO 2 or SiN membrane.The insulation layer is very important because it affects many key parameters of neupr...Silicon-based planar neuroprobes are composed of silicon substrate,conducting layer,and insulation layers of SiO 2 or SiN membrane.The insulation layer is very important because it affects many key parameters of neuprobes,like impedance,SNR(signal noise ratio),reliability,etc.Monolayer membrane of SiO 2 or SiN are not good choices for insulation layer,since defects and residual stress in these layers can induce bad passivation.In this paper a composite insulation structure is studied,with thermal SiO 2 as the lower insulation layer and with multilayer membrane composed of PECVD SiO 2 and SiN as the upper insulation layer.This structure not only solves the problem of residual stress but also ensures a good probe passivation.So it's a good choice for insulation layer of neuroprobes.展开更多
Thermal barrier coating(TBC)systems are widely used in industrial gas-turbine engines.However,premature failures have impaired the use of TBCs and cut down their lifetime,which requires a better understanding of their...Thermal barrier coating(TBC)systems are widely used in industrial gas-turbine engines.However,premature failures have impaired the use of TBCs and cut down their lifetime,which requires a better understanding of their failure mechanisms.In the present study,experimental studies of isothermal cycling are firstly carried out with the observation and estimation of microstructures.According to the experimental results,a finite element model is established for the analysis of stress perpendicular to the TBC/BC interface.Detailed residual stress distributions in TBC are obtained to reflect the influence of mechanical properties,oxidation,and interfacial roughness.The calculated results show that the maximum tensile stress concentration appears at the peak of TBC and continues to increase with thermal cycles.Because of the microstructural characteristics of plasma-sprayed TBCs,cracks initialize in tensile stress concentration(TSC)regions at the peaks of TBC and propagate along the TBC/BC interface resulting in the spallation of TBC.Also,the inclusion of creep is crucial to failure prediction and is more important than the inclusion of sintering in the simulation.展开更多
An extended one-dimensional stress model for the deposition of multilayer films is built based on the existing stress model by considering the influence of deposition conditions. Both thermal stress and intrinsic stre...An extended one-dimensional stress model for the deposition of multilayer films is built based on the existing stress model by considering the influence of deposition conditions. Both thermal stress and intrinsic stress are considered to constitute the final residual stress in the model. The deposition process conditions such as deposition temperature, oxygen pressure, and film growth rate are correlated to the full stress model to analyze the final residual stress distribution, and thus the deformation of the deposited multilayer system under different process conditions. Also, the model is numerically realized with in-house built code. A deposition of Ag-Cu multilayer system is simulated with the as-built extended stress model, and the final residual stresses under different deposition conditions are discussed with part of the results compared with experiment from other literature.展开更多
基金partially supported by the grant subsidy of the "Nano Project" for Private Universities: 2011-2014 from MEXT, Japansupported by the "Advanced Science Research Laboratory" in Saitama Institute of Technology, Japan
文摘To study the effect of annealing temperature on the joints between magnesium and aluminum alloys, and improve the properties of bonding layers, composite plates of magnesium alloy(AZ31 B) and aluminum alloy(6061) were welded using the vacuum diffusion bonding method. The composite specimens were continuously annealed in an electrical furnace under the protection of argon gas. The microstructures were then observed using scanning electron microscopy. X-ray diffractometry was used to investigate the residual stresses in the specimens. The elemental distribution was analyzed with an electron probe micro analyzer. The tensile strength and hardness were also measured. Results show that the diffusion layers become wide as the heat treatment temperature increases, and the residual stress of the specimen is at a minimum and tensile strength is the largest when being annealed at 250 ℃. Therefore, 250 ℃ is the most appropriate annealing temperature.
基金Project (51274248) supported by the National Natural Science Foundation of ChinaProject (20110946Z) supported by the State Key Laboratory of Powder Metallurgy, China
文摘Curvature method was used to measure the residual stress and substrate straining tensile test was carried out to study the debonding behavior of TiO2 nanotube film. The results indicate that the internal residual stress is -54 MPa. The strains of debonding initiation of TiO2 nanotube films without annealing, with 250 °C annealing and with 400 °C annealing are 2.6%, 5.1% and 8.6%, respectively, and the average radii of the debonding patches with debonding initiation are 27.5, 17.1 and 19.4 μm, respectively. The true critical debonding stresses of TiO2 nanotube films without annealing, with 250 °C annealing and with 400 °C annealing can be estimated as 220.4, 394.5 and 627.9 MPa, respectively. Interfacial shear lag model is modified and polynomial fitting equation of the interfacial shear strength of TiO2 nanotube film is demonstrated under debonding conditions. The modification and polynomial fitting are reliable since good agreement of the interfacial shear strengths after fitting is obtained compared with those results from the crack density analysis.
基金Project(ZR2011EMM014)supported by Shandong Provincial Natural Science Foundation of China
文摘Single Ni-P and Ni-Mo-P coatings as well as duplex Ni-P/Ni-Mo-P coatings with the same compositions were prepared by electroless plating.The residual stresses of the coatings on the surface and cross sections were measured by nanoindentation and AFM analysis,and the corrosion behaviour of the coatings in10%HCl solution was evaluated by electrochemical methods,to establish the correlation between the residual stresses and corrosion behaviour of the coatings.The results showed that the single Ni-P and duplex Ni-P/Ni-Mo-P coatings presented residual compressive stresses of241and206MPa respectively,while the single Ni-Mo-P coating exhibited a residual tensile stress of257MPa.The residual compressive stress impeded the growth of the pre-existing porosity in the coatings,protecting the integrity of the coating.The duplex Ni-P/Ni-Mo-P coatings had better corrosion resistance than their respective single coating.In addition,the stress states affect the corrosive form of coatings.
基金Project(1343-74236000005) supported by the Innovation Foundation for Postgraduates of Hunan Province, ChinaProject(ZKJ2008001) supported by the Open Fund for Valuable Instruments of Central South University, ChinaProject(2008112048) supported by the Open Fund of State Key Laboratory of Metallurgy, China
文摘Diamond films were deposited on high-speed steel substrates by hot filament chemical vapor deposition (HFCVD) method. To minimize the early formation of graphite and to enhance the diamond film adhesion, a WC-Co coating was used as an interlayer on the steel substrates by high velocity oxy-fuel spraying. The effects of methane content on nucleation, quality, residual stress and adhesion of diamond films were investigated. The results indicate that the increasing methane content leads to the increase in nucleation density, residual stress, the degradation of quality and adhesion of diamond films. Diamond films deposited on high-speed steel (HSS) substrate with a WC-Co interlayer exhibit high nucleation density and good adhesion under the condition of the methane content initially set to be a higher value (4%, volume fraction) for 30 min, and then reduced to 2% for subsequent growth at pressure of 3 kPa and substrate temperature of 800 ℃.
基金Supported by the National High Technology Research and Development Programme of China(No.2012AA09A203)Project of Sichuan Education Department(No.14ZA0321)
文摘A structure of gradient hard coatings( Ti,TiN,TiCN and TiAlN) is designed,and residual stress is simulated by a finite element method with ANSYS. The influence of the realistic situation including load and temperature on the residual stress of the coatings is investigated. Simulated results show that the realistic situation strongly affects the residual stress. To be specific,i) The main residual stress concentrates on the coatings prepared on YG8 substrate,and the residual stress and its gradient of the coatings are bigger than that of the substrate; ii) TiAlN and TiCN coatings have better resistance compression than that of TiN coatings in the same condition; iii) The improved multilayer structure of the gradient hard coatings produces weaker residual stress but higher anti-pressure of the substrate.
文摘Although plating is a necessary process for SMT components, it alters the magnetic characteristics and inductance level of Ni-Cu-Zn ferrite components. The results of this work show that the following three factors in plating affect these components, and the effects are different for Ni- and Sn-plating: (1) Plating layers exert stresses and react with the residual stress of components to change the inductance level, and the effect of the tin layer is greater than that of the nickel one; (2) The plating current induces a magnetic field inside the components directly and indirectly, and this remains as remanence inside the components and reduces the inductance level, and the effect level of Ni-plating is greater than that of Sn-plating; (3) The plating solution corrodes the interface of the termination and ferrite core of the components to release the residual stress, and causes an increase in inductance, and the effect of Sn-plating is greater than that of Ni-plating. In addition, the inductance level is the result of the net effect of these three factors, and if the sintering temperature is increased to change in the type of residual stress, the net effect will be changed.
文摘Silicon-based planar neuroprobes are composed of silicon substrate,conducting layer,and insulation layers of SiO 2 or SiN membrane.The insulation layer is very important because it affects many key parameters of neuprobes,like impedance,SNR(signal noise ratio),reliability,etc.Monolayer membrane of SiO 2 or SiN are not good choices for insulation layer,since defects and residual stress in these layers can induce bad passivation.In this paper a composite insulation structure is studied,with thermal SiO 2 as the lower insulation layer and with multilayer membrane composed of PECVD SiO 2 and SiN as the upper insulation layer.This structure not only solves the problem of residual stress but also ensures a good probe passivation.So it's a good choice for insulation layer of neuroprobes.
基金supported by the National Natural Science Foundation of China(Grant Nos.11232008 and 11372118)the Tsinghua University Initiative Scientific Research Program
文摘Thermal barrier coating(TBC)systems are widely used in industrial gas-turbine engines.However,premature failures have impaired the use of TBCs and cut down their lifetime,which requires a better understanding of their failure mechanisms.In the present study,experimental studies of isothermal cycling are firstly carried out with the observation and estimation of microstructures.According to the experimental results,a finite element model is established for the analysis of stress perpendicular to the TBC/BC interface.Detailed residual stress distributions in TBC are obtained to reflect the influence of mechanical properties,oxidation,and interfacial roughness.The calculated results show that the maximum tensile stress concentration appears at the peak of TBC and continues to increase with thermal cycles.Because of the microstructural characteristics of plasma-sprayed TBCs,cracks initialize in tensile stress concentration(TSC)regions at the peaks of TBC and propagate along the TBC/BC interface resulting in the spallation of TBC.Also,the inclusion of creep is crucial to failure prediction and is more important than the inclusion of sintering in the simulation.
基金supported by the National Natural Science Foundation of China(Grant Nos.51076075,91224008 and 91024032)
文摘An extended one-dimensional stress model for the deposition of multilayer films is built based on the existing stress model by considering the influence of deposition conditions. Both thermal stress and intrinsic stress are considered to constitute the final residual stress in the model. The deposition process conditions such as deposition temperature, oxygen pressure, and film growth rate are correlated to the full stress model to analyze the final residual stress distribution, and thus the deformation of the deposited multilayer system under different process conditions. Also, the model is numerically realized with in-house built code. A deposition of Ag-Cu multilayer system is simulated with the as-built extended stress model, and the final residual stresses under different deposition conditions are discussed with part of the results compared with experiment from other literature.