后续热处理对激光熔铸层残余应力的影响

本文在镍基合金ＤＺ４上激光熔铸钴基合金层，研究了后续热处理温度对熔铸层残余应力、显微硬度和金相组织的影响。结果表明，在低温退火处理时，可部分地消除熔铸层中的残余应力，而熔铸层组织和显微硬度并无明显变化；在高温退火处理时，熔铸层大部分应力得以消除，但熔铸层显微硬度下降，同时，熔铸层枝晶组织开始碎化。

Displacive transformation as pathway to prevent micro-cracks induced by thermal stress in additively manufactured strong and ductile high-entropy alloys

The micro-cracking behaviors of two high-entropy alloys(HEAs) of the FeMnCoCrNi family prepared by selective laser melting were systematically studied. Residual stresses were also analyzed by X-ray diffraction technique. Results show that the equiatomic FeMnCoCrNi HEAs with a relatively stable single-phase face-centered cubic(FCC) structure suffered from micro-cracking with residual tensile stress after laser melting. In contrast, the metastable non-equiatomic Fe MnCoCr HEAs with reduced stacking fault energy are free of micro-cracks with residual compressive stress at various volumetric energy densities(VEDs). The displacive transformation from the FCC matrix to the hexagonal close-packed(HCP) phase during cooling prevents the micro-cracking via consuming thermal stress related internal energy. Further, the displacive transformation during tensile deformation contributes to the higher strength and ductility of the metastable dual-phase HEA compared to that of the stable single-phase HEA. These findings provide useful guidance for the design of strong, ductile, and crack-free alloys for additive manufacturing by tuning phase stability.

Effect of Si content on laser welding performance of Al-Mn-Mg alloy

The correlation between Si content （0.1%-0.5%, mass fraction） and pulse laser welding performance of AI-Mn-Mg aluminum alloy sheets was studied. The sheets were fabricated in the laboratory, with gauge of 0.45 mm, H16 temper by pulse laser welding. It was found that no cracking existed in the welding pool as Si content was below 0.34%. However, when the Si content increased to 0.47%, cracking formed in the welding pool. Microstructure observations indicated that residual eutectic phases distributed at the grain boundaries were discontinuous and appeared to be small particles in lower Si content alloys; the residual eutectic phases distributed at the grain boundaries were partially continuous and appeared to be films in higher Si content alloys. These phenomena could explain why Si content adversely affected the laser welding performance.

Measuring internal residual stress in Al-Cu alloy forgings by crack compliance method with optimized parameters

Measuring the internal stress of Al alloy forgings accurately is critical for controlling the deformation during the subsequent machine process.In this work,the crack compliance method was used to calculate the internal residual stress of Al-Cu high strength alloys,and the effect of various model parameters of crack compliance method on the calculated precision was studied by combining the numerical simulation and experimental method.The results show that the precision first increased and then decreased with increasing the crack range.The decreased precision when using a high crack range was due to the strain fluctuation during the machining process,and the optimized crack range was 71%of the thickness of forgings.Low orders of Legendre polynomial can result in residual stress curve more smooth,while high orders led to the occurrence of distortion.The Tikhonov regularization method effectively suppressed the distortion of residual stress caused by the fluctuation of strain data,which significantly improved the precision.In addition,The crack compliance method with optimized parameters was used to measure the residual stress of Al-Cu alloy with different quenching methods.The calculated results demonstrated that the distribution of residual stress was obtained accurately.

Defect assessment of welded specimen considering weld induced residual stresses using SINTAP procedure and FEA

The defect assessment in butt-welded joint of ASTM A36 steel plates and 7075-T7351 aluminum alloy plates containing transverse through thickness crack was analyzed using SINTAP procedure and FEA incorporating weld induced residual stresses. Weld induced longitudinal residual stress profile can be obtained through SINTAP procedure, FEA or experimental analysis. This residual stress profile can be fitted with the trapezoidal residual stress profile available in SINTAP. For three different cases, crack length and residual stress intensity factor （SIF） are calculated and its comparison with the results obtained through FEA is plotted with respect to crack length. The stress intensity factor for mechanical loading is also plotted in the same graph. Using this graphical plot, the total SIF, including residual stress and mechanical loading, can be calculated for any particular crack size. The total SIF can be compared with the fracture toughness of the material for damage tolerance analysis. Also a failure assessment diagram is drawn for welded 7075-T7351 aluminum alloy plates with different crack sizes for as-welded （only residual stress） and mechanical loading along with the existing weld induced residual stresses to show the safety level for a particular crack size and mechanical loading.

Capillary gas chromatographic determination of dimethachlon residues in fresh tobacco leaves and cut-tobacco

Simple procedures for extraction and chromatographic determination of dimethachlon residues in fresh tobacco leaves and cut-tobacco are described.The determination was carried out by capillary gas chromatography(GC) with electron capture detection(ECD) and confirmed by GC-MS.The mean recoveries and relative standard deviation(RSD) were 93.2%～112.9% and 3.5%～6.7%,respectively at levels ranging from 0.01 to 0.1 mg/kg.The limit of determination was 0.001 mg/kg.Tobacco samples in routine check were successfully analyzed using the proposed method.

Effects of laser shock peening on fatigue crack growth rate and fracture properties of AA2524 aluminum alloy

In order to prolong the service life of aircraft skin made from AA2524, the effects of laser shock peening(LSP) on fatigue crack growth(FCG) rate and fracture toughness(K_(c)) of AA2524 were investigated. Multiple LSP treatment was performed on compact tension(CT) specimen from single side and double sides. The surface integrity was measured with Vickers hardness tester, X-ray diffractometer and confocal laser scanning microscope, respectively. FCG rate test and fracture toughness test under plane stress were carried out after LSP treatment. The microstructure features of cross-sections were observed with scanning electron microscope. The results showed that the micro-hardness and residual stress of CT specimens were increased dramatically after LSP treatment. Compared to the base metal(BM), the fatigue life was prolonged by 2.4 times and fracture toughness was increased by 22% after multiple LSP.