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浅谈食用碱重金属铅的检测方法的改进 被引量:2
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作者 鄂毓邦 《盐业与化工》 CAS 2015年第10期50-51,共2页
根据国家食品安全法要求,食用碱必须要做重金属铅的限量试验,可是依照国标的分析方法,在操作过程中存在一些问题,铅的分析中最主要的就是调p H值,因为铅只有在p H值为3~4时,才会显色,试样中加入国标规定的试剂的量即可达到要求,可是标... 根据国家食品安全法要求,食用碱必须要做重金属铅的限量试验,可是依照国标的分析方法,在操作过程中存在一些问题,铅的分析中最主要的就是调p H值,因为铅只有在p H值为3~4时,才会显色,试样中加入国标规定的试剂的量即可达到要求,可是标准比对溶液中加入规定的量并不能达到要求的p H值,而且为了达到要求的p H值要加入比试样多的试剂,溶液的体积很难控制到50 m L以内,所以,要找出解决这些问题的方法是非常必要的。 展开更多
关键词 食用碱 重金属 PH值 比对溶液
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浅谈环境实验室标准物质期间核查
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作者 张洪 《资源节约与环保》 2015年第12期115-115,共1页
基于环境实验室对标准物质期间的核查问题,文章阐述了环境实验室标准物质期间核查的具体定义。此外,还结合进行环境监测的实际情况,详细的分析了具体的核查方法。其目的是为相关行业的建设者提供一些理论依据。
关键词 标准物质 期间核查 标准溶液比对
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Experimental study on slime water flocculation sediment based on the montmorillonite hydration expansion inhibition 被引量:1
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作者 Wei-Dong WANG Hui-Feng WANG Jun-Tao SUN Yuan SUN 《Journal of Coal Science & Engineering(China)》 2013年第4期530-534,共5页
Through the montmorillonite settlement experiment in the clear water and electrolyte solution, the influence of slime water settling character was studied in clear water and different electrolyte solution, the montmor... Through the montmorillonite settlement experiment in the clear water and electrolyte solution, the influence of slime water settling character was studied in clear water and different electrolyte solution, the montmorillonite's hydration ex- pansion effectively restrained was verified, the process method to wash coal with the electrolyte was put forward, and the re- sults indicate that the solution of 10 g/L KC1 is optimal inhibitor on the montmorillonite in the tested three kinds of electrolyte solution. With the contrast test in clear water and electrolyte solution, two reagent adding way can be selected in KC1 solution: one way is to add PAM separately, the effectively sedimentation can be made with simply 0.1% anion; the other way is the co- ordination with polymeric aluminum and PAM, the anionic of PAM and polymeric aluminum are 0.02% and 0.5% respectively. However, in clear water, the polymeric aluminum must be joined together with the anionic PAM, and the amount of the PAM reaches 0.5%, which is 25 times as great as that in KCL solution. The field work with raw coal further verifies the above con- clusions further. 展开更多
关键词 coal slime water MONTMORILLONITE hydration expansion ELECTROLYTE
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