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流动气体捕集法测定贯叶连翘提取物中大孔树脂残留物 被引量:4
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作者 曹进 徐燕 +1 位作者 王义明 罗国安 《分析化学》 SCIE EI CAS CSCD 北大核心 2004年第3期309-312,共4页
采用流动气体捕集法 ,通过GC/MS法测定贯叶连翘提取物中大孔树脂残留物 苯、甲苯和二乙烯苯。与萃取、回流和顶空进样三种处理方式比较 ,自制的流动气体捕集装置能够很好地收集待测成分并有效地消除干扰。整体 (流动气体捕集法处理 +... 采用流动气体捕集法 ,通过GC/MS法测定贯叶连翘提取物中大孔树脂残留物 苯、甲苯和二乙烯苯。与萃取、回流和顶空进样三种处理方式比较 ,自制的流动气体捕集装置能够很好地收集待测成分并有效地消除干扰。整体 (流动气体捕集法处理 +含量测定 )检出限和回收率 (苯 :0 .3ng/g ,99.0 % ;甲苯 :0 .8ng/g ,99 5 % ;二乙烯苯 :0 .5ng/g ,99 2 % ) ,与GC/MS法所得结果 (苯 :0 .1ng/g ,99.2 % ;甲苯 :0 .2ng/g ,99.4 % ;二乙烯苯 :0 .1ng/g ,99.2 % )无显著差别 ,说明该法有较低的检出限和良好的回收率。经其他 3种方式处理后 ,检出限变差回收率下降。结果证明流动气体捕集法适于中药提取物中大孔树脂残留物的定量检测。 展开更多
关键词 贯叶连翘 提取物 大孔树脂 残留物 流动气体捕集 甲苯 二乙烯苯 气相色谱/质谱联用
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Cu2S—FeS—SnS系融体热力学研究
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作者 小池一男 黄书泽 《国外锡工业》 1995年第3期20-26,41,共8页
关键词 硫化锡 热力学 活度 气体流动法
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Numerical Simulation of Gas Holdup Distribution in a Standard Rushton Stirred Tank Using Discrete Particle Method 被引量:7
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作者 韩路长 刘跃进 罗和安 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2007年第6期808-813,共6页
The discrete particle method was used to simulate the distribution of gas holdup in a gas-liquid standard Rushton stirred tank. The gas phase was treated as a large number of bubbles and their trajectories were tracke... The discrete particle method was used to simulate the distribution of gas holdup in a gas-liquid standard Rushton stirred tank. The gas phase was treated as a large number of bubbles and their trajectories were tracked with the results of motion equations. The two-way approach was performed to couple the interphase momentum exchange. The turbulent dispersion of bubbles with a size distribution was modeled using a stochastic tracking model, and the added mass force was involved to account for the effect of bubble acceleration on the surrounding fluid. The predicted gas holdup distribution showed that this method could give reasonable prediction comparable to the reported experimental data when the effect of turbulence was took into account in modification for drag coefficient. 展开更多
关键词 numerical simulation gas holdup stirred tank discrete particle
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世界天然气管道干燥技术进展 被引量:16
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作者 刘炀 焦永涛 王波 《清洗世界》 CAS 2004年第6期18-23,45,共7页
概述了目前世界天然气管道采用的几种干燥技术方法以及这些方法在国内的应用情况,对国内外干燥技术的应用状况做了对比。
关键词 天然气管道 干燥技术 干空气干燥 清管 干燥剂 流动气体蒸发 氨气干燥 天然气干燥 真空干燥
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Human evacuation affected by smoke movement in mine fires 被引量:1
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作者 Peng Chen ShUong Guo Yong Wang 《International Journal of Coal Science & Technology》 EI 2016年第1期28-34,共7页
The objective of this work is to investigate the influence of smoke movement during mine fires on miner evacuation behaviors. A three-dimensional computational fluid dynamics method was conducted to reconstruct the la... The objective of this work is to investigate the influence of smoke movement during mine fires on miner evacuation behaviors. A three-dimensional computational fluid dynamics method was conducted to reconstruct the lane- way conveyor belt fire scenes under two ventilating conditions. The parameters, including temperature-time histories, soot density, carbon monoxide and heat release rate, were simulated to characterize the mine fires at various ventilating speeds. A miner evacuation model affected by fire smoke movement was advanced to describe the miner evacuation behaviors, which can be divided into three stages. Based on the evacuation model coupled with the mine fire smoke movement, the available safety evacuation time for miners involved in coal mine fire located in different sites was estimated. Two evacuation patterns were advanced according to the ventilating speeds combined with the model of miner evacuation behaviors. The results show that the miners located between the inlet-air end and the air door in lane 1 should be evacuated to the inlet-air end and other miners involved in coal mine fire could choose the air door as the escaping destination, when the ventilation speed is greater than 3 m/s. Accordingly, the research can be used as references for the mine safety administration authorities to design the safety evacuation. 展开更多
关键词 Mine fires Smoke movement Evacuation behaviors Evacuation patterns
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CFD Study of Ejector Flow Behavior in a Blast Furnace Gas Galvanizing Plant 被引量:5
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作者 Giorgio Besagni Riccardo Mereu Fabio Inzoli 《Journal of Thermal Science》 SCIE EI CAS CSCD 2015年第1期58-66,共9页
In recent years, there has been a growing interest toward Blast Furnace Gas (BFG) as a low-grade energy source for industrial furnaces. This paper considers the revamping of a galvanic plant furnace converted to BFG... In recent years, there has been a growing interest toward Blast Furnace Gas (BFG) as a low-grade energy source for industrial furnaces. This paper considers the revamping of a galvanic plant furnace converted to BFG from natural gas. In the design of the new system, the ejector on the exhaust line is a critical component. This paper studies the flow behavior of the ejector using a Computational Fluid Dynamics (CFD) analysis. The CFD model is based on a 3D representation of the ejector, using air and exhaust gases as working fluids. This paper is divided in three parts. In the first part, the galvanic plant used as case study is presented and discussed, in the second part the CFD approach is outlined, and in the third part the CFD approach is validated using experimental data and the numerical results are presented and discussed. Different Reynolds-Averaged Navier-Stokes (RANS) turbulence models (k-to SST and k-e Realizable) are evaluated in terms of convergence capability and accuracy in predicting the pressure drop along the ejector. Suggestions for future optimization of the system are also provided. 展开更多
关键词 CFD EJECTOR Blast Furnace Gas Galvanic plant RANS Turbulence models
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Analysis of the Water Film Behavior and its Breakup on Profile using Experimental and Numerical Methods 被引量:3
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作者 Tomas MUZIK Pavel SAFARIK Antonín TUCEK 《Journal of Thermal Science》 SCIE EI CAS CSCD 2014年第4期325-331,共7页
This paper deals with the description of water film behaviour on the airfoil NACA0012 using experimental and numerical methods. Properties of the water film on the profile and its breakup into droplets behind the prof... This paper deals with the description of water film behaviour on the airfoil NACA0012 using experimental and numerical methods. Properties of the water film on the profile and its breakup into droplets behind the profile are investigated in the aerodynamic tunnel and using CFD methods. The characteristic parameters of the water film, like its thickness and shape for different flow modes are described. Hereafter are described droplets drifted by the air, which water film is broken behind the profile. 展开更多
关键词 NACA0012 profile water film droplets BREAKUP CFD
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