Solid phase microextraction (SPME) is a solvent-flee method of sample collection. SPME is an appealing method for sample collection because it is designed for the sampling of trace level analytes with short sampling...Solid phase microextraction (SPME) is a solvent-flee method of sample collection. SPME is an appealing method for sample collection because it is designed for the sampling of trace level analytes with short sampling times in a variety of environments. Additionally, SPME can be used to directly deliver a sample to a gas chromatograph (GC) for analysis by means of thermal desorption. In this paper, the performance of SPME under dynamic conditions was investigated. Additionally, the competence of SPME sampling for the simultaneous analysis of multiple trace analytes was also evaluated. This work is discussed in the context of underground mine ventilation surveys but is applicable to any industry in which ventilation circuits must be evaluated. The results of this paper showed that the performance of the 100 ~m PDMS SPME fiber was both precise and rapid under dynamic conditions. This SPME fiber was also able to simultaneously collect sulfur hexafluoride (SF6) and perfluoromethylcyclohexane (PMCH) with adequate sensitivity.展开更多
A large number of debris flows occurred simultaneously at around 8:30 to 8:50 a.m.on July 27,2011,at the center of Seoul,Korea.This area is located in the southern part of Seoul and is a densely populated district.As ...A large number of debris flows occurred simultaneously at around 8:30 to 8:50 a.m.on July 27,2011,at the center of Seoul,Korea.This area is located in the southern part of Seoul and is a densely populated district.As a result of the debris flow event,16 people were killed,30 houses were buried,and 116 houses were damaged around Umyeon Mountain,a relatively small mountain with a height of 312.6 m.Since the debris flow event,field investigations on the initiation and transportation zones of debris flows have been carried out.Rainfall data were collected from the automatic weather stations(AWSs) which are operated by the Korea Meteorological Administration(KMA).Video files recorded by residents were also acquired and used to analyze the flow characteristics of the debris flow.Field investigation shows that about 40 debris flows occurred around Umyeon Mountain and most of the debris flows were initiated by small slope failures.The effects of the precipitation that triggered the debris flows were analyzed as well.A landslide hazard map which considers slope gradient and aspect,strength of soil,hazard record,rainfall conditions,and vegetation,was constructed and compared with the initiation zones of debris flows.展开更多
基金Contract No.200-2009-31933,awarded by the National Institute for Occupational Safety and Health(NIOSH)
文摘Solid phase microextraction (SPME) is a solvent-flee method of sample collection. SPME is an appealing method for sample collection because it is designed for the sampling of trace level analytes with short sampling times in a variety of environments. Additionally, SPME can be used to directly deliver a sample to a gas chromatograph (GC) for analysis by means of thermal desorption. In this paper, the performance of SPME under dynamic conditions was investigated. Additionally, the competence of SPME sampling for the simultaneous analysis of multiple trace analytes was also evaluated. This work is discussed in the context of underground mine ventilation surveys but is applicable to any industry in which ventilation circuits must be evaluated. The results of this paper showed that the performance of the 100 ~m PDMS SPME fiber was both precise and rapid under dynamic conditions. This SPME fiber was also able to simultaneously collect sulfur hexafluoride (SF6) and perfluoromethylcyclohexane (PMCH) with adequate sensitivity.
基金supported by the Basic Science Research Program through the National Research Foundation of Korea (NRF) funded by the Ministry of Education,Science and Technology (2012014940)supported by a grant(Code#’08 RTIP B01-01) from the Regional Technology Innovation Program (RTIP)funded by the Ministry of Land Transport and Maritime Affairs of the Korean government
文摘A large number of debris flows occurred simultaneously at around 8:30 to 8:50 a.m.on July 27,2011,at the center of Seoul,Korea.This area is located in the southern part of Seoul and is a densely populated district.As a result of the debris flow event,16 people were killed,30 houses were buried,and 116 houses were damaged around Umyeon Mountain,a relatively small mountain with a height of 312.6 m.Since the debris flow event,field investigations on the initiation and transportation zones of debris flows have been carried out.Rainfall data were collected from the automatic weather stations(AWSs) which are operated by the Korea Meteorological Administration(KMA).Video files recorded by residents were also acquired and used to analyze the flow characteristics of the debris flow.Field investigation shows that about 40 debris flows occurred around Umyeon Mountain and most of the debris flows were initiated by small slope failures.The effects of the precipitation that triggered the debris flows were analyzed as well.A landslide hazard map which considers slope gradient and aspect,strength of soil,hazard record,rainfall conditions,and vegetation,was constructed and compared with the initiation zones of debris flows.