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胶体黏度和纤维化工艺条件对80多晶氧化铝纤维性能的影响 被引量:3
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作者 傅顺德 徐建峰 +2 位作者 刘丽彬 贾佳 甘小明 《耐火材料》 CAS 北大核心 2010年第2期116-118,122,共4页
采用溶胶-凝胶法制备80多晶氧化铝纤维。以结晶氯化铝、铝粉和硅溶胶为主要原料制备出黏度分别为8、14、20、26和32Pa.s的甩丝胶体;采用甩丝法进行纤维化试验,控制甩丝盘转速分别为4000、5000、6000、7000和8000r.min-1;热风温度分别为6... 采用溶胶-凝胶法制备80多晶氧化铝纤维。以结晶氯化铝、铝粉和硅溶胶为主要原料制备出黏度分别为8、14、20、26和32Pa.s的甩丝胶体;采用甩丝法进行纤维化试验,控制甩丝盘转速分别为4000、5000、6000、7000和8000r.min-1;热风温度分别为60、70、80、90和100℃;并将甩丝后的纤维坯体于1250℃烧成,检测其平均直径和平均单丝拉伸强度。结果表明:在胶体黏度为20Pa.s、甩丝盘转速为6000r.min-1、热风温度为80℃时,纤维的平均直径为3.8μm,平均单丝拉伸强度超过1000MPa,是一种性能较优异的氧化铝纤维。 展开更多
关键词 氧化铝晶体纤维 甩丝 黏度 纤维化工艺条件
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氧化铝一维光子晶体薄膜的光纤折射率传感
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作者 何伟 朱青青 郭东来 《武汉理工大学学报》 CAS 北大核心 2017年第5期41-46,共6页
从光纤光栅的传感原理和特性出发,提出和实现了一种具有多孔光子晶体结构的光纤折射率传感器,并对其工作原理进行了理论分析和实验验证。该器件以阳极氧化铝(Anodic Aluminum Oxide,AAO)一维光子晶体薄膜与光纤陶瓷插芯端面的复合结构... 从光纤光栅的传感原理和特性出发,提出和实现了一种具有多孔光子晶体结构的光纤折射率传感器,并对其工作原理进行了理论分析和实验验证。该器件以阳极氧化铝(Anodic Aluminum Oxide,AAO)一维光子晶体薄膜与光纤陶瓷插芯端面的复合结构作为传感探头,来探测传感器所处环境的折射率变化。结果表明,该传感器件对外部环境的折射率变化敏感,其对应的中心波长会随着环境折射率的增大而发生红移,且两者之间呈线性的关系。折射率灵敏度可以通过调节多孔的AAO一维光子晶体薄膜的孔隙率来提高,并在折射率为1.333到1.376的范围内达到458.4 nm/RIU。 展开更多
关键词 光纤折射率传感器 氧化铝一维光子晶体 孔隙率
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由渣制取片CaO.6(Al,Ti)2O3晶体
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作者 В.,ВБ 李博英 《钒钛》 1991年第1期57-58,共2页
关键词 铁合金渣 片状晶体 β氧化铝晶体
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真空灭弧室瓷壳黄斑的形成机制及消除措施
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作者 赵智忠 张志慧 欧宁 《高压电器》 CAS CSCD 北大核心 2004年第6期431-432,共2页
对黄斑瓷壳和正常瓷壳进行了电性能测试、化学及烧氢烘烤等一系列试验,证明了高压老炼后真空灭弧室瓷壳黄斑的形成是由于氧化铝晶格配位结构的变化引起的,它不影响真空灭弧室的电气性能,而且加热至650℃后即可消除。
关键词 真空灭弧室 瓷壳黄斑 烧氢 真空烘烤 氧化铝晶体
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Alumina Photonic Crystals with Defect Modes for Sensor Application
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作者 闫鹏 费广涛 +3 位作者 李惠 商国亮 吴兵 张立德 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2014年第1期121-124,I0004,共5页
One-dimensional alumina photonic crystals with defect modes were successfully fabricated through inserting a constant voltage waveform into the periodic voltage signals. The trans-mission spectra show that the thickne... One-dimensional alumina photonic crystals with defect modes were successfully fabricated through inserting a constant voltage waveform into the periodic voltage signals. The trans-mission spectra show that the thickness of defects plays a key role in determining the trans-mittance of defect modes. When the thickness was ?180 nm, an obvious defect mode with the high transmittance of 55% and a narrow full width at half maximum of 18 nm was observed in the original photonic band gaps. The defect mode shifted linearly with the increasing of refractive index of the analytes infiltrated into pores, indicating its potential application in chemical sensing or bio-sensing. 展开更多
关键词 NANOMATERIAL Porous material ALUMINA Photonic crystal SENSOR
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Preparation and Characterization of Fe Nanowire Arrays Embedded in Porous Anodic Aluminum Oxide Templates 被引量:1
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作者 迟广俊 姚素薇 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2004年第2期315-318,共4页
Fe nanowire arrays are prepared by electrodeposition in porous anodic aluminum oxide template from a composite electrolyte solution. These nanowires have an uniform diameter of approximate 25 nm and a length in excess... Fe nanowire arrays are prepared by electrodeposition in porous anodic aluminum oxide template from a composite electrolyte solution. These nanowires have an uniform diameter of approximate 25 nm and a length in excess of 2.5 μm. The micrographs and crystal structures of Fe nanowires are studied by transmission electron microscopy (TEM), selected-area electron diffraction (SAED), and X-ray diffraction(XRD). It is found that each nanowire is essentially a single crystal and has a different orientation in each array. Hysteresis loops of Fe nanowire array show that its easy magnetization direction is perpendicular to the sample plane. 展开更多
关键词 ELECTRODEPOSITION NANOSTRUCTURE aluminum anodization
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α-Al_2O_3:C晶体热致发光和光致受激发光特性的数值模拟 被引量:5
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作者 杨新波 李红军 +3 位作者 徐军 程艳 苏良碧 唐强 《硅酸盐学报》 EI CAS CSCD 北大核心 2009年第2期247-252,共6页
通过α-Al2O3:C晶体的热致发光(thermoluminescence,TL)简单模型建立的速率方程,采用Mathematica 5.2软件用数值模拟的方法对α-Al2O3:C晶体的TL和光致受激发光(optically stimulated luminescence,OSL)特性进行了探讨。结果表明:随着... 通过α-Al2O3:C晶体的热致发光(thermoluminescence,TL)简单模型建立的速率方程,采用Mathematica 5.2软件用数值模拟的方法对α-Al2O3:C晶体的TL和光致受激发光(optically stimulated luminescence,OSL)特性进行了探讨。结果表明:随着辐照剂量的增加,α-Al2O3:C晶体TL峰向低温方向移动,OSL衰减速率逐渐加快;α-Al2O3:C晶体的TL和OSL剂量响应曲线呈线性-亚线性-饱和的特点,在低剂量范围内显示出良好的线性关系;OSL灵敏度明显优于TL灵敏度,具有更宽的线性剂量响应范围。数值模拟的计算结果和实验结果基本相符。 展开更多
关键词 掺碳氧化铝晶体 热致发光 光致受激发光 数值模拟
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Effect of Annealing on Aluminum Oxide Passivation Layer for Crystalline Silicon Wafer
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作者 Teng-Yu Wang Cheng-Chi Liu +2 位作者 Chien-Hsiung Hon Chen-Hsun Du Chung-Yuan Kung 《Journal of Energy and Power Engineering》 2013年第8期1505-1510,共6页
The surface of silicon was passivated by A1203 and acidify using nitric acid with SiOx as the bi-layer, it was expected that hydrogen bonding reduce interface states and negative field effect which yields maximum pass... The surface of silicon was passivated by A1203 and acidify using nitric acid with SiOx as the bi-layer, it was expected that hydrogen bonding reduce interface states and negative field effect which yields maximum passivation. By optimizing the thickness of passivation layer and annealing condition, the minority carrier lifetime of p-type single crystalline Czochralski wafer could be improved from 10 μs to 190 μs. The formation and variation of hillock defect on passivation layer was founded to be affected by the thermal annealing temperature. For the purpose of obtaining high minority carrier lifetime and low hillock defect density simultaneously, using a lower heating and cooling speed in thermal annealing process is suggested. 展开更多
关键词 SILICON PASSIVATION aluminum oxide atomic layer deposition.
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Molecular Dynamics Study of Interaction between Acrylamide Copolymers and Alumina Crystal 被引量:3
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作者 Feng-he Wang Feng-yun Wang Xue-dong Gong 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2012年第5期571-576,I0003,I0004,共8页
Four acrylamide polymer flocculants, anionic polyacrylamide P(AA-co-AM), cationic poly- acrylamide P(DMB-co-AM), nonionic polyacrylamide P(AM), and hydrophobical polyacry- lamide P(OA-co-AM) have been prepared... Four acrylamide polymer flocculants, anionic polyacrylamide P(AA-co-AM), cationic poly- acrylamide P(DMB-co-AM), nonionic polyacrylamide P(AM), and hydrophobical polyacry- lamide P(OA-co-AM) have been prepared by copolymerizing with acrylic acid, cationic monomer dimethylethyl (acryloxyethyl) ammonium bromide (DMB) and hydrophobical monomer octadecyl acrylate with acrylamide. The interactions between the flocculants with the (012) surface of alumina crystal (A1203) have been simulated by molecular dynamics method. All the polymers can bind tightly with A1203 crystal, the interaction between the O of polymers and A1 of the (012) surface of A1203 is significantly strong. The order of binding energy is as follows: P(DMB-co-AM)〉P(OA-co-AM)〉P(AA-co-AM)〉P(AM), implying a better flocculation performance of P(DMB-co-AM) than the others. Analy- sis indicates that binding energy is mainly determined by Coulomb interaction. Bonds are found between the O atoms of the polymers and the A1 atoms of A1203. The poly- mers' structures deform when they combine with A1203 crystal, but the deformation en- ergies are low and far less than non-bonding energies. Flocculation experiments in sus- pension medium of l%Kaolin show a transmittancy of 90.8% for 6 mg/L P(DMB-co-AM) and 73.0% for P(AM). The sequence of flocculation performance of four polymers is P(DMB-co-AM)〉P(OA-co-AM)〉P(AA-co-AM)〉P(AM), which is in excellent agreement with the simulation results of binding energy. 展开更多
关键词 Molecular dynamics simulation Acrylamide copolymer Binding energy Floc-culation
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Ti:Al_2O_3晶体紫外及可见光谱的浓度效应研究 被引量:5
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作者 刘建华 祁长鸿 +1 位作者 邓佩珍 干福熹 《光学学报》 EI CAS CSCD 北大核心 1995年第1期103-107,共5页
通过对不同浓度的Ti:Al2O3晶体紫外吸收光谱,可见偏振荧光光谱及其激发光谱的研究,发现峰值420nm的宽带可见荧光,室温下较强的σ偏振光在低温(77K)下变得比π偏振光弱。在液氮温度下π偏振光谱分裂成330nm,... 通过对不同浓度的Ti:Al2O3晶体紫外吸收光谱,可见偏振荧光光谱及其激发光谱的研究,发现峰值420nm的宽带可见荧光,室温下较强的σ偏振光在低温(77K)下变得比π偏振光弱。在液氮温度下π偏振光谱分裂成330nm,420nm,460nm,560nm等子荧光带。研究认为,这些发光带分别与色心(F+,F心)及Ti(4+)离子的电荷转移跃迁有关。并且室温下可见荧光具有的较强的浓度猝灭及现象来源于Ti(4+)离子的浓度猝灭及Ti(3+)离子的吸收增强两个因素。峰值于266nm的吸收带是Ti(4+),Fe(2+)离子的电荷转移吸收。 展开更多
关键词 掺钛氧化铝晶体 紫外光谱 可见光谱 浓度效应
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Low voltage organic devices and circuits with aluminum oxide thin film dielectric layer 被引量:2
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作者 SHANG LiWei JI ZhuoYu +4 位作者 CHEN YingPin WANG Hong LIU Xin HAN MaiXin LIU Ming 《Science China(Technological Sciences)》 SCIE EI CAS 2011年第1期95-98,共4页
Low voltage operating organic devices and circuits have been realized using atomic layer deposition deposited aluminum oxide thin film as dielectric layer. The dielectric film has per unit area capacitance of 165 nF/c... Low voltage operating organic devices and circuits have been realized using atomic layer deposition deposited aluminum oxide thin film as dielectric layer. The dielectric film has per unit area capacitance of 165 nF/cm2 and leakage current of 1 nA/cm2 at 1 MV/cm. The devices and circuits use the small-molecule hydrocarbon pentacene as the active semiconductor material. Transistors,inverters,and ring oscillators with operating voltage lower than 5 V were obtained. The mobility of organic field-effect transistors was extracted to be 0.16 cm2/Vs in saturation range,the threshold voltage is 0.3 V,and the on/off current ratio is larger than 105. The gain of inverters is estimated to be 12 at -5 V supply voltage,and the propagation delay is 0.25 ms per stage in 5-stage ring oscillators. 展开更多
关键词 OFET low voltage atomic layer deposition Al2O3 thin film high-k dielectric
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