The azaanalog of copper phthalocyanine（azaCuPc） complex C 24H 8CuN 16 was prepared by the so- lid phase synthesis technology and its single crystals was characterized by high power Xray from the synchrotron radi...The azaanalog of copper phthalocyanine（azaCuPc） complex C 24H 8CuN 16 was prepared by the so- lid phase synthesis technology and its single crystals was characterized by high power Xray from the synchrotron radiation. The crystal belongs to monoclinic system, space group P21/n with a=1.612 3（3） nm, b= 0.529 40（11） nm, c=1.906 4（4） nm, β=105.25（3）°, V=1.569 9（5） nm, Z=2, Mr=584.00, Dc=1.235 g/cm3, F（000）=586, the final R=0.063 1 and wR=0.153 9 for 757 observed reflections with I>2σ（I）, GOF=1.340.展开更多
文摘The azaanalog of copper phthalocyanine（azaCuPc） complex C 24H 8CuN 16 was prepared by the so- lid phase synthesis technology and its single crystals was characterized by high power Xray from the synchrotron radiation. The crystal belongs to monoclinic system, space group P21/n with a=1.612 3（3） nm, b= 0.529 40（11） nm, c=1.906 4（4） nm, β=105.25（3）°, V=1.569 9（5） nm, Z=2, Mr=584.00, Dc=1.235 g/cm3, F（000）=586, the final R=0.063 1 and wR=0.153 9 for 757 observed reflections with I>2σ（I）, GOF=1.340.
