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提取方式对土壤和植物水分提取率的影响及其氢氧同位素分析 被引量:12
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作者 刘文茹 沈业杰 +1 位作者 彭新华 陈效民 《生态学杂志》 CAS CSCD 北大核心 2012年第7期1870-1875,共6页
氢氧同位素示踪技术是研究土壤-作物-大气连续体(SPAC)水分循环的重要手段,而土壤水和作物水的提取方法是氢氧同位素研究最关键的一步。本文采用真空蒸馏和共沸蒸馏2种提取方法对不同含水量(35%、25%和15%)下的土壤(红粘土、红砂土和水... 氢氧同位素示踪技术是研究土壤-作物-大气连续体(SPAC)水分循环的重要手段,而土壤水和作物水的提取方法是氢氧同位素研究最关键的一步。本文采用真空蒸馏和共沸蒸馏2种提取方法对不同含水量(35%、25%和15%)下的土壤(红粘土、红砂土和水稻土)和植物(橘树和水稻)茎叶的水分分别进行了提取,并对提取出的水分进行了氢氧稳定同位素的对比分析,旨在提出合适的提取方法。结果表明:真空蒸馏对土壤和植物水分提取率显著高于共沸蒸馏(P<0.001);土壤含水量和土壤类型对水分提取率影响不显著;而水稻水分提取率显著高于橘树(P<0.001),且叶的水分提取率显著高于茎(P<0.001)。真空蒸馏提取出土壤水分的δD和δ18O值与标准样的差异不显著,而共沸蒸馏下提取出土壤水分的δD与标准样差异显著(P<0.001),水稻叶和橘树叶的δD和δ18O值高于茎。研究表明,真空蒸馏比共沸蒸馏更适合土壤和植物水分的提取且其提取出的水分更能真实反映样品中氢氧同位素组成。 展开更多
关键词 真空蒸馏 共沸蒸馏 水分提取 氢氧同位素
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葡萄酒中水分的冷冻离心提取法
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作者 孙海波 王绍清 +1 位作者 王琳琳 林立 《食品工业科技》 CAS CSCD 北大核心 2013年第13期113-115,共3页
为从葡萄酒中提取用于稳定氢氧同位素测定的水分,本研究开发了冷冻离心与活性炭吸附结合的方法,经该方法处理的葡萄酒样品中乙醇、色素及其他有机物接近完全去除;并且实验证明该分离方法没有引起葡萄酒样品的稳定氢氧同位素的分馏。因... 为从葡萄酒中提取用于稳定氢氧同位素测定的水分,本研究开发了冷冻离心与活性炭吸附结合的方法,经该方法处理的葡萄酒样品中乙醇、色素及其他有机物接近完全去除;并且实验证明该分离方法没有引起葡萄酒样品的稳定氢氧同位素的分馏。因此用该方法提取的水分能够用于葡萄酒中水分的稳定氢氧同位素比测定。 展开更多
关键词 葡萄酒 水分提取 冷冻-离心 稳定氢氧同位素
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Application of 3D stereotomography to the deep-sea data acquired in the South China Sea:a tomography inversion case 被引量:2
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作者 邢逢源 杨锴 +2 位作者 薛冬 汪小将 陈宝书 《Applied Geophysics》 SCIE CSCD 2017年第1期142-153,191,192,共14页
A 3D stereotomography algorithm, which is derived from the 3D Cartesian coordinate, is applied for the first time to the deep-sea data acquired in the LH area, South China Sea, to invert a macro velocity model for pre... A 3D stereotomography algorithm, which is derived from the 3D Cartesian coordinate, is applied for the first time to the deep-sea data acquired in the LH area, South China Sea, to invert a macro velocity model for pre-stack depth migration. The successful implementation of stereotomography is highly dependent on the correct extraction of slowness components and the proper application of regularization terms. With the help of the structure tensor algorithm, a high-quality 3D stereotomography data space is achieved in a very efficient manner. Then, considering that the horizontal slowness in cross-line direction is usually unavailable for 3D narrow-azimuth data, the regularization terms must be enhanced to guarantee a stable convergence of the presented algorithm. The inverted model serves as a good model for the 3D pre-stack depth migration. The synthetic and real data examples demonstrated the robustness and effectiveness of the presented algorithm and the related schemes. 展开更多
关键词 3D stereotomography structure tensor extraction of horizontal components of slowness REGULARIZATION
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Classification of underwater still objects based on multi-field features and SVM 被引量:4
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作者 TIAN Jie XUE Shan-hua HUANG Hai-ning ZHANG Chun-hua 《Journal of Marine Science and Application》 2007年第1期36-40,共5页
A Support Vector Machine is used as a classifier to the automatic detection and recognition of underwater still objects. Discrimination between the objects can be transferred into different projection spaces by the pr... A Support Vector Machine is used as a classifier to the automatic detection and recognition of underwater still objects. Discrimination between the objects can be transferred into different projection spaces by the process of multi-field feature extraction. The multi-field feature vector includes time-domain, spectral, time-frequency distribution and bi-spectral features. Underwater target recognition can be considered as a problem of small sample recognition. SVM algorithm is appropriate to this kind of problems because of its outstanding generalizability. The SVM is contrasted with a Gaussian classifier and a k-nearest classifier in some experiments using real data of lake or sea trial. The experimental results indicate that SVM is better than the others two. 展开更多
关键词 underwater still objects CLASSIFICATION feature support vector machine (SVM)
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Extraction of Astaxanthin from Euphausia pacific Using Subcritical 1,1,1,2-tetrafluoroethane 被引量:5
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作者 HAN Yuqian MA Qinchuan +1 位作者 WANG Lan XUE Changhu 《Journal of Ocean University of China》 SCIE CAS 2012年第4期562-568,共7页
Euphausia pacific is an important source of natural astaxanthin. Studies were carried out to assess the extractability of astaxanthin from E. pacific using subcritical 1, 1, 1,2-tetrafluoroethane (R134a). To examine... Euphausia pacific is an important source of natural astaxanthin. Studies were carried out to assess the extractability of astaxanthin from E. pacific using subcritical 1, 1, 1,2-tetrafluoroethane (R134a). To examine the effects of multiple process variables on the extraction yield, astaxanthin was extracted under various conditions of pressure (30-150bar), temperature (303-343 K), time (10-50rain), flow rate (2-10gmin-1), moisture content (5.5%-63.61%), and particle size (0.25-0.109mm). The results showed that the extraction yield increased with temperature, pressure, time and flow rate, but decreased with moisture content and particle size. A maximum yield of 87.74% was obtained under conditions of 100bar, 333K, and 30min with a flow rate of 6gmin-1 and a moisture content of 5.5%. The substantial astaxanthin yield obtained under low-pressure conditions demonstrates that subcritical R134a is a good alternative to CO2 for extraction of astaxanthin from E. pacific. 展开更多
关键词 subcritical R134a astaxanthin extraction Euphausia pacific
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Cluster analysis of the domain of microseismic event attributes for fl oor water inrush warning in the working face
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作者 Shang Guo-Jun Liu Xiao-Fei +3 位作者 Li Li Zhao Li-Song Shen Jin-Song Huang Wei-Lin 《Applied Geophysics》 SCIE CSCD 2022年第3期409-423,471,472,共17页
Differences are found in the attributes of microseismic events caused by coal seam rupture,underground structure activation,and groundwater movement in coal mine production.Based on these differences,accurate classific... Differences are found in the attributes of microseismic events caused by coal seam rupture,underground structure activation,and groundwater movement in coal mine production.Based on these differences,accurate classification and analysis of microseismic events are important for the water inrush warning of the coal mine working facefloor.Cluster analysis,which classifies samples according to data similarity,has remarkable advantages in nonlinear classification.A water inrush early warning method for coal minefloors is proposed in this paper.First,the short time average over long time average(STA/LTA)method is used to identify effective events from continuous microseismic records to realize the identification of microseismic events in coal mines.Then,ten attributes of microseismic events are extracted,and cluster analysis is conducted in the attribute domain to realize unsupervised classification of microseismic events.Clustering results of synthetic andfield data demonstrate the effectiveness of the proposed method.The analysis offield data clustering results shows that thefirst kind of events with time change rules is of considerable importance to the early warning of water inrush from the coal mine working facefloor. 展开更多
关键词 signal detection attribute extraction cluster analysis and water disaster warning
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Water bodies extraction from TM images
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作者 杜先荣 《Journal of Measurement Science and Instrumentation》 CAS 2014年第3期48-52,共5页
Aiming at the problems of high time-consuming, low accuracy and weak versatility of the existing methods of wa- ter extraction based on TM image, this paper combines principal component analysis (PCA) with the modif... Aiming at the problems of high time-consuming, low accuracy and weak versatility of the existing methods of wa- ter extraction based on TM image, this paper combines principal component analysis (PCA) with the modified normalized difference water index (MNDWI) which was improved by XU Han-qiu to construct a false color composite image that could separate water from others easily. This method can realize the water extraction based on TM image by analyzing the spectral characteristics of water in this false color image and establishing a water extraction model. This paper also compares the effi- ciency of this method with MNDWI, (TM2 + TM3) - (TM4 + TM5) and new water index (NWI), which were applied in the city and mountain of Taiyuan, respectively. The results show that the proposed method can extract water body from TM im- age more rapidly and efficiently and its accuracy is up to 94.03 %. In addition, this method does not require a manual selec- tion threshold, which meets the research reuuirement of high automaticm. 展开更多
关键词 TM image water extraction principal component analysis (PCA) modified normalized difference water index(MNDWI)
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Antiplasmodial Activity and Phytochemical Analysis of Phyllanthus niruri L. (Phyllanthaceae) and Morinda lucida Benth (Rubiaceae) Extracts
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作者 Rufin Nakweti Kikakedimau Patrick Doumas +5 位作者 Hity Mutambel AimeNdofunsu Diamuini Freddy Otono ABulubulu Joce1in Akalomia Kikalulu Sebastien Ndiku Luyindula Richard Kanyanga Cimanga 《Journal of Agricultural Science and Technology(A)》 2012年第3期373-383,共11页
The antiplasmodial activity and phytochemical analysis of P. niruri and All. lucida leaves and stem parts have been evaluated in different solvent (aqueous, ethanolic and dichloromethane). Phytochemical analysis has... The antiplasmodial activity and phytochemical analysis of P. niruri and All. lucida leaves and stem parts have been evaluated in different solvent (aqueous, ethanolic and dichloromethane). Phytochemical analysis has been done using 5-methoxyflavone 10-4 M andα-gluconolactone 10-4 M in methanol 80% (pH 2) solvent to the HPLC (high performance liquid chromatography) and the TLC (thin layer chromatography). RPMI 1640 (Rose Park Memorial Institute medium 1640) has been used for plasmodium strain culture and the antiplasmodial activity has been evaluated under microscopy with infected blood colored by Giemsa-stained thick. IC50 (The inhibitory concentration of extract would be killed 50% of parasites) was estimated. The results show that extracts of P. niruri exhibit more antiplasmodial activities (IC50:3.98 μg/50 μL for aqueous extract, between 9.5-19 μg/50 p.L for ethanolic extract and 5.3 Itg/50 laL for dichloromethane extract) than those of M. lucida (IC50:5.39 to 10.78 μg/50 μL, 12.265 μg/50 μL and 24.53 μg/50 μL) successively for queous, ethanolic and dichloromethane extracts. For the same antiplasmodial activity, the amount of extract of M. lucida is still higher than that of P. niruri. These results are explained by the composition of phenolic compounds that are found in P. niruri. This plant has therefore presented more spectra in the chromatogram (20 peaks for hydrolyzed extract and 27 peaks for unhydrolyzed extracts) comparing that ofM. lucida hydrolyzed or unhydrolyzed extracts with 13 and 14 peaks. TLC revealed compounds such as flavonols, flavan-3-ols. Nevertheless, quinine used as positive control presented the same antiplasmodial activity for the low doses for the drugs and our extracts presented weak antiplasmodial activity comparing previous works. The studies could continue for the isolation of active principle that of P. niruri. 展开更多
关键词 Antiplasmodial activity phytochemical analysis Phyllanthus niruri Morinda lucida malaria.
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Research on the Summer Drought in Chongqing Using MODIS-EVI Time Series Data
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作者 易佳 高阳华 +1 位作者 杨世琦 田永中 《Agricultural Science & Technology》 CAS 2010年第7期124-127,167,共5页
MODIS-EVI time series data from 2000 to 2009 in Chongqing were selected for this study.By the use of best index slope extraction (BISE) method for cloud elimination,analysis on the change vector of EVI time series d... MODIS-EVI time series data from 2000 to 2009 in Chongqing were selected for this study.By the use of best index slope extraction (BISE) method for cloud elimination,analysis on the change vector of EVI time series data were conducted to investigate the EVI response on drought; then,four typical regions were selected to study the relationship between precipitation,temperature and EVI when the sever drought occurred in 2006; finally,based on the time series of vegetation condition index (VCI) and precipitation abnormity percentage,the temporal and spatial distributions of drought were studied.The results showed that,the EVI value of the summer in 2006 was significantly lower than the average EVI at the corresponding period of the other years in Chongqing.In addition,summer drought occurred mainly during the hot and dry weather.Except the southeast area,most of the other regions in Chongqing were all under severe drought. 展开更多
关键词 Time series of vegetation condition index Precipitation abnormity percentage Best index slope extraction CHONGQING
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A Rapid Extraction Procedure for the Determination of Strontium-90 in Water Samples
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作者 Markus Zehringer Johannes Abraham +2 位作者 Franziska Kammerer Vlora Syla Michael Wagmann 《Journal of Chemistry and Chemical Engineering》 2017年第3期116-123,共8页
A beta spectrometric method for the rapid determination of strontium-90 (90Sr) in water samples was developed and tested. 90Sr is extracted directly from the water samples by means of a scintillator cocktail, contai... A beta spectrometric method for the rapid determination of strontium-90 (90Sr) in water samples was developed and tested. 90Sr is extracted directly from the water samples by means of a scintillator cocktail, containing the crown ether dicyclohexano-18-crown-6 as an extracting agent (STRONEX). Minimal clean-up is necessary when other beta nuclides are present, such as barium-140. These nuclides are eliminated by a barium chromate scavenge, prior to the extraction step. The method presented here allows for the investigation of at least 12 water samples a day and is therefore a suitable tool for emergency analysis. 展开更多
关键词 STRONTIUM-90 beta spectrometry emergency analysis STRONEX.
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Comparative Study on the Antibacterial Activity of Fresh and Fallen Leaves of Terminalia catappa L.
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作者 O. A. Ladokun M. O. Ojezele 《Journal of Agricultural Science and Technology(A)》 2011年第2X期217-220,共4页
In the work reported here, the potential of different methods (cold and hot water, and ethanolic) of extraction of Indian almond (Terminalia catappa L.), fresh and fallen leaves as an anti-bacterial agent was inve... In the work reported here, the potential of different methods (cold and hot water, and ethanolic) of extraction of Indian almond (Terminalia catappa L.), fresh and fallen leaves as an anti-bacterial agent was investigated. The hot water extract did not show any spectrum of activity against the selected bacteria while the cold water extract showed slight antibacterial activity suggesting that the effective components are heat labile. The ethanolic extracts of the leaves have higher antibiotic spectrum of activity than the cold water extract showing ethanol to be a better solvent in extracting the effective component. The fallen leaves seem to have a higher concentration of the effective component against the bacteria while ethanolic extract of the fresh leaves have similar spectrum of activity to Ciprofloxacin and Nitrofuratoin. These suggest that some effective components are lost when leaves fall off while some seem to increase in concentration. Fresh and fallen leaves contain tannin and flavonoids. In addition, the fallen leaves contain flavones. This might be responsible for the higher activity of fallen leaves extract observed against Pseudomonas and Staphylococcus spp. in our study. Combined use of extracts from fresh and fallen leaves broadened the spectrum of activity. 展开更多
关键词 Natural resources management Terminalia catappa leaves EXTRACTION antibacterial activity.
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A Comparative Study of Flavonoid Water-Ethanol Extraction Process in Planted Trollius Chinensis 被引量:1
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作者 Yongfeng Liang 《International Journal of Technology Management》 2014年第8期167-170,共4页
With rutin standard sample as the comparison, flavonoid extraction rate as an indicator, UV-2450 ultraviolet visible light spectrophotometer to measure flavonoid content in planted Trollius chinensis through orthogona... With rutin standard sample as the comparison, flavonoid extraction rate as an indicator, UV-2450 ultraviolet visible light spectrophotometer to measure flavonoid content in planted Trollius chinensis through orthogonal experiment, this experiment optimizes process condition of flavonoid in Trollius chinensis through water extraction and ethanol extraction. The result shows that flavonoid extraction rate of Trollius chinensis through ethanol extraction method is obviously higher than water extraction, and the optimal extraction process condition is: ethanol concentration is 75%, extraction time is 90min, extraction times are 3, and fluid material ratio is 20:1. 展开更多
关键词 planted Trollius chinensis flavonoid water extraction ethanol extraction method process study
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Intrinsic mode characteristic analysis and extraction in underwater cylindrical shell acoustic radiation 被引量:4
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作者 LIU QingYu FANG ShiLiang +3 位作者 CHENG Qiang CAO Jin AN Liang LUO XinWei 《Science China(Physics,Mechanics & Astronomy)》 SCIE EI CAS 2013年第7期1339-1345,共7页
Target dimension is important information in underwater target classification. An intrinsic mode characteristic extraction method in underwater cylindrical shell acoustic radiation was studied in this paper based on t... Target dimension is important information in underwater target classification. An intrinsic mode characteristic extraction method in underwater cylindrical shell acoustic radiation was studied in this paper based on the mechanism of shell vibration to gain the information about its dimension instead of accurate inversion processing. The underwater cylindrical shell vibration and acoustic radiation were first analyzed using mode decomposition to solve the wave equation. The characteristic of acoustic radiation was studied with different cylindrical shell lengths, radii, thickness, excitation points and fine structures. Simulation results show that the intrinsic mode in acoustic radiation spectrum correlates closely with the geometry dimensions of cylindrical shells. Through multifaceted analysis, the strongest intrinsic mode characteristic extracted from underwater shell acoustic radiated signal was most likely relevant to the radiated source radius. Then, partial information about unknown source dimension could be gained from intrinsic mode characteristic in passive sonar applications for underwater target classification. Experimental data processing results verified the effectiveness of the method in this paper. 展开更多
关键词 cylindrical shell mode decomposition acoustic radiation characteristic
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Comparative Study of Antimicrobial Activity and Phytochemical Analysis of Methanolic and Aqueous Extracts of the Fruit of Emblica Officinalis against Pathogenic Bacteria 被引量:4
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作者 Avneesh Kumar Bilal Ahmd Tantry +1 位作者 Shiak Rahiman Upasna Gupta 《Journal of Traditional Chinese Medicine》 SCIE CAS CSCD 2011年第3期246-250,共5页
Objective:To investigate antimicrobial potential of aqueous(infusions,decoctions) and methanlic extracts(1:2 and 1:5 concentrations) of Emblica officinalis(amla) against seven pathogenic bacteria namely Staph... Objective:To investigate antimicrobial potential of aqueous(infusions,decoctions) and methanlic extracts(1:2 and 1:5 concentrations) of Emblica officinalis(amla) against seven pathogenic bacteria namely Staphylococcs aureus,Staphylococcus saprophyticus,Escherichia coli,Enterococcus faecalis,Enterococcus cloacae,Proteus vulgaris and Klebsiella pneumoniae.Methods:The well diffusion technique was employed.The minimum inhibitory concentration(MIC) was determined using micro-broth dilution methods and phytochemical screening was done as per standard procedures.Results:Aqueous infusion extract of amla exhibited potent antimicrobial activity against E.cloacae followed by E.coli.Preliminary phytochemical analysis of E.officinalis aqueous extracts(infusions and decoctions) only showed presence of tannins,saponins,flavanoids,Terpenoids and phenols.MIC of aqueous extract of E.officinalis was most active against K.pneumoniae.Whereas MIC of methanol extract of E.officinalis shows maximum activity against E.coli.Conclusion:Emblica officinalis definitely possesses potent antimicrobial activities and this can serve as an important platform for the development of inexpensive,safe and effective medicines 展开更多
关键词 Emblica officinalis INFUSION DECOCTION traditional medicine
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Bench-top aqueous two-phase extraction of isolated individual single-walled carbon nanotubes 被引量:2
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作者 Navaneetha K. Subbaiyan A. Nicholas G. Parra-Vasquezt +7 位作者 Sofie Cambre Miguel A. Santiago Cordoba Sibel Ebru Yalcin Christopher E. Hamilton Nathan H. Mack Jeffrey L. Blackburn Stephen K. Doorn Juan G. Duque 《Nano Research》 SCIE EI CAS CSCD 2015年第5期1755-1769,共15页
Isolation and purification of single-walled carbon nanotubes (SWCNTs) are prerequisites for their implementation in various applications. In this work, we present a fast (-5 min), low-cost, and easily scalable ben... Isolation and purification of single-walled carbon nanotubes (SWCNTs) are prerequisites for their implementation in various applications. In this work, we present a fast (-5 min), low-cost, and easily scalable bench-top approach to the extraction of high-quality isolated SWCNTs from bundles and impurities in an aqueous dispersion. The extraction procedure, based on aqueous two-phase (ATP) separation, is widely applicable to any SWCNT source (tested on samples up to 1.7 nm in diameter) and independent of defect density, purity, diameter, and length. The extracted dispersions demonstrate that the removal of large aggregates, small bundles, and impurities is comparable to that by density gradient ultracentrifugation, but without the need for high-end instrumentation. Raman and fluorescence-excitation spectroscopy, single-nanotube fluorescence imaging, atomic force and transmission electron microscopy, and thermogravimetric analysis all confirm the high purity of the isolated SWCNTs. By predispersing the SWCNTs without sonication (only gentle stirring), full-length, pristine SWCNTs can be isolated (tested up to 20 μm). Hence, this simple ATP method will find immediate application in the generation of SWCNT materials for all levels of nanotube research and applications, from fundamental studies to high-performance devices. 展开更多
关键词 carbon nanotubes aqueous two-phase (ATP)separation aggregate removal isolation SORTING
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