A rapid and continuous method for production of LiFePO4/C nanoparticles in super heated water is described, wherein soluble starch was used as carbon precursor. The effects of pH, flow rate, temperature, and pressure ...A rapid and continuous method for production of LiFePO4/C nanoparticles in super heated water is described, wherein soluble starch was used as carbon precursor. The effects of pH, flow rate, temperature, and pressure on the formation of LiFePO4/C particles were investigated. Results showed that the pH value was the key factot on the formation of phase pure LiFePO4, which only formed at pH = 7; the LiFePO4/C-occurred as particles with about 70-200 nm size and LiFePO4 was covered by a thin carbon layer; higher flow rate, higher pressure, and lower temperature led to smaller particles of LiFePO4/C.展开更多
基金Supported by Shanghai Special Foundation on Nanomaterials (0243nm305)
文摘A rapid and continuous method for production of LiFePO4/C nanoparticles in super heated water is described, wherein soluble starch was used as carbon precursor. The effects of pH, flow rate, temperature, and pressure on the formation of LiFePO4/C particles were investigated. Results showed that the pH value was the key factot on the formation of phase pure LiFePO4, which only formed at pH = 7; the LiFePO4/C-occurred as particles with about 70-200 nm size and LiFePO4 was covered by a thin carbon layer; higher flow rate, higher pressure, and lower temperature led to smaller particles of LiFePO4/C.
