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基于拉曼光谱技术的山茶油不饱和度快速评价方法
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作者 马静静 田春 +4 位作者 陈江琳 李家伟 张运斌 侯如燕 金龙 《食品工业科技》 CAS 北大核心 2024年第11期205-212,共8页
为评价不同品种山茶油不饱和程度,有必要建立一种窄碘值范围(碘值差异小于10)的快速评价方法。本文以39组山茶油样品,10组市售油脂为研究对象,建立了一种基于线性回归、梯度下降法的高分辨拉曼光谱油脂碘值快速定量预测模型。采集不同... 为评价不同品种山茶油不饱和程度,有必要建立一种窄碘值范围(碘值差异小于10)的快速评价方法。本文以39组山茶油样品,10组市售油脂为研究对象,建立了一种基于线性回归、梯度下降法的高分辨拉曼光谱油脂碘值快速定量预测模型。采集不同饱和度的油脂样品在785 nm的拉曼谱图,采用平滑算法最小二乘平滑滤波(Savitzky-Golay)、多项式拟合和去卷积算法洛伦兹(Lorentzian)处理谱图信息。以筛选出的两个拉曼特征峰(1656 cm^(-1)和1440 cm^(-1))的峰强比值(I 1656/1440)作为不饱和度评价指标,结合传统滴定法测得的碘值数据进行相关性分析,所建定量模型测试集的决定系数(R^(2))>0.82,均方误差(MSE)<0.73,均方根误差(RMSE)<0.85,可准确、快速地评价山茶油等油脂的不饱和度。 展开更多
关键词 拉曼光谱 山茶油 油脂不饱和度 碘值 定量预测模型
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Total Replacement of Fish Oil with Vegetable Oils in the Diet of Juvenile Jade Perch Scortum barcoo Reared in Recirculating Aquaculture Systems 被引量:11
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作者 Stijn Van Hoestenberghe Ivo Roelants +1 位作者 Daniel Vermeulen Bruno Maria Goddeeris 《Journal of Agricultural Science and Technology(B)》 2013年第5期385-398,共14页
To determine the replacement of fish oil with vegetable oils in the diet of juvenile Jade perch Scortum barcoo, four feeds with each a different oil (fish, sunflower, linseed and a mixture of 75% canola and 25% linse... To determine the replacement of fish oil with vegetable oils in the diet of juvenile Jade perch Scortum barcoo, four feeds with each a different oil (fish, sunflower, linseed and a mixture of 75% canola and 25% linseed oil), were fed to Jade perch reared in recirculating aquaculture systems (RAS). The trial lasted for 10 weeks and the fatty acid (FA) profile of both feed and fish muscle tissue were examined. There was no difference in growth, feed conversion rate (FCR) and mortality. The fish grew from 10 g to 110 g with a FCR of 1.25 and 0 mortality. The FA profile of the fish muscle tissue reflected the FA profile of the feed. The flesh of the fish that were fed the linseed oil diet, were extremely high in omega-3 (n-3) polyunsaturated FA (n-3 PUFA) with 3.75% of wet weight. This is one of the highest concentrations of n-3 PUFA ever recorded in fish flesh. In a finishing feeding test, the remaining vegetable oil fed fish were fed the fish oil diet for another two weeks immediately after the 10 weeks trial, to check for a possible recovery of n-3 highly unsaturated fatty acids (HUFA). The wash out rate of FA towards n-3 HUFA in the muscle tissue was about 25% over this two weeks period. 展开更多
关键词 Recirculating aquaculture system fish oil replacement fatty acid synthesis feed conversion ratio omega 3 fatty acids long chain fatty acid recovery.
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Response of Hypercholesterolemic Rats to Sesamum indicum Linn Seed Oil Supplemented Diet
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作者 Olubunmi Bolanle Ajayi James Braimoh Karen Olasunkanmi 《Journal of Life Sciences》 2012年第11期1214-1219,共6页
Fatty acid composition of Sesamum indicum oil was determined by gas chromatography and the response of hypercholesterolemic rats to diet supplemented with Sesamum indicum seed oil was investigated. Twenty four rats we... Fatty acid composition of Sesamum indicum oil was determined by gas chromatography and the response of hypercholesterolemic rats to diet supplemented with Sesamum indicum seed oil was investigated. Twenty four rats weighing between 120-130 g were randomly assigned into four groups. Group A was fed normal diet, Group B, C and D were fed hypercholesterolemic diet (i.e. 20% fat + 1% cholesterol) for two weeks to establish hypercholesterolemia. Group B were maintained on hyper diet while C and D were fed 5% and 10% benniseed oil supplemented diet for four weeks. Plasma was collected and analyzed for TC (total cholesterol), HDL-C (high density lipoprotein), LDL-C (low density lipoprotein) and TG (triglycerides) levels. Linoleic acid (42.44%) and oleic acid (40.60%) were the major unsaturated fatty acid in the oil. Significant increase (P 〈 0.05) was observed in the TC, TG, LDL and LDL/HDL ratio of the hypercholesterolemic rats compared to the normal control. Supplementation with Sesamum indicum seed oil at 5% and 10% levels resulted in significant decrease (P 〈 0.05) in TC, TG, LDL and LDL/HDL ratio, and significant increase in the HDL-C. The high level of unsaturated fatty acid in the oil may in part be responsible for the hypocholesterolemic effect of the oil. 展开更多
关键词 Sesamum indicum fatty acid composition HYPERCHOLESTEROLEMIA lipid profile.
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食用油和煎炸油空芯光纤拉曼检测系统研究 被引量:4
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作者 王为 陈盼 +3 位作者 刘炳红 汤晓黎 朱晓松 石艺尉 《光学学报》 EI CAS CSCD 北大核心 2015年第9期73-81,共9页
基于食用油质量检测背景,使用内表面镀银空芯光纤作为传感腔,设计和搭建了食用油和煎炸油拉曼光谱检测系统。对系统的拉曼散射光强进行了理论建模,通过理论仿真与实验数据讨论了空芯光纤长度的优化。使用系统对常见食用油和小吃摊油进... 基于食用油质量检测背景,使用内表面镀银空芯光纤作为传感腔,设计和搭建了食用油和煎炸油拉曼光谱检测系统。对系统的拉曼散射光强进行了理论建模,通过理论仿真与实验数据讨论了空芯光纤长度的优化。使用系统对常见食用油和小吃摊油进行了拉曼光谱采集与分析,引入了衡量油脂不饱和度的参数I3005/I2897。对某品牌大豆油的不饱和度参数采集实验发现,该油样不饱和度参数随煎炸时长增加明显降低。提供了一种灵敏高效的检测系统,可实现食用油和煎炸油结构分析及油脂不饱和度评估,拉曼光谱特征峰清晰尖锐,为样品的结构分析提供了有效手段,可应用于食品安全检测领域。 展开更多
关键词 光纤光学 空芯光纤 拉曼光谱 油脂不饱和度 特征峰
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