A simple, rapid and sensitive flow injection chemiluminescence （FI-CL） method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium pe...A simple, rapid and sensitive flow injection chemiluminescence （FI-CL） method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium permanganate in a hydrochloric acid medium, enhanced by formaldehyde （HCHO）. Under optimum conditions, calibration curve over the range of 1.0-20.0μg/mL was obtained. The proposed method was successfully applied to the determination of meloxicam in capsules with no evi- dence of interference from common excipients. The detection limit of this method was 25.6 ng/mL. The relative standard deviation was 2.1% for 10.0 μg/mL meloxicam. The sample throughput was found to be 120 samples/h.展开更多
In reversed-phase high performance liquid chromatography （RP-HPLC）, the mobile phase condition for separating eight isoflavones （daidzin, glycitin, genistin, 6＇-o-acetyl daidzin, 6＇-o-malonyl genistin, daidzein, ...In reversed-phase high performance liquid chromatography （RP-HPLC）, the mobile phase condition for separating eight isoflavones （daidzin, glycitin, genistin, 6＇-o-acetyl daidzin, 6＇-o-malonyl genistin, daidzein, glycitein and genistein） was optimized using the HCI （High-Purity Separation Laboratory, Department of Chemical Engineering, Inha University） program software. The optimum composition of mobile phase for the separation of the eight isoflavones was obtained. The elution profiles were calculated by the plate theory based on the equations of retention factor, In k=A＋BF＋CF2, where F was the volume percentage of acetonitrile with 0.1% acetic acid （AA）. The first mobile phase composition was water with 0.1% AA/acetonitrile with 0.1% AA （88%/12%, by volume）, followed at 9min later by the second composition of mobile phase which was step-changed to 85%/15%, at 19rain by the third composition which was step-changed to 73%/27%, at 30min when it was changed to 65%/35% and finally it was maintained in isocratic mode to the end of the run time at 50rain. Although, using step gradient mode to separate the isoflavones, the calculated and experimented data were not achieved very good agreement, we could estimate the closed retention time before experiment. And the agreement between the experimental data and the calculated values was relatively good using isocratic separation for eight isoflavones, but the retention time is very long.展开更多
This paper introduces a novel automatic physical synthesis methodology for analog circuits based on the signal-flow analysis.Circuit analysis sub-system adopts the newly advanced methodology,circuit topology analysis,...This paper introduces a novel automatic physical synthesis methodology for analog circuits based on the signal-flow analysis.Circuit analysis sub-system adopts the newly advanced methodology,circuit topology analysis,and circuit sensitivity analysis to generate layout constraints and control performance degradations.Considering the heuristic information about signal-flow,complexity of the methodology is less than the pure performance-driven methodology.And then these constraints are implemented in device generation,placement,and routing sub-systems separately,which makes the different constraints be satisfied at most easily implemented stages.Excellent circuit performance obtained by the methodology is demonstrated by practical circuit examples.展开更多
Coal is primarily beneficiated by wet gravity methods. The wet processing of coal is an efficient practice. However, it introduces the moisture in the range of 6%-15%, depending upon the size of coal which is as detri...Coal is primarily beneficiated by wet gravity methods. The wet processing of coal is an efficient practice. However, it introduces the moisture in the range of 6%-15%, depending upon the size of coal which is as detrimental as ash content to the heating value of coal. Dry beneficiation of coal fines was carried out using an air fluidized vibrating table in which the coal particles get separated from the heavier mineral particles as a result of horizontal and vertical stratification. Two level factorial design matrix was used to optimize and assess the interactive effects of the operational parameters of a pneumatic table viz. deck eccentric, side tilt and air flow rate on the clean coal yield and its ash content. Double stage processing was found to be more effective for reducing the ash content of the clean coal. Initial stage of processing at a higher ash level generates a reject of high ash with low combustibles. Cleaning of the rougher concentrate at 34%-35% ash level shows significant improvement in the organic efficiency （88.6%） and useful heat value of clean coal （15690 kJ/kg）. The performance of air fluidized vibrating deck was measured by Ep value which is 0.18.展开更多
According to the structure characteristics of foreign fibers detection system,the foreign fiber flow flux mathematical model and fiber detection system were designed.The information fusion clustering structure of fore...According to the structure characteristics of foreign fibers detection system,the foreign fiber flow flux mathematical model and fiber detection system were designed.The information fusion clustering structure of foreign fiber flow flux was put forward.The data of the pressure difference,pressure,temperature,and density sensor which had impacted on flux were integrated and output by the Adaptive Resonance Theory-2(ART-2)network and BP network to clustering analysis of output space.The clustering control strategy will keep the output flow pressure stable,when the output pressure and temperature change.展开更多
The growing trend of network virtualization results in a widespread adoption of virtual switches in virtualized environments. However, virtual switching is confronted with great performance challenges regarding packet...The growing trend of network virtualization results in a widespread adoption of virtual switches in virtualized environments. However, virtual switching is confronted with great performance challenges regarding packet classification especially in Open Flow-based software defined networks. This paper first takes an insight into packet classification in virtual Open Flow switching, and points out that its performance bottleneck is dominated by flow table traversals of multiple failed mask probing for each arrived packet. Then we are motivated to propose an efficient packet classification algorithm based on counting bloom filters. In particular, counting bloom filters are applied to predict the failures of flow table lookups with great possibilities, and bypass flow table traversals for failed mask probing. Finally, our proposed packet classification algorithm is evaluated with real network traffic traces by experiments. The experimental results indicate that our proposed algorithm outperforms the classical one in Open v Switch in terms of average search length, and contributes to promote virtual Open Flow switching performance.展开更多
Genetic algorithms and artificial neural networks method were adopted to optimize the camber line shape of splitter cascade in a transonic axial fan. For a certain type of transonic axial fan, the isentropie efficienc...Genetic algorithms and artificial neural networks method were adopted to optimize the camber line shape of splitter cascade in a transonic axial fan. For a certain type of transonic axial fan, the isentropie efficiency was improved by 0. 6% with the modification of splitter cascade rotor. Numerical simulation studies show that the curvature of the optimum splitter cascade with larger suction side is increased, the static pressure gradient is reduced, the process of flow expansion on suction surface is controlled and the separation near hub is eliminated by changing the shock wave structure. The efficiency near hub is improved by 1.3%.展开更多
A new quenching process using the cold pyrolysis gas has been proposed for the partial oxidation(POX) of methane to recover the heat. The mixing of hot product gas and cold pyrolysis gas in milliseconds is critical to...A new quenching process using the cold pyrolysis gas has been proposed for the partial oxidation(POX) of methane to recover the heat. The mixing of hot product gas and cold pyrolysis gas in milliseconds is critical to this new approach. Two most widely-used rapid mixing configurations, i.e. the jet-in-cross-flow(JICF) and impinging flow configurations, are compared in terms of mixing and quenching performances using computational fluid dynamics(CFD) coupled with detailed reaction mechanism Leeds 1.5. The mixedness, residence time distribution, temperature decreasing rate and loss ratio of acetylene during the quenching are systematically studied. The results show that the impinging flow has a more uniform mixing and narrower residence time distribution than the JICF.However, the temperature decreasing rate of the mainstream is faster in the JICF than in the impinging flow. The loss ratio of acetylene in the quenching process is 2.89% for the JICF and 1.45% for the impinging flow, showing that the impinging flow configuration is better and feasible for the quenching of POX of methane.展开更多
A chromochemical reactive mass transfer technique has been employed to study local mass transfer characteristics of structured packing. This technology adopted by experiment is an Ammonia Adsorption Method （AAM） tha...A chromochemical reactive mass transfer technique has been employed to study local mass transfer characteristics of structured packing. This technology adopted by experiment is an Ammonia Adsorption Method （AAM） that yields the surface distribution of transferred mass by analyzing the color distribution on a filter paper with the results of the color chemical reaction. A digital image processing technology is applied for data visualiza-tion. The three-dimensional plot of the local mass transfer coefficients shows that there exist three peak values on different positions of a unit cell of structured packing. In order to improve mass transfer efficiency of the structured packing, one piece of baffle is added between packing sheets. As a result, the average mass transfer coefficient increases by （10 20）% and the pressure drop decreases by （15-55）%.展开更多
In this paper, the distributions of particle velocity in a gas–solid fluidized bed with branched pipe distributor or circle distributor were measured by using a laser Doppler velocimetry. Our results show that, withi...In this paper, the distributions of particle velocity in a gas–solid fluidized bed with branched pipe distributor or circle distributor were measured by using a laser Doppler velocimetry. Our results show that, within a certain range of superficial gas velocity, when using circle distributor, the particle velocity is large and the distribution of the particle velocity is even more compared with the branched pipe distributor. On the basis of the amplitude of tangential movement statistics, the amplitude of tangential movement statistics(AVATMS) decreases with increasing the axial height under the appropriate superficial gas velocity.展开更多
Through the analysis of forces acting on the waste rock in the gas solid fluidized bed, the waste rock velocity equations and displacement equations in the gas solids fluidized bed were achieved and the influential fa...Through the analysis of forces acting on the waste rock in the gas solid fluidized bed, the waste rock velocity equations and displacement equations in the gas solids fluidized bed were achieved and the influential factors of the waste rock motion in the fluidized bed were studied in this paper. The conclusions show that the primary factors influencing the waste rock motion are the waste rock grain size and the scraper velocity according to the computer simulation. This has provided the theoretical foundation both for improving the separating effect and ascertaining the length of the separating cell.展开更多
文摘A simple, rapid and sensitive flow injection chemiluminescence （FI-CL） method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium permanganate in a hydrochloric acid medium, enhanced by formaldehyde （HCHO）. Under optimum conditions, calibration curve over the range of 1.0-20.0μg/mL was obtained. The proposed method was successfully applied to the determination of meloxicam in capsules with no evi- dence of interference from common excipients. The detection limit of this method was 25.6 ng/mL. The relative standard deviation was 2.1% for 10.0 μg/mL meloxicam. The sample throughput was found to be 120 samples/h.
文摘In reversed-phase high performance liquid chromatography （RP-HPLC）, the mobile phase condition for separating eight isoflavones （daidzin, glycitin, genistin, 6＇-o-acetyl daidzin, 6＇-o-malonyl genistin, daidzein, glycitein and genistein） was optimized using the HCI （High-Purity Separation Laboratory, Department of Chemical Engineering, Inha University） program software. The optimum composition of mobile phase for the separation of the eight isoflavones was obtained. The elution profiles were calculated by the plate theory based on the equations of retention factor, In k=A＋BF＋CF2, where F was the volume percentage of acetonitrile with 0.1% acetic acid （AA）. The first mobile phase composition was water with 0.1% AA/acetonitrile with 0.1% AA （88%/12%, by volume）, followed at 9min later by the second composition of mobile phase which was step-changed to 85%/15%, at 19rain by the third composition which was step-changed to 73%/27%, at 30min when it was changed to 65%/35% and finally it was maintained in isocratic mode to the end of the run time at 50rain. Although, using step gradient mode to separate the isoflavones, the calculated and experimented data were not achieved very good agreement, we could estimate the closed retention time before experiment. And the agreement between the experimental data and the calculated values was relatively good using isocratic separation for eight isoflavones, but the retention time is very long.
文摘This paper introduces a novel automatic physical synthesis methodology for analog circuits based on the signal-flow analysis.Circuit analysis sub-system adopts the newly advanced methodology,circuit topology analysis,and circuit sensitivity analysis to generate layout constraints and control performance degradations.Considering the heuristic information about signal-flow,complexity of the methodology is less than the pure performance-driven methodology.And then these constraints are implemented in device generation,placement,and routing sub-systems separately,which makes the different constraints be satisfied at most easily implemented stages.Excellent circuit performance obtained by the methodology is demonstrated by practical circuit examples.
文摘Coal is primarily beneficiated by wet gravity methods. The wet processing of coal is an efficient practice. However, it introduces the moisture in the range of 6%-15%, depending upon the size of coal which is as detrimental as ash content to the heating value of coal. Dry beneficiation of coal fines was carried out using an air fluidized vibrating table in which the coal particles get separated from the heavier mineral particles as a result of horizontal and vertical stratification. Two level factorial design matrix was used to optimize and assess the interactive effects of the operational parameters of a pneumatic table viz. deck eccentric, side tilt and air flow rate on the clean coal yield and its ash content. Double stage processing was found to be more effective for reducing the ash content of the clean coal. Initial stage of processing at a higher ash level generates a reject of high ash with low combustibles. Cleaning of the rougher concentrate at 34%-35% ash level shows significant improvement in the organic efficiency （88.6%） and useful heat value of clean coal （15690 kJ/kg）. The performance of air fluidized vibrating deck was measured by Ep value which is 0.18.
基金National Programon Key Basic Research Project of China(973program)(No.2010CB334711)
文摘According to the structure characteristics of foreign fibers detection system,the foreign fiber flow flux mathematical model and fiber detection system were designed.The information fusion clustering structure of foreign fiber flow flux was put forward.The data of the pressure difference,pressure,temperature,and density sensor which had impacted on flux were integrated and output by the Adaptive Resonance Theory-2(ART-2)network and BP network to clustering analysis of output space.The clustering control strategy will keep the output flow pressure stable,when the output pressure and temperature change.
基金supported in part by National Natural Science Foundation of China(61272148,61572525,61502056,and 61602525)Hunan Provincial Natural Science Foundation of China(2015JJ3010)Scientific Research Fund of Hunan Provincial Education Department(15B009,14C0285)
文摘The growing trend of network virtualization results in a widespread adoption of virtual switches in virtualized environments. However, virtual switching is confronted with great performance challenges regarding packet classification especially in Open Flow-based software defined networks. This paper first takes an insight into packet classification in virtual Open Flow switching, and points out that its performance bottleneck is dominated by flow table traversals of multiple failed mask probing for each arrived packet. Then we are motivated to propose an efficient packet classification algorithm based on counting bloom filters. In particular, counting bloom filters are applied to predict the failures of flow table lookups with great possibilities, and bypass flow table traversals for failed mask probing. Finally, our proposed packet classification algorithm is evaluated with real network traffic traces by experiments. The experimental results indicate that our proposed algorithm outperforms the classical one in Open v Switch in terms of average search length, and contributes to promote virtual Open Flow switching performance.
文摘Genetic algorithms and artificial neural networks method were adopted to optimize the camber line shape of splitter cascade in a transonic axial fan. For a certain type of transonic axial fan, the isentropie efficiency was improved by 0. 6% with the modification of splitter cascade rotor. Numerical simulation studies show that the curvature of the optimum splitter cascade with larger suction side is increased, the static pressure gradient is reduced, the process of flow expansion on suction surface is controlled and the separation near hub is eliminated by changing the shock wave structure. The efficiency near hub is improved by 1.3%.
基金Supported by the National Natural Science Foundation of China(21276135)the Project of Chinese Ministry of Education(113004A)
文摘A new quenching process using the cold pyrolysis gas has been proposed for the partial oxidation(POX) of methane to recover the heat. The mixing of hot product gas and cold pyrolysis gas in milliseconds is critical to this new approach. Two most widely-used rapid mixing configurations, i.e. the jet-in-cross-flow(JICF) and impinging flow configurations, are compared in terms of mixing and quenching performances using computational fluid dynamics(CFD) coupled with detailed reaction mechanism Leeds 1.5. The mixedness, residence time distribution, temperature decreasing rate and loss ratio of acetylene during the quenching are systematically studied. The results show that the impinging flow has a more uniform mixing and narrower residence time distribution than the JICF.However, the temperature decreasing rate of the mainstream is faster in the JICF than in the impinging flow. The loss ratio of acetylene in the quenching process is 2.89% for the JICF and 1.45% for the impinging flow, showing that the impinging flow configuration is better and feasible for the quenching of POX of methane.
文摘A chromochemical reactive mass transfer technique has been employed to study local mass transfer characteristics of structured packing. This technology adopted by experiment is an Ammonia Adsorption Method （AAM） that yields the surface distribution of transferred mass by analyzing the color distribution on a filter paper with the results of the color chemical reaction. A digital image processing technology is applied for data visualiza-tion. The three-dimensional plot of the local mass transfer coefficients shows that there exist three peak values on different positions of a unit cell of structured packing. In order to improve mass transfer efficiency of the structured packing, one piece of baffle is added between packing sheets. As a result, the average mass transfer coefficient increases by （10 20）% and the pressure drop decreases by （15-55）%.
基金Supported by the National High-Tech R&D Program of China(2011AA05A204)the Fundamental Research Funds for the Central Universities(222201717013)
文摘In this paper, the distributions of particle velocity in a gas–solid fluidized bed with branched pipe distributor or circle distributor were measured by using a laser Doppler velocimetry. Our results show that, within a certain range of superficial gas velocity, when using circle distributor, the particle velocity is large and the distribution of the particle velocity is even more compared with the branched pipe distributor. On the basis of the amplitude of tangential movement statistics, the amplitude of tangential movement statistics(AVATMS) decreases with increasing the axial height under the appropriate superficial gas velocity.
文摘Through the analysis of forces acting on the waste rock in the gas solid fluidized bed, the waste rock velocity equations and displacement equations in the gas solids fluidized bed were achieved and the influential factors of the waste rock motion in the fluidized bed were studied in this paper. The conclusions show that the primary factors influencing the waste rock motion are the waste rock grain size and the scraper velocity according to the computer simulation. This has provided the theoretical foundation both for improving the separating effect and ascertaining the length of the separating cell.
