A simple, rapid and sensitive flow injection chemiluminescence (FI-CL) method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium pe...A simple, rapid and sensitive flow injection chemiluminescence (FI-CL) method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium permanganate in a hydrochloric acid medium, enhanced by formaldehyde (HCHO). Under optimum conditions, calibration curve over the range of 1.0-20.0μg/mL was obtained. The proposed method was successfully applied to the determination of meloxicam in capsules with no evi- dence of interference from common excipients. The detection limit of this method was 25.6 ng/mL. The relative standard deviation was 2.1% for 10.0 μg/mL meloxicam. The sample throughput was found to be 120 samples/h.展开更多
Arsenic (As) is one of the most important elemental pollutants in groundwater and drinking water because it causes health problem of arsenicosis after consumption of drinking arsenic-rich water more than 5-10 years....Arsenic (As) is one of the most important elemental pollutants in groundwater and drinking water because it causes health problem of arsenicosis after consumption of drinking arsenic-rich water more than 5-10 years. Arsenic contamination of groundwater is an emerging issue in Mekong Basin including Cambodia, Vietnam, and Thailand. In Thailand, information about arsenic contamination in drinking water resources are quite rare due to that arsenic is not the main element in water qualification assay. The objective of this study is to determine groundwater quality and arsenic contamination in rural Mekong Basin, Ubon Ratchathani. Groundwater samples were collected from 20 different sampling points, between August 2009 and February 2010 in Amphoe Khemmarat, Ubon Ratchathani, Thailand. Physical and chemical characteristics of groundwater were determined. It was observed that the groundwater was 27.9-30.3 ~C, pH 5.7-6.9. The conductivity was 707-767 p.S.cm". Dissolved oxygen was 2.04-5.12 mg.L-1 and TDS was 352-384 mg.L~. The samples showed soft- to very hardness-water properties. In some area, few parameters like CI, Fe, Mn, and As exceeded the WHO guideline limits. This result represents basic information for quality of groundwater and the arsenic contamination in rural Mekong Basin, Ubon Ratchathani. Thus, it is probably useful for arsenic standard level assignment and public health authorities. Moreover, it also leads to establish research activity in treatment of arsenic-contaminated groundwater for different purposes展开更多
American Indians are a substantial minority in both the United States and Canada and present with a disproportionate share of mental health and behavioral health problems. While a large proportion of the native popula...American Indians are a substantial minority in both the United States and Canada and present with a disproportionate share of mental health and behavioral health problems. While a large proportion of the native population resides on reservations that are self-managed and have few non-Indian residents, professional health services are mostly provided by clinicians from the dominant culture. The essay tries to highlight specific historical, sociological, and cultural variables the clinician must be aware of to work effectively in this setting. Particular emphasis is placed on using a flexible, eclectic approach, and a case vignette is included to illustrate the principle.展开更多
文摘A simple, rapid and sensitive flow injection chemiluminescence (FI-CL) method has been developed for the determination of meloxicam. The method is based on the CL-emitting reaction between meloxicam and potassium permanganate in a hydrochloric acid medium, enhanced by formaldehyde (HCHO). Under optimum conditions, calibration curve over the range of 1.0-20.0μg/mL was obtained. The proposed method was successfully applied to the determination of meloxicam in capsules with no evi- dence of interference from common excipients. The detection limit of this method was 25.6 ng/mL. The relative standard deviation was 2.1% for 10.0 μg/mL meloxicam. The sample throughput was found to be 120 samples/h.
文摘Arsenic (As) is one of the most important elemental pollutants in groundwater and drinking water because it causes health problem of arsenicosis after consumption of drinking arsenic-rich water more than 5-10 years. Arsenic contamination of groundwater is an emerging issue in Mekong Basin including Cambodia, Vietnam, and Thailand. In Thailand, information about arsenic contamination in drinking water resources are quite rare due to that arsenic is not the main element in water qualification assay. The objective of this study is to determine groundwater quality and arsenic contamination in rural Mekong Basin, Ubon Ratchathani. Groundwater samples were collected from 20 different sampling points, between August 2009 and February 2010 in Amphoe Khemmarat, Ubon Ratchathani, Thailand. Physical and chemical characteristics of groundwater were determined. It was observed that the groundwater was 27.9-30.3 ~C, pH 5.7-6.9. The conductivity was 707-767 p.S.cm". Dissolved oxygen was 2.04-5.12 mg.L-1 and TDS was 352-384 mg.L~. The samples showed soft- to very hardness-water properties. In some area, few parameters like CI, Fe, Mn, and As exceeded the WHO guideline limits. This result represents basic information for quality of groundwater and the arsenic contamination in rural Mekong Basin, Ubon Ratchathani. Thus, it is probably useful for arsenic standard level assignment and public health authorities. Moreover, it also leads to establish research activity in treatment of arsenic-contaminated groundwater for different purposes
文摘American Indians are a substantial minority in both the United States and Canada and present with a disproportionate share of mental health and behavioral health problems. While a large proportion of the native population resides on reservations that are self-managed and have few non-Indian residents, professional health services are mostly provided by clinicians from the dominant culture. The essay tries to highlight specific historical, sociological, and cultural variables the clinician must be aware of to work effectively in this setting. Particular emphasis is placed on using a flexible, eclectic approach, and a case vignette is included to illustrate the principle.