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能谱CT曲线斜率及碘浓度定量分析鉴别良恶性甲状腺结节的准确率观察 被引量:11
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作者 颜利辉 姚立正 +2 位作者 李新 王澍 陈飞 《医学影像学杂志》 2016年第10期1795-1798,共4页
目的探讨能谱CT曲线斜率及碘浓度定量分析在良恶性甲状腺结节鉴别诊断中的应用价值。方法选取48例经超声筛查的甲状腺结节患者为研究对象,以病理检查结果为依据,分别纳入恶性组(n=21)和良性组(n=27);将同期入院行颈部检查的20例无甲状... 目的探讨能谱CT曲线斜率及碘浓度定量分析在良恶性甲状腺结节鉴别诊断中的应用价值。方法选取48例经超声筛查的甲状腺结节患者为研究对象,以病理检查结果为依据,分别纳入恶性组(n=21)和良性组(n=27);将同期入院行颈部检查的20例无甲状腺结节正常受试者纳入正常组(n=20)。两组受试者均使用能谱CT行能谱CT成像(GSI)单能模式平扫及增强扫描,后应用GSI Viewer软件计算碘浓度和能谱曲线斜率。记录并对比三组受试者计算结果差异;以病理检查结果为依据分析能谱CT检查对良恶性甲状腺结节的鉴别准确性。结果能谱CT正确诊断良性结节26例,正确诊断恶性结节19例,对良恶性甲状腺结节的鉴别诊断准确率为93.8%(45/48)。恶性组不同期相能谱曲线斜率及动脉期、静脉期碘浓度值检测结果均显著低于其他两组受试者(P<0.05);平扫期内,良、恶性两组碘浓度值均显著低于正常组(P<0.05),但两组对比无统计学意义(P>0.05)。结论能谱CT在甲状腺结节的良恶性鉴别诊断中具有较高的准确率,临床可将其作为切实可行的影像学检查手段应用于诊疗工作中,为后续治疗方案的拟定提供条件。 展开更多
关键词 曲线斜率 浓度定量分析 甲状腺结节 良恶性鉴别诊断 体层摄影术 X线计算机
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正丁基锂的直接碳谱测试与简易浓度定量探讨 被引量:1
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作者 林崇熙 杨波 《分析化学》 SCIE EI CAS CSCD 北大核心 2002年第10期1279-1279,共1页
关键词 正丁基锂 直接碳谱测试 浓度定量 核磁共振碳谱
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基于气体浓度定量的嗅觉刺激器优化设计 被引量:1
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作者 孙韦 王慧 +2 位作者 张寅 常严 杨晓冬 《波谱学杂志》 CAS 北大核心 2021年第1期12-21,共10页
现有的基于磁共振测量的嗅觉刺激器,通过调节嗅剂液体浓度的方法可以实现不同浓度的嗅觉刺激,但随着实验进行,受到嗅剂挥发以及实验环境(温度、湿度、气流量)变化的影响,很难确保输送至鼻腔的嗅剂气体浓度的稳定性,进而影响实验结果的... 现有的基于磁共振测量的嗅觉刺激器,通过调节嗅剂液体浓度的方法可以实现不同浓度的嗅觉刺激,但随着实验进行,受到嗅剂挥发以及实验环境(温度、湿度、气流量)变化的影响,很难确保输送至鼻腔的嗅剂气体浓度的稳定性,进而影响实验结果的准确性.本研究对本实验室前期开发的嗅觉刺激装置进行改进,实现了气体浓度精确定量.改进后的嗅觉刺激器主要分为三个部分:控制系统、反馈系统和气路系统.控制系统主要实现气路系统的送气控制和嗅剂气体浓度调节;反馈系统则负责对气体浓度进行测量;气路系统则在原有基础上添加活性炭装置,降低无关因素干扰.装置改进之后,不同气路切换时间为75.2 ms,比原装置减少了1 s,有效提高刺激精度.实验结果显示,气体浓度调节前,300 s内乙醇、吡啶、乙酸戊酯嗅剂气体浓度分别下降6.7%、71.4%、79.2%,嗅剂气体浓度短时间内发生较大改变.加入气体浓度调节功能后,当气体浓度下降至目标浓度的90%时,可通过调节气泵电压改变嗅剂气流与空气气流比例,从而调节嗅剂气体浓度至目标值,其中吡啶、乙酸戊酯用时13 s. 展开更多
关键词 嗅觉刺激器 气体浓度定量 反馈调节 光离子化气体传感器(PID)
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从浓度定量分析探讨异丙醇作原油萃取剂的可行性 被引量:3
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作者 栾晓宁 王春艳 +2 位作者 李颖 辛美丽 郑荣儿 《海洋湖沼通报》 CSCD 北大核心 2009年第2期151-156,共6页
分别采用正己烷与异丙醇作为萃取剂获得不同浓度下的2组相同原油样品的萃取液,进行波长差为40nm的同步荧光光谱测量。通过插值拟合得到相应的两组相同原油样品的浓度三维荧光光谱图,并据此对相同原油样品萃取液的未知浓度进行计算,并与... 分别采用正己烷与异丙醇作为萃取剂获得不同浓度下的2组相同原油样品的萃取液,进行波长差为40nm的同步荧光光谱测量。通过插值拟合得到相应的两组相同原油样品的浓度三维荧光光谱图,并据此对相同原油样品萃取液的未知浓度进行计算,并与实际值比较,得出相应误差。文中通过对不同萃取剂中光谱谱形、峰位、荧光强度以及浓度计算的误差进行对比分析,得出采用异丙醇作为石油定量荧光分析仪的萃取剂比用正己烷更具优势,从而在定量分析的基础上论证了采用异丙醇取代正己烷作为原油萃取剂的可行性。 展开更多
关键词 正己烷 异丙醇 浓度荧光定量分析
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柴油喷雾撞壁特性的定量研究 被引量:5
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作者 毛立伟 苏万华 裴毅强 《燃烧科学与技术》 EI CAS CSCD 北大核心 2015年第6期521-529,共9页
在一个定容弹里,利用复合激光诱导荧光(PLIEF)技术定量研究了柴油喷雾撞击平板后的燃油分布.研究发现,在气、液相喷雾同时撞壁的条件下气相喷雾瞬态最大当量比出现在撞壁点附近,瞬态最低温度出现在瞬态最大当量比位置并与其发展规律截... 在一个定容弹里,利用复合激光诱导荧光(PLIEF)技术定量研究了柴油喷雾撞击平板后的燃油分布.研究发现,在气、液相喷雾同时撞壁的条件下气相喷雾瞬态最大当量比出现在撞壁点附近,瞬态最低温度出现在瞬态最大当量比位置并与其发展规律截然相反.撞壁后气相壁面贯穿距离和壁面高度随时间发展逐渐增加,液相壁面贯穿距离和高度先随着时间增加而增大,到某一时刻后保持基本不变.气、液相壁面贯穿距离和壁面高度受各种参数的影响很大.根据实验数据,利用多元非线性回归法,拟合了可以较好预测气、液相壁面贯穿距离和壁面高度的经验公式. 展开更多
关键词 柴油喷雾 撞壁特性 喷雾浓度和温度定量标定 壁面贯穿距离和壁面高度 复合激光诱导荧光
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CS_(2)燃烧火焰光谱辐射模型的构建与特征污染产物浓度反演研究 被引量:1
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作者 彭吴迪 宁甲练 +3 位作者 陈志莉 唐瑾 刘礼喜 陈林 《光谱学与光谱分析》 SCIE EI CAS CSCD 北大核心 2022年第3期672-677,共6页
CS_(2)在当今化工等领域占据了重要地位,而CS_(2)火灾污染事故危害性极大。通过研究CS_(2)燃烧火焰光谱辐射以探究其火灾污染特性极为必要。搭建了CS_(2)燃烧火焰光谱测试平台,采用黑体辐射源对VSR仪器进行了标定,通过多用途傅里叶变换(... CS_(2)在当今化工等领域占据了重要地位,而CS_(2)火灾污染事故危害性极大。通过研究CS_(2)燃烧火焰光谱辐射以探究其火灾污染特性极为必要。搭建了CS_(2)燃烧火焰光谱测试平台,采用黑体辐射源对VSR仪器进行了标定,通过多用途傅里叶变换(VSR)红外光谱辐射仪测试了5,10和20 cm三种燃烧尺度下CS_(2)燃烧的火焰光谱,并通过热电偶测试了整个燃烧时间段内不同燃烧时刻下的火焰温度,以及在火焰上方安装了烟气分析仪对火焰中的燃烧产物浓度进行监测。测量了CS_(2)整个燃烧时间段内火焰温度,以及不同燃烧时间、不同燃烧尺度下的火焰光谱、燃烧产物组分信息。测试结果表明,CS_(2)火焰中主要含有高温SO_(2),CO_(2),CO气体和空气中卷入的H_(2)O分子,并获取了特征污染产物SO_(2)的浓度。由于现有光谱仪测量分辨率有限,室内实验测量的火焰尺度有限,为了能实现火灾在线监测需要建立一个火焰光谱辐射模型来反演CS_(2)火灾时的污染物浓度相关信息。基于HITRAN数据库可知在2.7μm附近为高温水蒸气的发射峰,4.2μm附近特征峰为高温CO_(2)气体的发射峰,4.7μm附近有CO微弱的发射峰,在7.4μm附近特征峰为高温SO_(2)气体的发射峰,并获得了CS_(2)燃烧时产生的SO_(2),CO_(2),CO和H_(2)O气体在火焰燃烧相同温度下的吸收系数,通过计算得到了CS_(2)燃烧时产生的SO_(2),CO_(2),CO和H_(2)O混合气体的透过率与发射率,并结合气体辐射传输方程、气体吸收系数等方程,创建了CS_(2)燃烧的火焰光谱辐射模型。利用该光谱辐射模型反演了不同燃烧时间下特征污染产物SO_(2)的浓度,并与实验测得的数据进行了对比分析。结果表明,该模型精度高,可用于燃烧产物浓度的定量化反演,SO_(2)分子含量在燃烧时间20,40,60和80 s时的反演精度分别是89.5%,82.5%,85.6%和86.5%。为遥感反演CS_(2)型大尺度火灾中燃烧产物的浓度奠定基础。 展开更多
关键词 二硫化碳 火焰光谱 光谱辐射模型 气体浓度定量反演
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湛江港海域叶绿素a浓度的高光谱遥感反演 被引量:4
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作者 蒋城飞 廖珊 +5 位作者 付东洋 王文芳 李薛 刘大召 张莹 黄雄杰 《广东海洋大学学报》 CAS 2016年第6期107-113,共7页
基于表观光学法研究冬季湛江港海域高光谱遥感叶绿素a浓度的反演模型构建,结果表明,该海域单波段遥感反射率与叶绿素a浓度相关性低,波段比值和遥感反射率的一阶微分法可提高叶绿素a浓度反演精度。665nm处的遥感反射率一阶微分值与叶绿素... 基于表观光学法研究冬季湛江港海域高光谱遥感叶绿素a浓度的反演模型构建,结果表明,该海域单波段遥感反射率与叶绿素a浓度相关性低,波段比值和遥感反射率的一阶微分法可提高叶绿素a浓度反演精度。665nm处的遥感反射率一阶微分值与叶绿素a浓度相关性良好,相关系数可达0.84。一阶微分相关系数大于0.8的波段大部分处于叶绿素a红光强烈吸收区域,对于富营养化的湛江港海域采用一阶微分方法构建叶绿素a浓度的遥感反演模型具有合理性。 展开更多
关键词 湛江港海域 叶绿素a浓度 高光谱遥感 定量反演
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两种不同材料角膜接触镜的蛋白质沉淀分析 被引量:3
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作者 李长兵 孙复钱 栾洁 《实用临床医药杂志》 CAS 2009年第4期108-109,共2页
关键词 角膜接触镜 蛋白质沉淀 BCA蛋白质浓度定量 甲基丙烯酸-β-羟乙酯(HEMA) 硅水凝胶
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Comparisons of Nectar Quantity and Sugar Concentration of Pomegranate Blossom in a Day 被引量:1
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作者 余玉生 卢焕仙 +2 位作者 宋文菲 张祖芸 张学文 《Agricultural Science & Technology》 CAS 2013年第1期69-71,共3页
[Objective] The aim was to research the rules of nectar quantity and sugar concentration of perfect and staminate flowers in a day. [Method] Based on nine Tianguang Yan pomegranate trees, nectar quantity and sugar con... [Objective] The aim was to research the rules of nectar quantity and sugar concentration of perfect and staminate flowers in a day. [Method] Based on nine Tianguang Yan pomegranate trees, nectar quantity and sugar concentration of per- fect and staminate flowers were measured and analyzed in morning and afternoon. [Result] Average nectar quantity and sugar concentration differed insignificantly in morning and afternoon of perfect flowers, which could also be applied to staminate flowers. However, average nectar quantity of perfect flower was 64.09 μI and of staminate flower was 44.07 μl. It is obvious that the two were of extremely signifi- cant differences (t=4.642, P〈0.01), and the former was significantly higher by 45,43%. On the other hand, average sugar concentration of perfect flower was 48.44% and of staminate flower was 37.16%. The two were of extremely significant differences and the former is higher by 30.36%, compared with the latter. These suggested that nectar quantity and sugar concentration would maintain unchanged in different periods for a day, if nectars are not consumed by pollinators, such as bees and butterflies. In the same period, nectar quantity and sugar concentration of per- fect flowers were higher than those of staminate flowers. [Conclusion] The research provides references for benefits increase of bee farmers and fruit farmers, as well as exploration of bee pollination. 展开更多
关键词 Quantity of secreted nectar Sugar concentration MEASUREMENT Com- parisons
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智能车载安全检测系统的研究
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作者 尹世超 许浩 《数码设计》 2021年第2期58-59,共2页
酒驾及车内儿童窒息问题是社会关注的焦点,针对这一热点问题,本文设计了一种基于GPS/GSM的智能车载安全监测系统。该系统自制酒精检测模块,通过算法,定量算出酒精浓度。然后利用GPS/GSM技术,将车辆定位信息、车主信息传输到家人的手机... 酒驾及车内儿童窒息问题是社会关注的焦点,针对这一热点问题,本文设计了一种基于GPS/GSM的智能车载安全监测系统。该系统自制酒精检测模块,通过算法,定量算出酒精浓度。然后利用GPS/GSM技术,将车辆定位信息、车主信息传输到家人的手机上。当出现异常情况时,蜂鸣器发出警报,同时向家人发送短信,通过open/close控制天窗开关实现救援。 展开更多
关键词 酒后驾驶 酒精浓度定量检测 GPS/GSM 智能车载
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巧借抽水马桶虹吸管吸力的一项发明
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作者 王建华 《今日科技》 1997年第3期24-24,共1页
关键词 药液浓度定量控制系统 抽水马桶 虹吸管 吸力
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探讨分析化学中几项分析性能指标 被引量:3
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作者 刘栋 李妍 《广州化工》 CAS 2019年第8期137-138,172,共3页
在分析化学中,检出限(DL)、定量下限(QL)和最低定量浓度是判定分析方法的重要性能指标。阐述了各项性能指标的概念和确定方法,及其在职业卫生检测中的应用。在实际职业卫生检测过程中,检测结果报告应当以定量指标表征,使得检测报告更加... 在分析化学中,检出限(DL)、定量下限(QL)和最低定量浓度是判定分析方法的重要性能指标。阐述了各项性能指标的概念和确定方法,及其在职业卫生检测中的应用。在实际职业卫生检测过程中,检测结果报告应当以定量指标表征,使得检测报告更加合理和科学。初步讨论了检出限、定量下限和最低定量浓度之间的关系与区别,对实际检测工作具有一定的指导意义。 展开更多
关键词 检出限 定量下限 最低定量浓度 职业卫生检测
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Development of a concentration method for detection of tobacco mosaic virus in irrigation water 被引量:1
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作者 Wei Chen Wenting Liu +3 位作者 Honghong Jiao Huawei Zhang Julong Cheng Yunfeng Wu 《Virologica Sinica》 SCIE CAS CSCD 2014年第3期155-161,共7页
Tobacco mosaic virus(TMV) causes significant yield loss in susceptible crops irrigated with contaminated water. However, detection of TMV in water is difficult owing to extremely low concentrations of the virus. Here,... Tobacco mosaic virus(TMV) causes significant yield loss in susceptible crops irrigated with contaminated water. However, detection of TMV in water is difficult owing to extremely low concentrations of the virus. Here, we developed a simple method for the detection and quantification of TMV in irrigation water. TMV was reliably detected at concentrations as low as 10 viral copies/μL with real-time PCR. The sensitivity of detection was further improved using polyethylene glycol 6000(PEG6000, MW 6000) to concentrate TMV from water samples. Among the 28 samples from Shaanxi Province examined with our method, 17 were tested positive after virus concentration. Infectivity of TMV in the original water sample as well as after concentration was confirmed using PCR. The limiting concentration of TMV in water to re-infect plants was determined as 102 viral copies/mL. The method developed in this study offers a novel approach to detect TMV in irrigation water, and may provide an effective tool to control crop infection. 展开更多
关键词 tobacco mosaic virus polyethylene glycol real-time PCR irrigation water
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Approach to increasing the quality of pressure-relieved gas drained from protected coal seam using surface borehole and its industrial application 被引量:14
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作者 Yingke Liu Fubao Zhou +1 位作者 Jianlong Wang Jun Liu 《International Journal of Coal Science & Technology》 EI 2015年第1期46-51,共6页
During mining of lower protective coal seam, a surface borehole can efficiently extract not only the pressure-relieved gas from the protected layer, but also the gas from the mining layer gob. If the distance between ... During mining of lower protective coal seam, a surface borehole can efficiently extract not only the pressure-relieved gas from the protected layer, but also the gas from the mining layer gob. If the distance between the borehole and gob is too large, the quantity of gas drained from the protected layer decreases substantially. To solve this problem, a mathematical model for extracting pressure-relieved gas from a protected coal seam using a surface borehole was established, based on the radial gas flow theory and law of conservation of energy. The key factors influencing the quantity of gas and the drainage flow network using a surface borehole were presented. The results show that the quantity of pressure-relieved gas drained from the protected layer can be significantly increased by increasing the flow resistance of the borehole bottom. Application of this method in the Wulan Coal Mine of the Shenhua Group significantly increased the flow of pure gas and the gas concentration (by factors of 1.8 and 2.0, respectively), thus demonstrating the remarkable effects of this method. 展开更多
关键词 Surface borehole Gas drainage Borehole bottom resistance Pressure-relieved gas
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Isolation of Uranium by Anionic Exchange Resins
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作者 Fablola Monroy-Guzman 《Journal of Chemistry and Chemical Engineering》 2016年第2期90-95,共6页
A separation methodology to isolate natural uranium from its radioactive daughters: Th, Ra, Bi, Pb, Pa and Po, was developed using an only one anion exchange resin and varying concentrations of HC1 solutions. Three t... A separation methodology to isolate natural uranium from its radioactive daughters: Th, Ra, Bi, Pb, Pa and Po, was developed using an only one anion exchange resin and varying concentrations of HC1 solutions. Three types of anion exchange resins were tested and the separation process was followed by gamma and alpha spectrometry. Uranium can be quantitatively isolated from its descendants using Dowex IX8 (20-50 mesh) or Amerlite IRA (100 mesh) resins in three steps: using 4 and 8 mol/L-1 HCI and water to recover uranium. The method is easy, quick, and inexpensive. 展开更多
关键词 Anion exchange resin URANIUM separation.
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Development Trends and Evaluation of Egbe Reservoir Water Nutrient Status in Ekiti State, Nigeria
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作者 Josephine Bolaji Edward Adiaha Aldah Alex Ugwumba 《Journal of Life Sciences》 2010年第1期7-16,共10页
A study about some physicochemical parameters of Egbe reservoir was carried out from September 2005 to December 2006. The parameters include mean temperature, pH, conductivity, alkalinity, TSS, TDS, DO and BOD which h... A study about some physicochemical parameters of Egbe reservoir was carried out from September 2005 to December 2006. The parameters include mean temperature, pH, conductivity, alkalinity, TSS, TDS, DO and BOD which have values of 28.7±0.9 ℃ ; 8.3±0.3; 831±172.5 μS/cm; 165.4±18.3 mg/L; 0.06±0.1 mg/L; 0.4±0.6 mg/L; 7.8±2.4 mg/L and 5.2±1.6mg/L, respectively. Temperature and pH were measured in the field using mercury-in-glass thermometer calibrated in degrees Celsius and pH meter, respectively. TSS and TDS were measured by grayimetric methods, while alkalinity was measured titrimetrically and DO and BOD were measured by Winkler's method. For the nutrients, nitrate was measured color±metrically, phosphate by Stannous Chloride method and sulphate by turbidimetric method. Mean concentration of nitrate, phosphate, and sulphate were 15.6±8.6 rag/L; 42.5±19.4 mg/L and 72.3±14.7 mg/L respectively. Nowadays, eutrophication of natural waters is one of the most significant causes of deterioration of water quality, and nitrates and phosphates are probably the key nutrients in controlling the growth of aquatic plants. Though the mean concentration of nitrates and phosphates in the reservoir water were within the acceptable limit, yet their concentrations in some locations of reservoir were high enough to encourage the growth of aquatic macrophytes which would increase productivities. Hence, it is necessary to check their further increase, and periodic monitoring and preventive measures must be adopted to save the reservoir from eutrophication. 展开更多
关键词 Physico-chemical parameters development trends NUTRIENTS Egbe reservoir.
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