铸钢用锆砂涂模剂中放射性测试与分析

对大连铸造行业所用锆砂放射性进行调查 ,测试 ,分析说明 :不同产地的锆砂放射性比活度不同 ;不同工作部位 ,不同的工艺操作所受照射剂量不同。指出锆砂不同于普通铸造用砂 ,因其含有放射性而应引起注意 。

氯化聚丙烯与醇酸树脂共混物的红外光谱测定

利用FTIR红外光谱法对氯化聚丙烯与短油度醇酸树脂共混物的相容性进行了研究 ,并用涂膜光泽度进行对比。结果表明 ,在氯化聚丙烯与醇酸树脂共混物的谱图中 ,羟基谱带发生了明显的位移。且当短油醇酸树脂的固含量x小于 0 5时 ,两种树脂基本上是相容的 ;x大于 0 5时 ,共混物是不相容的。

微机拉深模CAD系统研究

本文介绍了作者自行开发的拉深模CAD系统的组成和功能。该系统以设计人员为中心，采用人机交互式设计环境，整个系统采用菜单统一管理，并配以大量的图象及文字提示。系统运行时，只要输入零件尺寸数据就可根据菜单选项和人机对话完成整个设计过程，最后输出工序图、模具零件图和总装图。

Application of ultra-smooth composite diamond film coated WC-Co drawing dies under water-lubricating conditions

A specific revised HFCVD apparatus and a novel process combining HFCVD and polishing technique were presented to deposit the micro-and nano-crystalline multilayered ultra-smooth diamond（USCD） film on the interior-hole surface of WC-Co drawing dies with aperture ranging from d1.0 mm to 60 mm.Characterization results indicate that the surface roughness values（Ra） in the entry zone,drawing zone and bearing zone of as-fabricated USCD coated drawing die were measured as low as 25.7,23.3 and 25.5 nm,respectively.Furthermore,the friction properties of USCD films were examined in both dry sliding and water-lubricating conditions,and the results show that the USCD film presents much superior friction properties.Its friction coefficients against ball-bearing steel,copper and silicon nitride balls（d4 mm）,is always lower than that of microcrystalline diamond（MCD） or WC-Co sample,regardless of the lubricating condition.Meanwhile,it still presents competitive wear resistance with the MCD films.Finally,the working lifetime and performance of as-fabricated USCD coated drawing dies were examined under producing low-carbon steel pipes in dry-sliding and water-lubricating conditions.Under the water-lubricating drawing condition,its production significantly increases by about 20 times compared with the conventional WC-Co drawing dies.

混凝土界面剂的开发与应用

随着我国经济建设的蓬勃发展,工程建筑量也极其庞大,然而混凝土搭接面的界面处理,绝大部分为简单、粗放的二次凿毛工艺,既耗时、耗力,又无法保证界面的处理质量。笔者为此做了大量试验,开发出一种新型界面处理剂,并在工程中推广应用,获得了比较成功的效果。

Formation characteristic of Ca-P coatings on magnesium alloy surface

A chemical method was used to deposit dicalcium phosphate dehydrate coatings on AZ91 magnesium alloy. The aim was to improve the biodegradation behavior of magnesium alloy in a simulated body fluid. The microstructures of the coating before and after immersion in the simulated body fluid were characterized by scanning electron microscopy （SEM） and X-ray diffraction （XRD） The results indicated that the dicalcium phosphate dehydrate coatings exhibited two morphologies during the pre-calcification process. The titration speed of the pre-calcification process had great influence on the morphologies of the pre-calcification coatings. As the soaking time increased, the diffraction peaks of dicalcium phosphate dehydrate disappeared and hydroxyapatite precipitated on the coated substrate surfaces. This indicates the dissolution of dicalcium phosphate dehydrate during the immersion process. The structures of the dicalcium phosphate dehydrate coatings and the formation mechanisms of the hydroxyapatite coatings were investigated in detail.

Hydroxyapatite Coatings on Titanium Prepared by Electrodeposition in a Modified Simulated Body Fluid

Hydroxyapatite coatings were directly prepared on anodized titanium by electro-deposition method in a modified simulated body fluid.The configuration,structure and bioactivity of the coating were investigated with scanning electron microscopy(SEM),X-ray diffraction analyzer(XRD)and Fourier transform infrared spectros-copy(FTIR)techniques.The results demonstrated that pure and homogeneous hydroxyapatite coating can be obtained without any post-treatment.The prepared coating showed good bioactivity in simulated body fluid(SBF).The time required for a fully covered dense hydroxyapatite coatings was 4 days immersion in SBF.

Bonding strength in carbon steel sandwich panels under condition of diffusion-rolling with small reduction

One of the key problems by diffusion-rolling bonding with small reduction for carbon steel plates is the bonding assistant coat. Abonding assitant coat used below 850℃ was developed. It contained copper as basic element and zinc as main alloy element. Other small elements and rear metals were added to decrease the melting point and to obtain a better clouding and bigh plasticity. Based on the theory of brazing and transient liquid diffusion welding, two carbon steel plates were rolled with small reduction by using self-made bonding assistant coat. Temperature, pressure and holding time are the main technology parameters for controlling the process of diffusion-rolling. The results show that the bonding strength is the greatest when the bonding temperature is 830℃, holding time is 3 min and the reduction rate is 9%.

Effects of thickness and elastic modulus on stress condition of fatigue-resistant coating under rolling contact

The distribution and magnitude of surface substrates were investigated by finite element method and subsurface stresses of the （FEM）. The models of coating single-layer sprayed-coatings on monolithic configurations with different thicknesses and elastic modulus ratios of coating to substrate were introduced, and the effects of thickness and elastic modulus ratio on the stresses were addressed. The calculation results show that the coating/substrate interface shear stress obviously decreases with increasing coating thickness, due to the location of the maximum shear stress moving away from the coating/substrate interface. At the same time, the magnitude of von Mises stress also declines in the case of thicker coatings. However, the high elastic modulus ratio results in extremely high maximum shear stress and the severe discontinuity of the von Mises stress curves, which leads to the intensive stress concentration on the coating/substrate interface. So the coating configurations with the larger coating thickness and lower difference of elastic modulus between coating and substrate exhibit excellent resistant performance of rolling contact fatigue （RCF）.

Effect of pattern coating thickness on characteristics of lost foam Al-Si-Cu alloy casting

An experimental study on lost foam casting of an Al-Si-Cu alloy was conducted. The main objective was to study the effect of pattern coating thickness on casting imperfection and porosity percentage as well as eutectic silicon spacing of the alloy. The results showed that increasing slurry viscosity and flask dipping time influenced the casting integrity and microstructural characteristics. It was found that thinner pattern coating produced improved mould filling, refined microstructure and higher quality castings containing less porosity.

Effect of coating material and lubricant on forming force and surface defects in wire drawing process

A pilot wire drawing machine as well as wire end-pointing roller was developed. Using these machines, a wire drawing test for four different coating materials and two different lubricants was performed as the reduction ratio increased from 10% to 30%. Materials used for a substrate in this study are plain carbon steel （AIS11045） and ultra low carbon bainite steel. To compute the friction coefficient between the coating layer of wire and the surface of die lbr a specific lubricant, a series of finite element analyses were carried out. SEM observations were also conducted to investigate the surface defects of wire deformed. Results show that the behavior of drawing force varies with the lubricant-type at the initial stage of drawing. The powder-typed lubricant with a large particle causes the retardation of lull lubrication on the entire contact surface and the local delamination of coating layer on the wire surface. As the flow stress of a substrate increases, the delamination becomes severe.

Effects of process parameters on microstructure and wear resistance of TiN coatings deposited on TC11 titanium alloy by electrospark deposition

In the present study,the effects of process parameters(output voltage x,nitrogen flux l and specific strengthening time s)on the microstructure and wear resistance properties of TiN coatings prepared by electrospark deposition(ESD)were investigatedsystematically.The microstructure of the coatings was characterized for thickness(TOC),content of TiN(CON)and porosity(POC).A statistical model was developed to identify the significant factors affecting the microstructure and wear resistance of the coatings.The results show that the output voltage x and nitrogen flux l present significant effects on majority of the evaluation indexes such asTOC,friction coefficient(COF)and wear mass loss(Id),while the specific strengthening time s has a significant effect on POC and asmall effect on the other indexes.The optimal process parameters were obtained as follows:output voltage(x,60V),nitrogen flux(l,15L/min)and specific strengthening time(s,3min/cm2).The variation of wear mass loss(Id)by the variation of the outputvoltage(x)and nitrogen flux(l)is attributed to the change of wear mechanisms of TiN coatings.The main wear mechanism of TiNcoating prepared under optimal process parameters is micro-cutting wear accompanied by micro-fracture wear.

Analysis of Forging Dies Coated with Tungsten Carbide through HVOF Processing

In this paper we present a performance evaluation of thermal spraying coated hot forging dies conducted in a production line. The High Velocity Oxy-Fuel process was used for the deposition of a tungsten carbide coating, which is characterized by its optimal adherence and low porosity. A metallurgical characterization of the layer was previously done, in order to obtain reference information to assist in the interpretation of the practical tests results. The coated die allowed an increase in productivity of 37.5%, besides better dimensional stability results through the process and legibility of printed numbers.

Structural behaviors of steel roof truss exposed to pool fire

Experimental research was conducted to study the structural behaviors of a steel roof truss model without fire-proof coating under pool fire conditions. The data of temperature distribution and displacements of typical members were obtained. It is found that the temperature distribution of environment inside the structure, which is found to be in accordance with the multi-zone model with height, has a decisive effect on the tempera^tre evolution of steel members. Besides, it can also be observed that due to the restriction and coordination among the truss members in the localized fire, the maximum relative deflection, which occurs at the mid-span of the top chord, is relatively slight and has not exceeded 1 mm under experimental conditions. On the other hand, the column experiences a notable thermal expansion during the test. Then, a finite element model is presented and validated by the test results.

Calcium phosphate deposition on surface of porous and dense TiNi alloys in simulated body fluid

Porous and dense TiNi alloys were successfully fabricated by powder metallurgy(P/M) method, and to further improve their surface biocompatibility, surface modification techniques including grind using silicon-carbide(SiC) paper, acid etching and alkali treatment were employed to produce either irregularly rough surface or micro-porous surface roughness. X-ray diffractometry(XRD), scanning electron microscopy(SEM) and energy dispersive X-ray spectroscopy(EDX) attached to SEM were used to characterize surface structure and the Ca-P coatings. Effects of the above surface treatments on the surface morphology, apatite forming ability were systematically investigated. Results indicate that all the above surface treatments increase the apatite forming ability of TiNi alloys in varying degrees when soaked in simulated body fluid(SBF). More apatite coatings formed on TiNi samples sintered at 1050℃ and 1100℃ due to their high porosity and pure TiNi phase that is beneficial to heterogeneous nucleation. Furthermore, more uniform apatite was fabricated on the sample sintered from the mixture of Ni and Ti powders.

Modeling and of Diatom Mud in Residential Space and the Application Scenario Research

Our original ecological diatom mud qualities as a starting point for research, analyzes people’s consumption concept, aesthetics, environmental protection awareness. This article describes the basics and the origin of diatom mud, diatom mud analyzes the features, functions and defects, the diatom mud paint and wallpaper were compared to explain the process and the market situation diatom mud, silicon Prospects algae mud were discussed. Through analysis of this environmentally friendly decorative paint diatom mud, summed diatom mud there are some problems in the conventional construction; through research and exploration of the diatom mud module series is proposed in the form of modules forming diatom mud can serialization assembly decorative product design concept.

Investigations of Spray Painting Processes Using an Airless Spray Gun

This paper presents experimental and numerical studies on spray painting processes by using airless spray guns for ship painting. A computational fluid dynamics code was applied to calculate the flow field and the droplet trajectories. Droplet size distributions and droplet velocities as necessary inlet characteristics for the simulations were experimentally obtained using a Spraytec Fraunhofer type particle sizer and laser-Doppler anemometry. Effects of shoreline winds and painting distance on the transfer efficiency and on the paint film thickness distributions on the target were numerically studied.

Wear Behavior of Diamond-Coated Drawing Dies

The failure behavior of diamond-coated die was investigated experimentally and analytically through finite element method (FEM) simulation in the present work. Diamond coatings were fabricated by straight hot filament chemical vapor deposition (CVD) passing through the interior hole of the drawing die using a mixture of hydrogen and acetone as source gases. The performance tests were made under real drawing condition. Scanning electron microscopy (SEM) was used for the study of coating wear after die service. The coating wear appears on two regions of the reduction zone: one is near the entrance where the contact begins, and the other is at the end of the reduction zone. FEM simulation was made for calculating the von Mises stresses distribution on the coating and substrate during the drawing process. The present work was of great practical significance for the improvement of drawing performance of diamond-coated drawing dies.