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利用液滴实验探究几个典型沉淀反应 被引量:2
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作者 曾涛 廖连燕 +1 位作者 杨兴 张瑞 《化学教学》 CAS 北大核心 2018年第7期75-78,共4页
利用微量化液滴实验方法,对BaSO4、CaCO3、A1(OH)3、Zn(OH)2、Fe(OH),典型沉淀反应进行探索和条件优化,对沉淀在浊态和干态下的电子显微镜成像表征进行对比考察,达到r耗试剂微量、操作简单、实验仪器经济、实验现象明显、实... 利用微量化液滴实验方法,对BaSO4、CaCO3、A1(OH)3、Zn(OH)2、Fe(OH),典型沉淀反应进行探索和条件优化,对沉淀在浊态和干态下的电子显微镜成像表征进行对比考察,达到r耗试剂微量、操作简单、实验仪器经济、实验现象明显、实验结果生动有趣等效果,弥补了常规实验用量大,观察不到反应过程等缺陷,实现了对传统沉淀实验方法的优化和补充。 展开更多
关键词 液滴实验 微量化实验 沉淀反应 玻璃片 电子显微镜成像
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空间液滴蒸发实验中液滴图像的无损压缩算法 被引量:1
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作者 周晓波 于强 蔡世界 《空间科学学报》 CAS CSCD 北大核心 2010年第3期283-288,共6页
为了提高空间液滴蒸发实验中图像无损压缩率,根据连续采集到的液滴图像之间相关性很大的特点,提出了一种基于JPEG-LS和帧间预测误差编码的图像序列无损压缩算法.该算法对图像序列第一帧采用JPEG-LS算法编码,对帧间预测误差帧进行Golomb... 为了提高空间液滴蒸发实验中图像无损压缩率,根据连续采集到的液滴图像之间相关性很大的特点,提出了一种基于JPEG-LS和帧间预测误差编码的图像序列无损压缩算法.该算法对图像序列第一帧采用JPEG-LS算法编码,对帧间预测误差帧进行Golomb编码,从而实现对连续采集到的液滴图像序列进行无损压缩.实验结果表明,该算法比单纯采用JPEG-LS算法的压缩率有明显提高,编解码过程更简单,编码需要时间更少. 展开更多
关键词 空间蒸发实验 无损压缩 JPEG-LS Golomb编码 帧间预测
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几种液体燃料指数蒸发率模型的实验研究
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作者 王方 姜文彬 +2 位作者 罗虎 张学智 金捷 《推进技术》 EI CAS CSCD 北大核心 2016年第11期2080-2087,共8页
燃烧室设计需要精确的气液两相质量传输关系,通过显微高速摄影测量了电加热炉中的悬挂液滴蒸发情况,得到了不同环境温度和气体组分条件下乙醇、煤油等五种液体燃料的定量蒸发率关系。经数据检验实验方法可行,最大相对误差不超过5%。实... 燃烧室设计需要精确的气液两相质量传输关系,通过显微高速摄影测量了电加热炉中的悬挂液滴蒸发情况,得到了不同环境温度和气体组分条件下乙醇、煤油等五种液体燃料的定量蒸发率关系。经数据检验实验方法可行,最大相对误差不超过5%。实验数据对比表明,常用的两相质量传输规律在燃烧室工作温度范围内有明显偏差。提出指数蒸发率模型,航空煤油等燃料的模型值与实验值的标准差小于0.23。 展开更多
关键词 液滴实验 体燃料 蒸发率 RP3航空煤油 指数模型
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次氯酸钠窦腔滴注液的制备及其稳定性 被引量:5
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作者 王金龙 厉辉 龙小华 《中国医院药学杂志》 CAS CSCD 北大核心 2001年第4期240-241,共2页
目的 :对次氯酸钠窦腔滴注液的制备及其稳定性进行研究。方法 :采用留样观察法。结果 :2 .5 %次氯酸钠液 ,pH =13时 ,t0 .9为 170d ,加入氮化硼作为稳定剂 ,t0 .9为 30 6d ,0 .0 2 5 %次氯酸钠窦腔滴注液 ,pH =7.2 ,含氮化硼 0 .0 0 75... 目的 :对次氯酸钠窦腔滴注液的制备及其稳定性进行研究。方法 :采用留样观察法。结果 :2 .5 %次氯酸钠液 ,pH =13时 ,t0 .9为 170d ,加入氮化硼作为稳定剂 ,t0 .9为 30 6d ,0 .0 2 5 %次氯酸钠窦腔滴注液 ,pH =7.2 ,含氮化硼 0 .0 0 75μg·ml-1时有效期为 18d。结论 :次氯酸钠窦腔滴注液在碱性 (pH =13)环境下稳定 。 展开更多
关键词 次氯酸钠 氮化硼 制备 稳定性 实验 强氧化性消毒剂
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工业高盐废水液滴蒸发特性研究进展
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作者 詹凌霄 陈恒 +2 位作者 赵宁 冯永新 杨林军 《水处理技术》 CAS CSCD 北大核心 2022年第4期1-5,共5页
雾化液滴蒸发特性是利用喷雾干燥法处理工业高盐废水的关键基础。综述了高盐废水液滴蒸发特性相关研究,首先介绍了喷雾蒸发技术处理工业废水的应用现状,通过对液滴群和单液滴蒸发特性进行了总结,分析表明,单液滴实验可以弥补液滴群实验... 雾化液滴蒸发特性是利用喷雾干燥法处理工业高盐废水的关键基础。综述了高盐废水液滴蒸发特性相关研究,首先介绍了喷雾蒸发技术处理工业废水的应用现状,通过对液滴群和单液滴蒸发特性进行了总结,分析表明,单液滴实验可以弥补液滴群实验无法反映液滴蒸发动态过程的缺陷。综述了高含固含盐溶液单液滴蒸发的理论和实验研究,比较了几类单液滴测试方法的优缺点,归纳了内外部因素对单液滴蒸发特性的影响,指出未来可依靠单液滴实验构建废水液滴干燥动力学模型,并将其耦合CFD精确描述喷雾蒸发进程,同时需要进一步开展对废水液滴蒸发特性的研究,根据废水水质等条件合理配置工艺参数控制蒸发进行,为废水零排放提供理论基础。 展开更多
关键词 高盐废水 蒸发特性 液滴实验 喷雾干燥 废水零排放
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首次液滴太空喜迁移
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《太空探索》 2003年第4期13-13,共1页
液滴热毛细迁移实验是神舟四号飞船有效载荷的一部分。
关键词 热毛细迁移实验 神舟四号飞船 有效载荷 浮力作用 温度梯度 运动轨迹 微重力环境 流体物理学 中国
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Experimental and Numerical Investigations of Single Drop Mass Transfer in Solvent Extraction Systems with Resistance in Both Phases 被引量:2
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作者 李天文 毛在砂 +1 位作者 陈家镛 费维扬 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2002年第1期1-14,共14页
Numerical simulation of transient mass transfer to a single dropcontrolled by the internal resistance or by the resistance in bothphases was mathematically formulated and simulated in aboundary-fitted orthogonal coord... Numerical simulation of transient mass transfer to a single dropcontrolled by the internal resistance or by the resistance in bothphases was mathematically formulated and simulated in aboundary-fitted orthogonal coordinate system. The simulated resultson the transient mass transfer dominated by the internal resistanceare in good agreement with the Newman and Kronig-Brink models fordrops with low Reynolds number. When the drop Reynolds number is upto 200, the mass transfer coefficient from numerical simulation isvery low as compared with The Handlos-Baron model. 展开更多
关键词 solvent extraction single drop numerical simulation mass transferexperiment
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Experimental Study on Thermal Interaction of LBE and Lead Droplet with Subcooled Water 被引量:2
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作者 R. Sa M. Takahashi 《Journal of Energy and Power Engineering》 2011年第7期579-589,共11页
Characteristics of thermal-hydraulic interaction of LBE (45w%Pb-55w%Bi) and lead with subcooled water in pool water were investigated experimentally. Two kinds of interaction zones (deformation and fragmentation) ... Characteristics of thermal-hydraulic interaction of LBE (45w%Pb-55w%Bi) and lead with subcooled water in pool water were investigated experimentally. Two kinds of interaction zones (deformation and fragmentation) and three kinds of interaction zones (solidification, deformation and fragmentation) were observed during LBE droplet/water interaction and lead droplet/water interaction, respectively. The fragmentation zone (FZ) could be identified exactly by two border lines: spontaneous nucleation temperature and minimum film boiling temperature. Within fragmentation zone, 10% to 35% tiny debris (diameter 〈 1 mm) of LBE and 5 to 8 kPa peak pressure generated with increasing the LBE temperature and no effect with increasing the subcooling of water. Only 2%-4% tiny debris (diameter 〈 1 mm) of lead and 2 kPa peak pressure generated regardless of lead and water temperature. 展开更多
关键词 Lead alloy droplet fast reactor fragmentation.
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节能型矿井排风热提取系统及风——水参数耦合优化探究
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作者 武梦婷 范帅杰 +1 位作者 吴汉 陈世强 《科技风》 2020年第16期157-157,共1页
为了突破排风与水压运行参数匹配的传统试凑法,缩短参数优化匹配耗时,达到更加高效地进行热湿交换,特设计矿井排风热提取系统。并进行单喷嘴上喷液滴群实验,运用控制变量法,在不同的喷嘴压差下,改变主通风机风量,由马尔文激光粒度分析... 为了突破排风与水压运行参数匹配的传统试凑法,缩短参数优化匹配耗时,达到更加高效地进行热湿交换,特设计矿井排风热提取系统。并进行单喷嘴上喷液滴群实验,运用控制变量法,在不同的喷嘴压差下,改变主通风机风量,由马尔文激光粒度分析仪测得在不同风量条件下喷水室各点的喷雾液滴粒径数据,绘制关联曲线图进行分析,得出排风与喷淋水的优化运行参数。 展开更多
关键词 矿井排风热提取系统 单喷嘴上喷实验 优化运行参数
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Numerical and Experimental Study on Droplet Spreading Motion after Impingement Considering Dynamic Contact Angle with CCUP (CIP-Combined Unified Procedure) Method
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作者 Soyoun Son Gwonhyun Ko Hongsun Ryou 《Journal of Energy and Power Engineering》 2013年第1期10-16,共7页
The contact angle is one of important parameters to simulate droplet spreading and impingement phenomena on the surface. In the most numerical research, it is assumed constant value and it is implemented as boundary c... The contact angle is one of important parameters to simulate droplet spreading and impingement phenomena on the surface. In the most numerical research, it is assumed constant value and it is implemented as boundary condition. However, contact angle is changed according to contact line velocity and time. Hence, for accurate simulation, dynamic contact angle which has various values as time elapsed is adopted. In the present study, the numerical analysis is performed on the droplet spreading phenomena considering dynamic contact angle function which is obtained from single droplet spreading experiment on the flat and bare surface. The CIP (cubic interpolated pseudo-particle) method by Yabe is used for analysis of interface between liquid and gas phases. The numerical results considering contact angle function which newly modeled as time and contact angle are compared with numerical results considering Hoffman's function and experimental data for range of Weber number which are 4.427 and 11.334. In contrast of numerical result considering Hoffman's function, the numerical result shows good agreement with experimental data as time elapsed in contact angle evolution, deformation of droplet spreading radius and height. Indeed, overall, the results display the increasing maximum spreading radius and the decreasing height as Weber numbers increased. 展开更多
关键词 CIP method droplet spreading height droplet spreading radius dynamic contact angle Hoffman's fimction.
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Experimental Study on Latent Heat Storage Characteristics of W/O Emulsion-Supercooling Rate of Dispersed Water Drops by Direct Contact Heat Exchange
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作者 Shin-ichi Morita Yasutaka Hayamizu +2 位作者 Akihiko Horibe Naoto Haruki Hideo Inaba 《Journal of Thermal Science》 SCIE EI CAS CSCD 2013年第2期145-151,共7页
Recently, much attention has been paid to investigate the latent heat storage system. Using of ice heat storage system brings an equalization of electric power demand, because it will solved the electric -power-demand... Recently, much attention has been paid to investigate the latent heat storage system. Using of ice heat storage system brings an equalization of electric power demand, because it will solved the electric -power-demand-concentration on day-time of summer by the air conditioning. The flowable latent heat storage material, Oil/Water type emulsion, microencapsulated latent heat material-water mixture or ice slurry, etc., is enable to transport the latent heat in a pipe. The flowable latent heat storage material can realize the pipe size reduction and system efficiency improvement. Supercooling phenomenon of the dispersed latent heat storage material in continuous phase brings the obstruction of latent heat storage. The latent heat storage rates of dispersed water drops in W/O (Water/Oil) emulsion are investigated experimentally in this study. The water drops in emulsion has the diameter within 3 ~ 25μm, the averaged water drop diameter is 7.3μm and the standard deviation is 2.9μm. The direct contact heat exchange method is chosen as the phase change rate evaluation of water drops in W/O emulsion. The supercooled temperature and the cooling rate are set as parameters of this study. The evaluation is performed by comparison between the results of this study and the past research. The obtained experimental result is shown that the 35K or more degree from melting point brings 100% latent heat storage rate of W/O emulsion. It was clarified that the supercooling rate of dispersed water particles in emulsion shows the larger value than that of the bulk water. 展开更多
关键词 Heat Storage Latent Heat W/O Emulsion Direct Contact Heat Exchange
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